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公开(公告)号：US20150191410A1
公开(公告)日：2015-07-09
申请号：US14413503
申请日：2013-06-18
Applicant: Oxea GmbH
Inventor： Guido D. Frey , Matthias Eisenacher , Kristina Kockrick , Heinz Strutz
IPC: C07C51/235 , C07C53/126 , C07C67/04 , C07C67/10 , C07C1/24 , C07C51/60 , C07C51/56 , C07C231/02 , C07D301/30 , C07C45/50 , C07C67/08
CPC classification number: C07C51/235 , C07C1/24 , C07C45/50 , C07C51/56 , C07C51/60 , C07C53/126 , C07C67/04 , C07C67/08 , C07C67/10 , C07C231/02 , C07C2521/04 , C07D301/30 , C07C11/02 , C07C47/02
Abstract: Process for preparing isononanoic acid proceeding from 2-ethylhexanol, characterized in that (a) 2-ethylhexanol is dehydrated to octene in the presence of a catalyst; (b) the octene obtained in step a) is reacted in the presence of a transition metal compound of group VIII of the periodic table of the elements with carbon monoxide and hydrogen to give isononanal; and (c) the isononanal obtained in step b) is oxidized to isononanoic acid.
Abstract translation: 由2-乙基己醇制备异壬酸的方法，其特征在于（a）2-乙基己醇在催化剂存在下脱水至辛烯; （b）步骤a）中获得的辛烯在元素周期表第Ⅷ族过渡金属化合物与一氧化碳和氢气存在下反应，得到异壬醛; 和（c）步骤b）中获得的异壬醛被氧化成异壬酸。
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2.发明申请Vinyl Esters of Isononanoic Acid Starting from 2-Ethyl Hexanol, Methods for the Production Thereof and Use Thereof 有权由2-乙基己醇开始的异壬酸的乙烯基酯，其生产方法和用途公开(公告)号：US20150166456A1
公开(公告)日：2015-06-18
申请号：US14413429
申请日：2013-06-19
Applicant: Oxea Gmbh
Inventor： Leif Johnen , Guido D. Frey , Matthias Eisenacher , Kristina Kockrick , Heinz Strutz
IPC: C07C67/04 , C07C51/21 , C08F220/68 , C07C1/24
CPC classification number: C07C67/04 , C07C1/24 , C07C45/50 , C07C51/14 , C07C51/21 , C07C51/235 , C07C67/10 , C07C2521/04 , C07C2521/08 , C07C2523/755 , C07C2527/173 , C08F220/68 , C07C11/02 , C07C47/02 , C07C53/126 , C07C69/24
Abstract: Process for preparing the vinyl ester of isononanoic acid starting out from 2-ethylhexanol, characterized in that (a) 2-ethylhexanol is dehydrated in the presence of a catalyst to form octene; (b) the octene obtained in step a) is converted into an isononanoic acid having one more carbon atom; and (c) the isononanoic acid obtained in step b) is converted into the corresponding vinyl ester.
Abstract translation: 从2-乙基己醇开始制备异壬酸乙烯基酯的方法，其特征在于（a）2-乙基己醇在催化剂存在下脱水形成辛烯; （b）将步骤a）中获得的辛烯转化为具有一个以上碳原子的异壬酸; 和（c）将步骤b）中获得的异壬酸转化成相应的乙烯基酯。
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公开(公告)号：US09434672B2
公开(公告)日：2016-09-06
申请号：US14413503
申请日：2013-06-18
Applicant: Oxea GmbH
Inventor： Guido D. Frey , Matthias Eisenacher , Kristina Kockrick , Heinz Strutz
IPC: C07C51/235 , C07C1/24 , C07C45/50 , C07C51/56 , C07C51/60 , C07C53/126 , C07C67/04 , C07C67/08 , C07C67/10 , C07C231/02 , C07D301/30
CPC classification number: C07C51/235 , C07C1/24 , C07C45/50 , C07C51/56 , C07C51/60 , C07C53/126 , C07C67/04 , C07C67/08 , C07C67/10 , C07C231/02 , C07C2521/04 , C07D301/30 , C07C11/02 , C07C47/02
Abstract: Process for preparing isononanoic acid proceeding from 2-ethylhexanol, characterized in that (a) 2-ethylhexanol is dehydrated to octene in the presence of a catalyst; (b) the octene obtained in step a) is reacted in the presence of a transition metal compound of group VIII of the periodic table of the elements with carbon monoxide and hydrogen to give isononanal; and (c) the isononanal obtained in step b) is oxidized to isononanoic acid.
