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公开(公告)号：US11634659B2
公开(公告)日：2023-04-25
申请号：US17261444
申请日：2018-07-23
申请人： SYMRISE AG
IPC分类号： C11D3/50 , C11B9/00 , A61K8/35 , A61Q5/02 , C07C29/14 , C07C35/08 , C07C47/32 , C07C49/403 , C11D3/00 , C11D3/20 , C11D17/06
摘要： The present invention primarily concerns the use of compounds of the following formula (I) wherein X represents an oxygen atom, a —CHO, an —OH, or a —CH2OH group, a single bond or a double bond is present at the respective location of one of the dotted lines, at least one double bond is present when X is an OH group, and the 3-isopentyl or 3-isopent-2-enyl residue is connected to the ring in the ortho, meta, or para position to the X group, as perfuming and/or flavouring agents. The invention further relates to fragrance and flavour compositions containing one or more of these compounds, perfumed or flavoured articles comprising one or more of these compounds and corresponding processes for imparting, modifying and/or enhancing certain odour notes.
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公开(公告)号：US10994263B2
公开(公告)日：2021-05-04
申请号：US16130008
申请日：2018-09-13
申请人： George Chase , Dinesh Lolla , Ahmed Abutaleb
发明人： George Chase , Dinesh Lolla , Ahmed Abutaleb
IPC分类号： C07C49/403 , B01J23/44 , B01J35/06 , B01J35/00 , B01J37/34 , B01J37/02 , B01J31/06 , B01J37/08 , B01J23/46 , B01J21/06 , B01J23/42 , B01J23/52
摘要： A polymer-catalyst assembly includes polarized polymeric nanofibers retaining a plurality of catalytic metallic nanoparticles. A method of making the polarized polymer-catalyst assembly may include providing a fiber mat having polymeric nanofibers retaining a plurality of catalytic metallic nanoparticles, stretching the fiber mat in a uniaxial direction, simultaneous with the step of stretching, thermally heating the fiber mat, simultaneous with the steps of stretching and thermally heating, subjecting the fiber mat to an electric field, whereby the simultaneous steps of stretching, thermally heating, and subjecting thereby form a polarized fiber mat.
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公开(公告)号：US10246397B2
公开(公告)日：2019-04-02
申请号：US16066540
申请日：2016-12-22
申请人： INSTITUTO SUPERIOR TÉCNICO , INSTITUTO SUPERIOR DE ENGENHARIA DE LISBOA , UNIVERSIDADE DO PORTO
发明人： Armando Jose L. De Oliveira Pombeiro , Luisa Margarida Dias R. De Sousa Martins , Ana Paula Da Costa Ribeiro , Sonia Alexandra Correia Carabineiro , Jose Luis Cabral Da Conceicao
IPC分类号： C07C45/29 , B01J31/00 , C07C49/403 , C07C49/78 , B01J31/18
摘要： The present invention relates to the process for production of ketones from secondary alcohols by the use of a hybrid material, formed by the dichlorohydrotris(pyrazol-1-yl)methane iron (II) complex covalently bound to multi-walled carbon nanotubes functionalized with superficial carboxylate groups, as efficient and selective catalyst of peroxidative oxidation, microwave-assisted and without solvent addition.
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公开(公告)号：US10130895B2
公开(公告)日：2018-11-20
申请号：US15535795
申请日：2015-12-15
申请人： CAP III B.V.
IPC分类号： B01D3/00 , C07C45/82 , B01D3/12 , B01D3/10 , B01D3/14 , C07C27/28 , C07C35/08 , C07C45/00 , C07C49/403
摘要： A process for the construction of a second chemical plant, which second chemical plant is suitable for the separation of cyclohexanone from a second mixture, which second mixture comprises reaction products from the hydrogenation of phenol. The process comprises providing a first chemical plant, which first chemical plant is suitable for the separation of cyclohexanone from a first mixture, and a second chemical plant comprising a distillation column suitable for distilling overhead cyclohexanone reused from the first chemical plant.
