公开(公告)号：US20240327323A1

公开(公告)日：2024-10-03

申请号：US18584756

申请日：2024-02-22

申请人： REGENTS OF THE UNIVERSITY MICHIGAN

发明人： Anne J. McNeil ,  Danielle Fagnani ,  Dukhan Kim ,  Rahul Jha

IPC分类号： C07C41/22 ,  C25B3/11 ,  C25B3/25 ,  C25B3/27

CPC分类号： C07C41/22 ,  C25B3/11 ,  C25B3/25 ,  C25B3/27

摘要： A method for halogenation of an organic compound with a halogen from a waste source comprising a halogen containing polymer includes admixing waste source with the organic compound, a solvent, and an electrolyte, wherein the solvent swells and/or dissolves the halogen containing polymer in the waste source; and exposing the admixture to a negative voltage in an electrochemical cell comprising a cathode and an oppositely disposed anode. The halogen containing polymer is dehalogenated by the cathode to generate a halogen anion. The halogen anode is formed into a reactive halogen species by the anode. The halogen species reacts with the organic compound to halogenate the organic compound

公开(公告)号：US20230331651A1

公开(公告)日：2023-10-19

申请号：US18212841

申请日：2023-06-22

申请人： AGC INC.

发明人： Taku YAMADA ,  Toshifumi NIHEI

IPC分类号： C07C41/22 ,  C07C41/46

CPC分类号： C07C41/22 ,  C07C41/46

摘要： To provide a method for producing a fluorovinyl ether compound, whereby it is possible to suppress the generation of byproducts. The method for producing a fluorovinyl ether compound of the present invention is a method for producing a fluorovinyl ether compound, which comprises heat-treating a compound having a group represented by the formula (1): F—C(═O)—CF(X)—(CF2)n—O— in the presence of an oxide containing at least one element selected from the group consisting of alkali metal elements and alkaline earth metal elements, to obtain a fluorovinyl ether compound having a group represented by the formula (2): CF2═CF—O—, wherein the specific surface area of the oxide before the heat treatment is at least 1.0 m2/g. In the formula (1), n is 0 or 1, wherein when n is 0, X is CF3 and when n is 1, X is F.

公开(公告)号：US20230312454A1

公开(公告)日：2023-10-05

申请号：US18303008

申请日：2023-04-19

申请人： Shin-Etsu Chemical Co., Ltd.

发明人： Yuki Miyake ,  Takeshi Kinsho ,  Yusuke Nagae

IPC分类号： C07C67/08 ,  C07C29/132 ,  C07C41/22 ,  C07C41/24 ,  C07C41/30 ,  C07C43/178

CPC分类号： C07C67/08 ,  C07C29/132 ,  C07C41/22 ,  C07C41/24 ,  C07C41/30 ,  C07C43/178

摘要： The present invention relates to a 6-hydroxy-3-hexenyl alkoxymethyl ether compound of the following general formula (1): HOCH2CH2CH=CHCH2CH2OCH2OCH2R1 (1), R1 representing a hydrogen atom, an n-alkyl group having 1 to 9 carbon atoms, or a phenyl group; and also relates to a process for preparing a 3,13-octadecadien-1-ol compound of the following formula (6): CH3(CH2)3CH=CH(CH2)8CH=CHCH2CH2OH (6) from the 6-hydroxy-3-hexenyl alkoxymethyl ether compound (1).

公开(公告)号：US20230242468A1

公开(公告)日：2023-08-03

申请号：US18127959

申请日：2023-03-29

申请人： DAIKIN INDUSTRIES, LTD.

发明人： Atsushi SHIRAI ,  Takashi NAMIKAWA ,  Sumi ISHIHARA ,  Kenji ADACHI ,  Yosuke KISHIKAWA ,  Yoshichika KUROKI

IPC分类号： C07C41/22 ,  C07C319/20 ,  C07C231/02 ,  C07C41/06

CPC分类号： C07C41/22 ,  C07C319/20 ,  C07C231/02 ,  C07C41/06 ,  C07C2601/14

摘要： Provided is a novel production method for a fluorinated organic compound (1), the method comprising step A of fluorinating a hydrogen atom-containing organic compound (2) using IF5 in a liquid composition comprising an organic solvent, the amount of the hydrogen atom-containing organic compound (2) being 1.8 mol or more per liter of the organic solvent.