Abstract translation: 由2-乙基己醇制备异壬酸的方法，其特征在于（a）2-乙基己醇在催化剂存在下脱水至辛烯; （b）步骤a）中获得的辛烯在元素周期表第Ⅷ族过渡金属化合物与一氧化碳和氢气存在下反应，得到异壬醛; 和（c）步骤b）中获得的异壬醛被氧化成异壬酸。
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4.发明授权Vinyl esters of isononanoic acid starting from 2-ethyl hexanol, methods for the production thereof and use thereof 有权从2-乙基己醇开始的异壬酸的乙烯基酯，其制备方法和用途公开(公告)号：US09334225B2
公开(公告)日：2016-05-10
申请号：US14413429
申请日：2013-06-19
Applicant: Oxea GmbH
Inventor： Leif Johnen , Guido D. Frey , Matthias Eisenacher , Kristina Kockrick , Heinz Strutz
IPC: C07B33/00 , C07C67/04 , C07C67/10 , C07C1/24 , C07C45/50 , C07C51/14 , C07C51/235 , C07C51/21 , C08F220/68
CPC classification number: C07C67/04 , C07C1/24 , C07C45/50 , C07C51/14 , C07C51/21 , C07C51/235 , C07C67/10 , C07C2521/04 , C07C2521/08 , C07C2523/755 , C07C2527/173 , C08F220/68 , C07C11/02 , C07C47/02 , C07C53/126 , C07C69/24
Abstract: Process for preparing the vinyl ester of isononanoic acid starting out from 2-ethylhexanol, characterized in that (a) 2-ethylhexanol is dehydrated in the presence of a catalyst to form octene; (b) the octene obtained in step a) is converted into an isononanoic acid having one more carbon atom; and (c) the isononanoic acid obtained in step b) is converted into the corresponding vinyl ester.
Abstract translation: 从2-乙基己醇开始制备异壬酸乙烯基酯的方法，其特征在于（a）2-乙基己醇在催化剂存在下脱水形成辛烯; （b）将步骤a）中获得的辛烯转化为具有一个以上碳原子的异壬酸; 和（c）将步骤b）中获得的异壬酸转化成相应的乙烯基酯。
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公开(公告)号：US09714201B2
公开(公告)日：2017-07-25
申请号：US14413444
申请日：2013-06-19
Applicant: Oxea GmbH
Inventor： Jens Theuerkauf , Guido D. Frey , Matthias Eisenacher , Kristina Kockrick , Heinz Strutz
IPC: C07C1/24 , C07C209/26 , C07C211/03 , C07C333/16 , C07C45/50 , C10M135/18
CPC classification number: C07C1/24 , C07C45/50 , C07C209/26 , C07C211/03 , C07C333/16 , C07C2521/04 , C10M135/18 , C07C11/02 , C07C47/02
Abstract: Process for preparing isononylamines starting out from 2-ethylhexanol, characterized in that (a) 2-ethylhexanol is dehydrated in the presence of a catalyst to form octene; (b) the octene obtained in step a) is reacted with carbon monoxide and hydrogen in the presence of a transition metal compound of group VIII of the Periodic Table of the Elements to form isononanal; and (c) the isononanal obtained in step b) is converted into isononylamines.
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Patent Agency Ranking
6.发明授权公开(公告)号：US09434675B2
公开(公告)日：2016-09-06
申请号：US14413550
申请日：2013-06-18
Applicant: Oxea GmbH
Inventor： Guido D. Frey , Matthias Eisenacher , Kristina Kockrick , Heinz Strutz
IPC: C07C67/08 , C07C1/24 , C07C45/50 , C07C51/235 , C10M129/70 , C10M129/74 , C07C29/48 , C08K5/103 , C08K5/10
CPC classification number: C07C67/08 , C07C1/24 , C07C29/48 , C07C45/50 , C07C51/235 , C07C2521/04 , C08K5/10 , C08K5/103 , C10M129/70 , C10M129/74 , C10M2207/281 , C10M2207/283 , C07C11/02 , C07C47/02 , C07C53/126 , C07C69/28 , C07C69/30 , C07C69/33
Abstract: A Process for preparing carboxylic esters of a mixture of structurally branched C9 monocarboxylic acids proceeding from 2-ethylhexanol is characterized in that (a) 2-ethylhexanol is dehydrated to an octene mixture in the presence of a catalyst; (b) the octene mixture obtained in step a) is reacted in the presence of a transition metal compound of group VIII of the periodic table of the elements with carbon monoxide and hydrogen to give a mixture of isomeric isononanals; (c) the mixture of isomeric isononanals obtained in step b) is oxidized to a mixture of structurally branched C9 monocarboxylic acids; and (d) the mixture of structurally branched C9 monocarboxylic acids obtained in step c) is reacted with alcohols to give carboxylic esters.