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公开(公告)号：US20180194705A1
公开(公告)日：2018-07-12
申请号：US15743367
申请日：2016-06-17
发明人： Jihad M. Dakka , Ashley J. Malik , Christopher L. Becker , Jason D. Davis , Kirk C. Nadler , Jose M. Vargas , Tan-Jen Chen , Seth M. Washburn , Jörg F.W. Weber
CPC分类号： C07C45/006 , B01J8/06 , B01J23/44 , B01J23/58 , B01J23/96 , B01J35/008 , B01J38/04 , B01J38/06 , B01J38/10 , B01J38/12 , B01J38/50 , B01J38/52 , B01J38/56 , B01J38/64 , B01J2219/00081 , B01J2219/00162 , C07C2/74 , C07C37/001 , C07C49/403 , C07C407/00 , C07C2601/14 , Y02P20/584
摘要： Disclosed are novel processes for making cyclohexanone compositions, from a mixture comprising phenol, cyclohexanone, and cyclohexylbenzene. The process includes hydrogenation of a feed stream comprising phenol, cyclohexanone, and cyclohexylbenzene. The feed stream may be subjected to one or more pre-hydrogenation treatments, such as passing through one or more sorbents, addition of basic chemical agents, and/or addition of water, so as to improve catalyst activity, minimize undesired side reactions, and/or remove catalyst poisons from the feed stream. The feed stream may be provided to a hydrogenation reaction zone in the vapor phase, with periodic alterations to hydrogenation reaction conditions such that the feed is provided in mixed liquid and vapor phase in order to carry out liquid washing of a hydrogenation catalyst bed within the hydrogenation reaction zone.
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公开(公告)号：US20180065903A1
公开(公告)日：2018-03-08
申请号：US15551839
申请日：2016-01-15
IPC分类号： C07C7/08 , C07C7/12 , C07C37/80 , C07C37/82 , C07C45/79 , C07C45/83 , C07C39/04 , C07C49/403
CPC分类号： C07C7/08 , C07C7/04 , C07C7/12 , C07C37/80 , C07C37/82 , C07C39/04 , C07C45/79 , C07C45/82 , C07C45/83 , C07C49/403 , C07C2601/14 , C07C13/28
摘要： In a process for separating a mixture comprising cyclohexanone and phenol, a solid-phase basic material, such as basic ion-exchange resin, is used to remove acid and/or sulfur from the mixture prior to separation. The process results in reduced amount of contamination such as cyclic ethers in the cyclohexanone and/or phenol products.
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公开(公告)号：US09815759B2
公开(公告)日：2017-11-14
申请号：US14800042
申请日：2015-07-15
IPC分类号： C07C49/403 , C07C407/00 , C07C37/82 , C07C37/86 , C07C45/85 , C07C37/08 , C07C39/04
CPC分类号： C07C49/403 , C07C37/08 , C07C37/82 , C07C37/86 , C07C39/04 , C07C45/85 , C07C407/00 , C07C2601/14 , Y02P20/52
摘要： Disclosed herein is a process for producing phenol. The process includes oxidizing at least a portion of a feed comprising cyclohexylbenzene to produce an oxidation composition comprising cyclohexyl-1-phenyl-1-hydroperoxide. The oxidation composition may then be cleaved in the presence of an acid catalyst to produce a cleavage reaction mixture comprising the acid catalyst, phenol and cyclohexanone. At least a portion of the cleavage reaction mixture may be neutralized with a basic material to form a treated cleavage reaction mixture. In various embodiments, the treated cleavage reaction mixture contains no greater than 50 wppm of the acid catalyst or no greater than 50 wppm of the basic material.
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公开(公告)号：US09169190B2
公开(公告)日：2015-10-27
申请号：US13856631
申请日：2013-04-04
发明人： Wayne J. Brouillette , Donald D. Muccio , Venkatram Reddy Atigadda , John M. Ruppert , Susan M. Lobo Ruppert
IPC分类号： C07C205/00 , C07C229/00 , C07C59/40 , C07C63/333 , C07C61/00 , A61K31/20 , A61K31/195 , C07C57/50 , C07C29/14 , C07C45/29 , C07C45/30 , C07C45/51 , C07C45/61 , C07C45/67 , C07C45/68 , C07C47/238 , C07C49/403 , C07C49/417 , C07C49/603 , C07C49/683 , C07C49/713 , C07C49/753 , C07C51/09 , C07C67/343 , C07C403/08 , C07C403/14 , C07C403/20 , C07D311/96 , C12C11/02 , C07C57/26
CPC分类号： A61K31/202 , A61K9/0014 , A61K45/06 , C07B2200/09 , C07C29/14 , C07C45/29 , C07C45/292 , C07C45/30 , C07C45/513 , C07C45/61 , C07C45/673 , C07C45/68 , C07C47/238 , C07C49/403 , C07C49/417 , C07C49/603 , C07C49/683 , C07C49/713 , C07C49/753 , C07C51/09 , C07C57/26 , C07C57/50 , C07C67/343 , C07C403/08 , C07C403/14 , C07C403/20 , C07C2601/02 , C07C2601/14 , C07C2601/16 , C07C2602/10 , C07C2602/28 , C07D311/96 , C12C11/02 , C07C33/16 , C07C69/618
摘要： Described herein are methods for making retinoids. Also described herein are retinoids and methods of use thereof.