公开(公告)号：US20190152779A1

公开(公告)日：2019-05-23

申请号：US16261737

申请日：2019-01-30

申请人： DAIKIN INDUSTRIES, LTD. ,  NATIONAL UNIVERSITY CORPORATION HOKKAIDO UNIVERSITY

发明人： Shoji HARA ,  Yosuke KISHIKAWA ,  Atsushi SHIRAI ,  Takashi NAMIKAWA ,  Sumi ISHIHARA

IPC分类号： C01B7/24 ,  C07C67/307 ,  C01D3/02 ,  C07D309/10 ,  C07C17/354 ,  C07C17/361 ,  C07C41/22 ,  C07C45/63 ,  C07C45/67 ,  C07D493/04 ,  C07C67/333 ,  C07C209/74 ,  C07C231/12 ,  C07C319/20 ,  C07D209/10 ,  C01D13/00

CPC分类号： C01B7/24 ,  C01D3/02 ,  C01D13/00 ,  C07C17/354 ,  C07C17/361 ,  C07C41/22 ,  C07C45/63 ,  C07C45/673 ,  C07C67/307 ,  C07C67/333 ,  C07C209/74 ,  C07C231/12 ,  C07C319/20 ,  C07C2603/86 ,  C07D209/10 ,  C07D309/10 ,  C07D493/04

摘要： An object of the present invention is to provide a novel substance that has a high reactivity as a fluorinating agent, is effectively used in various fluorination reactions, and is safely handled even in air. As the solution for achieving this object, the present invention provides a complex obtained by reacting bromine trifluoride with at least one metal halide selected from the group consisting of halogenated metals and halogenated hydrogen metals in a nonpolar solvent. This complex serves as a fluorinating agent that provides excellent fluorination performance and that is stable in air.

公开(公告)号：US10071943B2

公开(公告)日：2018-09-11

申请号：US15303087

申请日：2015-04-10

申请人： THE REGENTS OF THE UNIVERSITY OF MICHIGAN

发明人： Peter J. H. Scott ,  Melanie S. Sanford ,  Naoko Ichiishi ,  Allen F. Brooks ,  Melissa Rodnick ,  Joseph J. Topczewski

IPC分类号： C07C41/22 ,  A61K51/04 ,  C07B59/00 ,  C07C231/12 ,  C07C233/51 ,  C07C67/307 ,  C07C45/63 ,  C07C17/361 ,  C07C51/363 ,  C07J1/00

CPC分类号： C07C41/22 ,  A61K51/04 ,  A61K51/0402 ,  A61K51/0493 ,  C07B59/00 ,  C07B2200/05 ,  C07C17/361 ,  C07C45/63 ,  C07C51/363 ,  C07C67/307 ,  C07C231/12 ,  C07C233/51 ,  C07J1/0066 ,  C07C233/15 ,  C07C69/76 ,  C07C47/55 ,  C07C43/225

摘要： Copper-catalyzed radiofluorination of iodonium salts, iodonium salts, and compounds obtained by copper-catalyzed radiofluorination of iodonium salts are disclosed. Diagnostic and therapeutic methods involving such compounds also are disclosed.