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7.发明申请公开(公告)号：US20150158805A1
公开(公告)日：2015-06-11
申请号：US14413550
申请日：2013-06-18
Applicant: Oxea GmbH
Inventor： Guido D. Frey , Matthias Eisenacher , Kristina Kockrick , Heinz Strutz
IPC: C07C67/08 , C10M129/70 , C08K5/103 , C07C29/48 , C07C51/235
CPC classification number: C07C67/08 , C07C1/24 , C07C29/48 , C07C45/50 , C07C51/235 , C07C2521/04 , C08K5/10 , C08K5/103 , C10M129/70 , C10M129/74 , C10M2207/281 , C10M2207/283 , C07C11/02 , C07C47/02 , C07C53/126 , C07C69/28 , C07C69/30 , C07C69/33
Abstract: A Process for preparing carboxylic esters of a mixture of structurally branched C9 monocarboxylic acids proceeding from 2-ethylhexanol is characterized in that (a) 2-ethylhexanol is dehydrated to an octene mixture in the presence of a catalyst; (b) the octene mixture obtained in step a) is reacted in the presence of a transition metal compound of group VIII of the periodic table of the elements with carbon monoxide and hydrogen to give a mixture of isomeric isononanals; (c) the mixture of isomeric isononanals obtained in step b) is oxidized to a mixture of structurally branched C9 monocarboxylic acids; and (d) the mixture of structurally branched C9 monocarboxylic acids obtained in step c) is reacted with alcohols to give carboxylic esters.
Abstract translation: 由2-乙基己醇制备的结构分支的C9单羧酸的混合物的羧酸酯的制备方法的特征在于：（a）2-乙基己醇在催化剂存在下脱水至辛烯混合物; （b）将步骤a）中获得的辛烯混合物在元素周期表第Ⅷ族的过渡金属化合物与一氧化碳和氢气存在下反应，得到异构异壬醛的混合物; （c）步骤b）中获得的异构异壬醛的混合物被氧化成结构支化的C9单羧酸的混合物; 和（d）将步骤c）中获得的结构分支的C 9单羧酸的混合物与醇反应，得到羧酸酯。
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8.发明授权公开(公告)号：US09695100B1
公开(公告)日：2017-07-04
申请号：US15311676
申请日：2015-06-26
Applicant: Oxea GmbH
Inventor： Kristina Kockrick , Leif Johnen , Heinz Strutz
IPC: C07C51/00 , C07C53/128 , C07C51/373
CPC classification number: C07C51/373 , C07C51/00 , C07C53/128
Abstract: A process for producing a mixture comprising tertiary isononanoic acids proceeding from 2-ethylhexanol is characterized in that 2-ethylhexanol is (a) reacted at a temperature of 0° C. to 40° C. with a mixture of concentrated formic acid and a concentrated Brønsted acid, wherein 2 to 10 mol of formic acid are used per mole of 2-ethylhexanol and the concentrated Brønsted acid is used in an amount that corresponds to 6 to 90 mol of protons per mole of 2-ethylhexanol. The resulting reaction mixture from step (a) is subsequently (b) brought into contact with water, and the mixture comprising tertiary isononanoic acids formed according to step b) is removed.
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公开(公告)号：US20150167029A1
公开(公告)日：2015-06-18
申请号：US14406910
申请日：2013-07-01
Applicant: Oxea GmbH
Inventor： Jens Klabunde , Heinz Strutz , Kristina Kockrick
CPC classification number: C12P7/52 , C07C45/50 , C07C51/14 , C07C51/235 , C07C51/295 , C12P5/026 , C12P7/24 , C07C53/126 , C07C47/02
Abstract: The present invention relates to a method of producing isopentane derivatives from fermentatively produced isobutene, the higher purity of which improves the method and the properties of the produced isopentane derivatives.
Abstract translation: 本发明涉及由发酵生产的异丁烯生产异戊烷衍生物的方法，其纯度越高，改进了所生产的异戊烷衍生物的方法和性质。
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10.发明申请Isononylamines from 2-Ethylhexanol, Processes for Their Preparation, and Their Use 有权来自2-乙基己醇的异壬基胺，其制备方法及其用途公开(公告)号：US20150152023A1
公开(公告)日：2015-06-04
申请号：US14413444
申请日：2013-06-19
Applicant: Oxea GmbH
Inventor： Jens Theuerkauf , Guido D. Frey , Matthias Eisenacher , Kristina Kockrick , Heinz Strutz
IPC: C07C1/24 , C10M135/18 , C07C211/03 , C07C333/16 , C07C45/50 , C07C209/26
CPC classification number: C07C1/24 , C07C45/50 , C07C209/26 , C07C211/03 , C07C333/16 , C07C2521/04 , C10M135/18 , C07C11/02 , C07C47/02
Abstract: Process for preparing isononylamines starting out from 2-ethylhexanol, characterized in that (a) 2-ethylhexanol is dehydrated in the presence of a catalyst to form octene; (b) the octene obtained in step a) is reacted with carbon monoxide and hydrogen in the presence of a transition metal compound of group VIII of the Periodic Table of the Elements to form isononanal; and (c) the isononanal obtained in step b) is converted into isononylamines.
Abstract translation: 从2-乙基己醇开始制备异壬基胺的方法，其特征在于（a）2-乙基己醇在催化剂存在下脱水形成辛烯; （b）步骤a）中获得的辛烯在元素周期表第Ⅷ族过渡金属化合物存在下与一氧化碳和氢气反应形成异壬醛; 和（c）步骤b）中获得的异壬醛转化为异壬基胺。
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