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    TRANSAMINATION OF NITROGEN-CONTAINING COMPOUNDS TO MAKE CYCLIC AND CYCLIC/ACYCLIC POLYAMINE MIXTURES
    8.
    发明申请
    TRANSAMINATION OF NITROGEN-CONTAINING COMPOUNDS TO MAKE CYCLIC AND CYCLIC/ACYCLIC POLYAMINE MIXTURES 有权
    含氮化合物的复合以制备环状和环状/环状聚胺混合物

    公开(公告)号：US20130231476A1

    公开(公告)日：2013-09-05

    申请号：US13884430

    申请日：2011-10-20

    申请人： Stephen W. King

    发明人： Stephen W. King

    IPC分类号： C07D295/023 ,  C07D295/13

    CPC分类号： C07D295/023 ,  C07D243/08 ,  C07D295/13

    摘要： A transamination process is described to prepare polyamine product mixtures from reactants comprising mixed nitrogen-containing compounds with binary carbon spacing between nitrogen-containing groups (a binary component). A second nitrogen-containing component with a second carbon atom spacing between nitrogen-containing groups may also be employed. The molar ratio between the binary and second components can be adjusted to customize the product composition for desired end uses.

    摘要翻译： 描述了一种转氨过程，以从包含含氮基团（二元组分）之间的二元碳间隔的混合含氮化合物的反应物制备多胺产物混合物。 也可以使用在含氮基团之间具有第二碳原子间隔的第二含氮组分。 可以调整二元和第二成分之间的摩尔比以定制所需最终用途的产品组成。

    METHOD FOR THE CONTINUOUS SEPARATION OF MIXTURES COMPRISING MORPHONLINE (MO), MONOAMINODIGLYCOL (ADG), AMMONIA AND WATER BY MEANS OF DISTILLATION
    9.
    发明申请
    METHOD FOR THE CONTINUOUS SEPARATION OF MIXTURES COMPRISING MORPHONLINE (MO), MONOAMINODIGLYCOL (ADG), AMMONIA AND WATER BY MEANS OF DISTILLATION 有权
    通过蒸馏法连续分离含有摩尔（MO），单胺基（ADG），氨和水的混合物的方法

    公开(公告)号：US20120024689A1

    公开(公告)日：2012-02-02

    申请号：US12443581

    申请日：2007-09-12

    申请人： Helmut Schmidtke ,  Oliver Bußmann ,  Ralph Versch ,  Udo Rheude ,  Uwe Leyk ,  Manfred Julius ,  Martin Rudloff ,  Erhard Henkes

    发明人： Helmut Schmidtke ,  Oliver Bußmann ,  Ralph Versch ,  Udo Rheude ,  Uwe Leyk ,  Manfred Julius ,  Martin Rudloff ,  Erhard Henkes

    IPC分类号： B01D3/34 ,  B01D3/14

    CPC分类号： C07C213/10 ,  C07D295/023 ,  C07C217/08

    摘要： Processes for the continuous fractional distillation of a mixture comprising morpholine (MO), monoaminodiglycol (ADG), ammonia and water from a reaction of diethylene glycol (DEG) with ammonia, the process comprising: (i) separating off ammonia from the mixture at a top of a first distillation column K10; (ii) feeding a bottom fraction from the first distillation column to a second distillation column K20, wherein water and an organic product are separated off at a top of the second distillation column at a top temperature of 45 to 198° C. and a pressure in the range from 0.1 to 15 bar; (iii) feeding a bottom fraction from the second distillation column to a third distillation column K30, wherein morpholine and an organic product having a boiling point of 190° C. (1.013 bar) are separated off at a bottom of the third ditillation column, and (iv) feeding the morpholine-comprising stream from the third distillation column to a fourth column K40, wherein morpholine is separated off at a side offtake of the fourth column, an organic product having a boiling point of ≦128° C. (1.013 bar) is separated off at a top of the fourth distillation column and an organic product having a boiling point of ≧128° C. (1.013 bar) is separated off at a bottom of the fourth distillation column.

    摘要翻译： 用于从二甘醇（DEG）与氨的反应连续分馏含有吗啉（MO），单氨基二甘醇（ADG），氨和水的混合物的方法，该方法包括：（i）在 第一蒸馏塔K10顶部; （ii）将底部馏分从第一蒸馏塔进料到第二蒸馏塔K20，其中在顶部温度为45至198℃的温度下，在第二蒸馏塔的顶部分离出水和有机产物，并将压力 在0.1至15巴的范围内; （iii）将第二蒸馏塔的塔底馏分进料到第三蒸馏塔K30，其中将吗啉和沸点<140℃（1.013巴）的有机产物在选自顶部和 在第三蒸馏塔的底部分离出第三蒸馏塔的侧馏分和单胺二醇和沸点> 190℃（1.013巴）的有机产物，（iv）将含吗啉 从第三蒸馏塔到第四塔K40的流，其中吗啉在第四塔的出口侧分离出，沸点为＆amp; NlE的有机产物为128℃（1.013巴）在顶部分离 的第四蒸馏塔和沸点为≧128℃的有机产物（1.013巴）在第四蒸馏塔的底部分离。