公开(公告)号：US20180222834A1

公开(公告)日：2018-08-09

申请号：US15473940

申请日：2017-03-30

申请人： CENTRAL GLASS COMPANY, LIMITED

发明人： Takaaki YOSHIMURA ,  Toshihiko OONO ,  Shinya AKIBA ,  Masaki FUJIWARA

IPC分类号： C07C41/42 ,  C07C41/22

CPC分类号： C07C41/42 ,  C07C41/22 ,  C07C41/44 ,  C07C43/123

摘要： An object of the present invention is to remove a compound A from “sevoflurane containing fluoromethyl-1,1,3,3,3-pentafluoroisopropenyl ether (compound A)” so as to collect high-purity sevoflurane. The present invention concerns a method for producing sevoflurane containing substantially no compound A, comprising the following steps of: bringing a composition containing hydrogen fluoride (HF) and water at a mass ratio of 1:1 to 1:30 into contact with a 1st organic liquid containing sevoflurane and a compound A, thereby obtaining a 2nd organic liquid containing the compound A in an amount that is lower than that in the 1st organic liquid (step 1a); and distilling the 2nd organic liquid under the presence of a degradation inhibitor, thereby obtaining sevoflurane containing substantially no compound A as a main distillation fraction (step 2).

公开(公告)号：US09914964B2

公开(公告)日：2018-03-13

申请号：US14523410

申请日：2014-10-24

申请人： LIFE TECHNOLOGIES CORPORATION

发明人： Parul Angrish ,  Zhiwei Yang

IPC分类号： C12Q1/68 ,  C07D207/16 ,  C07C41/22 ,  C07C211/63 ,  C07C303/28 ,  C07D211/60 ,  C11D1/88 ,  C12N9/12 ,  C12N9/96

CPC分类号： C12Q1/686 ,  C07C41/22 ,  C07C211/63 ,  C07C303/28 ,  C07D207/16 ,  C07D211/60 ,  C11D1/88 ,  C12N9/1252 ,  C12N9/96

摘要： This disclosure relates to novel compounds for use in various compositions, kits and methods, including, for example, use in polymerase storage buffers and in nucleic acid synthesis or amplification reactions such as a polymerase chain reaction (PCR). Methods for preparing the novel compounds are also described.

公开(公告)号：US20180037526A1

公开(公告)日：2018-02-08

申请号：US15549040

申请日：2016-02-09

申请人： The Trustees of Princeton University

发明人： John T. Groves ,  Xiongyi Huang

IPC分类号： C07C17/363 ,  B01J31/32 ,  C07B39/00 ,  B01J31/22 ,  C07C22/08 ,  C07C23/46

CPC分类号： C07C17/363 ,  B01J31/22 ,  B01J31/32 ,  C07B39/00 ,  C07B2200/05 ,  C07C22/08 ,  C07C23/46 ,  C07C41/22 ,  C07C45/676 ,  C07C67/297 ,  C07C253/30 ,  C07C255/35 ,  C07C2601/14 ,  C07C2603/74 ,  C07D209/46 ,  C07D209/48 ,  C07D319/20 ,  C07D333/12 ,  C07D493/18 ,  C07J1/0059 ,  C07C22/00 ,  C07C43/225 ,  C07C49/813 ,  C07C69/65

摘要： Methods of preparing fluorinated compounds by carboxylative fluorination using fluoride are contained herein. Fluorinated compounds are provided. Methods of using fluorinated compounds are contained herein.

公开(公告)号：US20170137448A1

公开(公告)日：2017-05-18

申请号：US15312694

申请日：2015-04-23

申请人： THE GOVERNING COUNCIL OF THE UNIVERSITY OF TORONTO

发明人： CONOR PRANCKEVICIUS ,  DOUGLAS WADE STEPHAN

IPC分类号： C07F15/00

CPC分类号： C07F15/0046 ,  C07C5/03 ,  C07C29/172 ,  C07C41/22 ,  C07C45/63 ,  C07C67/303 ,  C07C201/12 ,  C07C2531/22 ,  C07C2601/14 ,  C08C19/02 ,  C08L15/005 ,  C07C9/15 ,  C07C9/18 ,  C07C13/18 ,  C07C15/073 ,  C07C205/06 ,  C07C69/34 ,  C07C49/403 ,  C07C35/08 ,  C07C43/184

摘要： The present invention provides stable, cyclic bent allene metal complexes and methods of conducting chemical processes, preferably olefin hydrogenation, comprising contacting an olefin substrate, preferably an unsaturated polymer, with a cyclic bent allene metal complex as described herein, under hydrogenation conditions.