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    Divinyl-ether compound and manufacturing method therefor
    1.
    发明授权
    Divinyl-ether compound and manufacturing method therefor 有权
    二乙烯基醚化合物及其制备方法

    公开(公告)号：US09133090B2

    公开(公告)日：2015-09-15

    申请号：US13824072

    申请日：2011-10-06

    Applicant: Youichi Fukunishi ,  Masahiro Murotani

    Inventor： Youichi Fukunishi ,  Masahiro Murotani

    IPC: C07C43/162 ,  C07C41/08

    CPC classification number: C07C43/162 ,  C07C41/08 ,  C07C2602/42

    Abstract: A novel divinyl ether compound having the formula (I): wherein A indicates a single bond or a double bond which is low in odor, low in volatility, and low in skin irritability, which have low toxicities, which are useful as a starting material for a polymer composition having excellent curability, adhesiveness and transmission in the ultraviolet light region, and further, having a special reactivity alone or with other compounds, and a process for producing the same.

    Abstract translation: 一种具有式（I）的新型二乙烯基醚化合物：其中A表示单键或双键，其具有低毒性，低毒性，低挥发性，低毒性，可用作原料 对于在紫外线区域具有优异的固化性，粘附性和透射性，并且还具有单独或与其它化合物具有特殊反应性的聚合物组合物及其制备方法。

    Addition reaction of hydroxy1-containing compounds with alkynes or allenes
    3.
    发明授权
    Addition reaction of hydroxy1-containing compounds with alkynes or allenes 失效
    含羟基的化合物与炔或丙烯的加成反应

    公开(公告)号：US6120744A

    公开(公告)日：2000-09-19

    申请号：US97818

    申请日：1998-06-16

    Applicant: Joaquim Henrique Teles ,  Norbert Rieber ,  Klaus Breuer ,  Dirk Demuth ,  Hartmut Hibst

    Inventor： Joaquim Henrique Teles ,  Norbert Rieber ,  Klaus Breuer ,  Dirk Demuth ,  Hartmut Hibst

    IPC: B01J23/06 ,  B01J37/02 ,  C07B61/00 ,  C07C41/06 ,  C07C41/08 ,  C07C41/54 ,  C07C43/15 ,  C07C43/303 ,  C01G9/00 ,  C01G11/00 ,  C22B13/00 ,  C22B17/00 ,  C22B43/00

    CPC classification number: C07C41/54 ,  B01J23/06 ,  B01J37/0203 ,  C07C41/06 ,  C07C41/08

    Abstract: A process for preparing compounds of the formulae I and II ##STR1## where R.sup.1 and R have the meanings indicated in the specification by an addition reaction of a compound of the formula IIIR.sup.1 OH IIIwith an acetylene or allene of the formula IV or V ##STR2## in the gas phase at elevated temperatures in the presence of a heterogeneous catalyst. The catalyst is obtained by impregnating silica with a zinc salt, by a process in which the reaction is carried out at below 200.degree. C. and the catalyst contains, as an active component, an X-ray amorphous zinc silicate or cadmium silicate containing from 1 to 40% by weight, calculated as oxide, of zinc or cadmium, obtainable by applying a salt of zinc or cadmium and an inorganic oxo acid, which salt is decomposable at below 400.degree. C., to amorphous silica and forming the catalyst before the reaction at from 50 to 500.degree. C. or during the reaction in situ at from 50 to 200.degree. C. in the presence of a hydroxyl-containing compound such as water, alkanols of 1 to 6 carbon atoms, diols and polyols having 2 to 6 carbon atoms and 2 or 3 OH groups and low molecular weight carboxylic acids.

    Abstract translation: 制备式I和II化合物的方法，其中R1和R具有本说明书中通过式III的化合物R1OH III与乙炔或式IV或V的烯在气相中的加成反应所示的含义 在非均相催化剂存在下在升高的温度下进行。 通过在低于200℃下进行反应的方法，用锌盐浸渍二氧化硅得到催化剂，催化剂含有作为活性成分的X射线无定形硅酸锌或含有 以氧化物计的锌或镉1〜40重量％，可通过将该盐在低于400℃下分解的锌或镉和无机含氧酸盐与无定形二氧化硅反应而形成催化剂 在50至500℃的反应或在50-200℃下在含羟基的化合物如水，1至6个碳原子的链烷醇存在下的反应期间的反应，二醇和多元醇具有2 至6个碳原子和2或3个OH基团和低分子量羧酸。

    Preparation of nonionic surfactants
    6.
    发明授权
    Preparation of nonionic surfactants 失效
    制备非离子表面活性剂

    公开(公告)号：US4721817A

    公开(公告)日：1988-01-26

    申请号：US948378

    申请日：1986-12-31

    Applicant: Charles L. Edwards

    Inventor： Charles L. Edwards

    IPC: B01J31/02 ,  B01J31/00 ,  C07B61/00 ,  C07C41/00 ,  C07C41/03 ,  C07C41/08 ,  C07C43/11 ,  C07C67/00

    CPC classification number: C07C41/03

    Abstract: Alkylene oxide adducts of higher alkanols are prepared by a process which comprises contacting and reacting an alkylene oxide reactant comprising one or more C.sub.2 to C.sub.4 vicinal alkylene oxides with an alkanol reactant comprising one or more C.sub.6 to C.sub.30 alkanols in the presence of a catalytically effective amount of a catalyst which combines (i) one or more phosphorus-containing acids with (ii) one or more aluminum compounds selected from the group consisting of aluminum alcoholates and aluminum phenolates, the relative molar ratio of component (i) to component (ii) being in the range from about 0.1:1 to 2.5:1. Alkanol alkoxylates, and particularly alkanol ethoxylates, prepared in this manner are characterized by a relatively narrow-range distribution of alkylene oxide adducts and by a relatively low content of residual alkanol. The products of this process are nonionic surfactants, particularly useful as components of detergent formulations.

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