Process for synthesizing alkylene bisdithiocarbamates or the ammonia
adducts thereof as well as mixtures that can be synthesized thereby
    9.
    发明授权
    Process for synthesizing alkylene bisdithiocarbamates or the ammonia adducts thereof as well as mixtures that can be synthesized thereby 失效
    用于合成亚二烷基双二硫代氨基甲酸酯或其氨加合物的方法以及可由其合成的混合物

    公开(公告)号:US4853475A

    公开(公告)日:1989-08-01

    申请号:US911364

    申请日:1986-09-25

    CPC classification number: C07C333/16

    Abstract: The invention relates to a process for synthesizing alkylene bisdithiocarbamates or the ammonia adducts thereof as well as mixtures that can be synthesized thereby. The starting materials are carbon disulfide, ammonia, a diamine and a metal oxide, which may be manganese(II) oxide, or the hydrate or hydroxide thereof. The metal oxide, its hydrate or hydroxide thereof is allowed to react either with a mixture syntheiszed from an alkylenediamine, carbon disulfide and ammonia in water, or with an aqueous solution of the ammonium alkylene bisdithiocarbamate. The concentration of the individual starting materials both relative to each other and to water is of prime importances as to which compounds in particular are ultimately obtained.

    Abstract translation: 本发明涉及一种合成亚二烷基双二硫代氨基甲酸酯或其氨加成物的方法以及可由其合成的混合物。 原料是二硫化碳,氨,二胺和金属氧化物,其可以是氧化锰(II)或其水合物或氢氧化物。 使金属氧化物,其水合物或氢氧化物与由亚烷基二胺,二硫化碳和氨在水中合成的混合物或与二亚硫代氨基甲酸亚烷基亚铵的水溶液反应。 各个起始材料相对于彼此和水的浓度对于最终获得哪些化合物是重要的。

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