摘要翻译： 本文描述了制备类视黄醇的方法。 本文还描述了类视黄醇及其使用方法。
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公开(公告)号：US09115068B2
公开(公告)日：2015-08-25
申请号：US13816618
申请日：2011-08-16
IPC分类号： C07C49/403 , C07C37/86 , C07C45/85 , C07C37/08 , C07C39/04
CPC分类号： C07C49/403 , C07C37/08 , C07C37/82 , C07C37/86 , C07C39/04 , C07C45/85 , C07C407/00 , C07C2601/14 , Y02P20/52
摘要： Disclosed herein is a process for producing phenol. The process includes oxidizing at least a portion of a feed comprising cyclohexylbenzene to produce an oxidation composition comprising cyclohexyl-1-phenyl-1-hydroperoxide. The oxidation composition may then be cleaved in the presence of an acid catalyst to produce a cleavage reaction mixture comprising the acid catalyst, phenol and cyclohexanone. At least a portion of the cleavage reaction mixture may be neutralized with a basic material to form a treated cleavage reaction mixture. In various embodiments, the treated cleavage reaction mixture contains no greater than 50 wppm of the acid catalyst or no greater than 50 wppm of the basic material.
摘要翻译： 本文公开了一种生产苯酚的方法。 该方法包括氧化至少一部分包含环己基苯的进料以产生包含环己基-1-苯基-1-氢过氧化物的氧化组合物。 然后可以在酸催化剂的存在下将氧化组合物切割，以产生包含酸催化剂，苯酚和环己酮的裂解反应混合物。 裂解反应混合物的至少一部分可以用碱性物质中和以形成经处理的裂解反应混合物。 在各种实施方案中，处理的裂解反应混合物含有不大于50wppm的酸催化剂或不大于50wppm的碱性物质。
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公开(公告)号：US09090545B2
公开(公告)日：2015-07-28
申请号：US14351240
申请日：2012-10-12
IPC分类号： C07C205/00 , C07C45/61 , C07B53/00 , C07C45/69 , C07C49/403 , C07C49/413 , C07C49/463 , C07D309/30 , C07F7/18 , C07J1/00 , C07J21/00
CPC分类号： C07C45/61 , C07B53/00 , C07C45/69 , C07C49/403 , C07C49/413 , C07C49/463 , C07C2601/08 , C07C2601/14 , C07C2601/16 , C07C2603/40 , C07D309/30 , C07F7/1892 , C07J1/0011 , C07J21/003 , C07J51/00 , C07C49/617 , C07C49/657 , C07C49/697 , C07C49/753
摘要： The present invention provides processes for the production of chiral compounds in a stereoisomeric excess. The present processes involve reacting a hydrometallated alkene compound with a compound comprising a conjugated-bond system under conditions such that the compounds undergo an asymmetric 1,4- or 1,6-conjugate addition reaction, generating a chiral compound in a stereoisomeric excess. The reaction is performed in the presence of a metal catalyst, which catalyst preferably comprises a non-racemic chiral ligand.
摘要翻译： 本发明提供了以立体异构体过量生产手性化合物的方法。 本发明的方法包括使湿法化烯烃化合物与包含共轭键系统的化合物在使得化合物经历不对称的1,4-或1,6-偶合物加成反应的条件下反应，产生立体异构过量的手性化合物。 该反应在金属催化剂的存在下进行，该催化剂优选包含非外消旋手性配体。
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