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    Methods for the isolation, recovery and purification of non-polar compounds using novel hydrophobically-modified polysaccharide gels
    8.
    发明授权
    Methods for the isolation, recovery and purification of non-polar compounds using novel hydrophobically-modified polysaccharide gels 失效
    使用新的疏水改性多糖凝胶分离，回收和纯化非极性化合物的方法

    公开(公告)号：US06989098B2

    公开(公告)日：2006-01-24

    申请号：US10340026

    申请日：2003-01-10

    申请人： F. William Collins ,  A. Bachir Sarr ,  David Fielder

    发明人： F. William Collins ,  A. Bachir Sarr ,  David Fielder

    IPC分类号： B01D15/08

    CPC分类号： B01J20/291 ,  A61K36/00 ,  A61K36/899 ,  B01D15/166 ,  B01D15/203 ,  B01D15/327 ,  B01J20/26 ,  B01J20/262 ,  B01J20/265 ,  B01J20/287 ,  B01J20/3212 ,  B01J20/3221 ,  B01J20/3274 ,  B01J2220/54 ,  A61K2300/00

    摘要： A process is described for the preparation f electrostatically-linked, aliphatic- or alicyclic-substituted anionic or cationic polysaccharide gels from readily available macroporous ionic polysaccharide chromatographic media, such as diethylaminoethyl (DEAE), quaternary aminoethyl (QAE) and sulfopropyl (SP) substituted polysaccharide gels. These novel gels are used for the isolation, recovery and purification of non-polar extractives using one or more extracting solvents from the group of lower alcohols, ketones, and water. The non-polar extractives may be alk(n)lyresorcinols, steroid, triterpenoid, cardiac glycosides and saponins, steryl ferulates and other phenolic acid conjugates, flavonoids, lipids, alcohol-soluble antimicrobials, prolamines or other alcohol-soluble proteolipid complexes.

    摘要翻译： 描述了用于从容易获得的大孔离子多糖色谱介质如二乙基氨基乙基（DEAE），季氨基乙基（QAE）和磺丙基（SP）取代的静电连接的脂族或脂环取代的阴离子或阳离子多糖凝胶的制备方法 多糖凝胶。 这些新型凝胶用于使用来自低级醇，酮和水的一种或多种提取溶剂的非极性萃取物的分离，回收和纯化。 非极性提取物可以是烷（n）溶解性间苯二酚，类固醇，三萜，强心苷和皂苷，甾体阿魏酸酯和其它酚酸共轭物，类黄酮，脂质，醇溶性抗微生物剂，醇溶醇或其它醇溶性蛋白脂质复合物。

    Coated ion exchange substrate and method of forming
    9.
    发明申请
    Coated ion exchange substrate and method of forming 有权
    涂层离子交换基板和成型方法

    公开(公告)号：US20050181224A1

    公开(公告)日：2005-08-18

    申请号：US10782366

    申请日：2004-02-18

    申请人： Christopher Pohl ,  Charanjit Saini

    发明人： Christopher Pohl ,  Charanjit Saini

    IPC分类号： B01D15/36 ,  B01J39/18 ,  B01J39/26 ,  B01J41/12 ,  B01J41/20 ,  B01J47/00 ,  B32B27/34

    CPC分类号： B01J41/20 ,  B01D15/362 ,  B01D15/363 ,  B01J20/28014 ,  B01J20/28042 ,  B01J20/3221 ,  B01J20/3293 ,  B01J39/26 ,  B01J47/016 ,  B01J2220/54 ,  Y10T428/2998 ,  Y10T428/31725

    摘要： A method for making an ion exchange coating (e.g., a chromatographic medium) on a substrate comprising (a) reacting at least a first amine compound comprising amino groups, with at least a first polyfunctional compound, in the presence of a substrate to form a first condensation polymer reaction product, with a first unreacted excess of either at least said first amino group or polyfunctional compound functional moieties, irreversibly attached to the substrate, and (b) reacting at least a second amine compound or at least a second polyfunctional compound with unreacted excess in the first condensation polymer reaction product to form a second condensation polymer reaction product, and repeating the steps to produce the desired coating. A coated ion exchange substrate so made.

    摘要翻译： 一种用于在基材上制备离子交换涂层（例如，色谱介质）的方法，包括（a）使至少含有氨基的第一种胺化合物与至少第一多官能化合物在底物存在下反应，形成 第一缩合聚合物反应产物，具有至少所述第一氨基或多官能化合物官能部分的第一未反应过量，不可逆地附着于所述底物，和（b）使至少第二种胺化合物或至少第二种多官能化合物与 在第一缩聚物反应产物中的未反应过量以形成第二缩聚物反应产物，并重复以产生所需涂层的步骤。 如此制成的涂覆的离子交换衬底。