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    Method for the production of 4,4′-[1-(trifluoromethyl)alkylidene]-bis-(2,6-diphenylphenols)
    2.
    再颁专利
    Method for the production of 4,4′-[1-(trifluoromethyl)alkylidene]-bis-(2,6-diphenylphenols) 有权
    制备4,4' - [1-（三氟甲基）亚烷基] - 双（2,6-二苯基苯酚）

    公开(公告)号：USRE46151E1

    公开(公告)日：2016-09-20

    申请号：US14321865

    申请日：2014-07-02

    申请人： BASF SE

    发明人： Gabriele Gralla ,  Gunnar Heydrich ,  Klaus Ebel ,  Wolfgang Krause

    IPC分类号： C07C39/16 ,  C07C39/12 ,  C07C45/74 ,  C07C37/07 ,  C07C37/20 ,  C07C37/62

    CPC分类号： C07C45/74 ,  C07C37/07 ,  C07C37/20 ,  C07C37/62 ,  C07C49/613 ,  C07C49/653 ,  C07C39/15 ,  C07C39/367

    摘要： The present invention relates to a process for preparing 4,4′-[1-(trifluoromethyl)alkylidene]bis(2,6-diphenylphenols), in particular for preparing 4,4′-[1-(trifluoromethyl)ethylidene]bis(2,6-diphenylphenol), which comprises the self-condensation of cyclohexanone in the presence of a basic catalyst to form tricyclic condensation products, dehydrogenation of the resulting tricyclic condensation products in the presence of a supported transition metal catalyst in the condensed phase to form 2,6-diphenylphenol and reaction of the 2,6-diphenylphenol with a trifluoromethyl ketone. The invention further provides an improved process for preparing 2,6-diphenylphenol by aldol self-condensation of cyclohexanone.

    摘要翻译： 本发明涉及一种制备4,4' - [1-（三氟甲基）亚烷基]双（2,6-二苯基苯酚）的方法，特别是制备4,4' - [1-（三氟甲基）亚乙基]双（ 2,6-二苯基苯酚），其包括环己酮在碱性催化剂存在下的自缩合以形成三环缩合产物，所得三环缩合产物在冷凝相中负载的过渡金属催化剂存在下脱氢形成 2,6-二苯基苯酚和2,6-二苯基苯酚与三氟甲基酮的反应。 本发明还提供了通过环己酮的醛醇自缩合制备2,6-二苯基苯酚的改进方法。

    METHOD FOR THE PRODUCTION OF 4,4'-[1-TRIFLUOROMETHYL)ALKYLIDENE]-BIS-(2,6-DIPHENYLPHENOLS)
    7.
    发明申请
    METHOD FOR THE PRODUCTION OF 4,4'-[1-TRIFLUOROMETHYL)ALKYLIDENE]-BIS-(2,6-DIPHENYLPHENOLS) 有权
    生产4,4' - [1-三氟甲基）亚苄基] -BIS-（2,6-二苯基苯酚）的方法

    公开(公告)号：US20100312020A1

    公开(公告)日：2010-12-09

    申请号：US12808865

    申请日：2008-12-17

    申请人： Gabriele Gralla ,  Gunnar Heydrich ,  Klaus Ebel ,  Wolfgang Krause

    发明人： Gabriele Gralla ,  Gunnar Heydrich ,  Klaus Ebel ,  Wolfgang Krause

    IPC分类号： C07C37/62 ,  C07C37/00

    CPC分类号： C07C45/74 ,  C07C37/07 ,  C07C37/20 ,  C07C37/62 ,  C07C49/613 ,  C07C49/653 ,  C07C39/15 ,  C07C39/367

    摘要： The present invention relates to a process for preparing 4,4′-[1-(trifluoromethyl)alkylidene]bis(2,6-diphenylphenols), in particular for preparing 4,4′-[1-(trifluoromethyl)ethylidene]bis(2,6-diphenylphenol), which comprises the self-condensation of cyclohexanone in the presence of a basic catalyst to form tricyclic condensation products, dehydrogenation of the resulting tricyclic condensation products in the presence of a supported transition metal catalyst in the condensed phase to form 2,6-diphenylphenol and reaction of the 2,6-diphenylphenol with a trifluoromethyl ketone. The invention further provides an improved process for preparing 2,6-diphenylphenol by aldol self-condensation of cyclohexanone.

    摘要翻译： 本发明涉及一种制备4,4' - [1-（三氟甲基）亚烷基]双（2,6-二苯基苯酚）的方法，特别是制备4,4' - [1-（三氟甲基）亚乙基]双（ 2,6-二苯基苯酚），其包括环己酮在碱性催化剂存在下的自缩合以形成三环缩合产物，所得三环缩合产物在冷凝相中负载的过渡金属催化剂存在下脱氢形成 2,6-二苯基苯酚和2,6-二苯基苯酚与三氟甲基酮的反应。 本发明还提供了通过环己酮的醛醇自缩合制备2,6-二苯基苯酚的改进方法。

    METHOD OF PRODUCING IODIZING AGENT, AND METHOD OF PRODUCING AROMATIC IODINE COMPOUND
    9.
    发明申请
    METHOD OF PRODUCING IODIZING AGENT, AND METHOD OF PRODUCING AROMATIC IODINE COMPOUND 失效
    生产化学试剂的方法和生产芳族碘化合物的方法

    公开(公告)号：US20100105969A1

    公开(公告)日：2010-04-29

    申请号：US12530274

    申请日：2008-03-07

    申请人： Junichi Yoshida ,  Seiji Suga ,  Kazuhide Kataoka ,  Koji Midorikawa ,  Yuji Hagiwara

    发明人： Junichi Yoshida ,  Seiji Suga ,  Kazuhide Kataoka ,  Koji Midorikawa ,  Yuji Hagiwara

    IPC分类号： C07C17/02 ,  C25B1/24

    CPC分类号： C07C17/02 ,  C07B39/00 ,  C07C17/12 ,  C07C37/62 ,  C07C41/22 ,  C07C209/74 ,  C07C253/30 ,  C25B1/24 ,  C25B3/06 ,  C07C25/18 ,  C07C25/22 ,  C07C211/52 ,  C07C255/50 ,  C07C39/27 ,  C07C43/225

    摘要： A method of the present invention, for producing an iodizing agent, includes the step of electrolyzing iodine molecules in a solution by using an acid as a supporting electrolyte. This realizes (i) a method of producing an iodine cation suitable for use as an iodizing agent that does not require a sophisticated separation operation after iodizing reaction is completed, and (ii) an electrolyte used in the method. Further, a method of the present invention, for producing an aromatic iodine compound, includes the step of causing an iodizing agent, and an aromatic compound whose nucleus has one or more substituent groups and two or more hydrogen atoms, to react with each other under the presence of a certain ether compound. This realizes such a method of producing an aromatic iodine compound that position selectivity in iodizing reaction of an aromatic compound is improved.

    摘要翻译： 本发明的制备碘化剂的方法包括通过使用酸作为支持电解质在溶液中电解碘分子的步骤。 这实现了（i）生产适合用作碘化剂的碘阳离子的方法，其在碘化反应完成后不需要复杂的分离操作，和（ii）该方法中使用的电解质。 此外，本发明的芳香族碘化合物的制造方法包括使碘化剂和其中具有一个以上取代基和两个以上氢原子的芳香族化合物在其下反应的工序 存在某种醚化合物。 这实现了提高芳族化合物的碘化反应中选择性的芳香族碘化合物的制造方法。