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    Method and Apparatus for Fabricating Fibers and Microstructures from Disparate Molar Mass Precursors
    7.
    发明申请
    Method and Apparatus for Fabricating Fibers and Microstructures from Disparate Molar Mass Precursors 审中-公开
    用于从不同摩尔质量前体制造纤维和微结构的方法和装置

    公开(公告)号：US20160369400A1

    公开(公告)日：2016-12-22

    申请号：US14827752

    申请日：2015-08-17

    申请人： Dynetics, Inc.

    发明人： James L. Maxwell ,  Nicholas Webb ,  James Allen

    IPC分类号： C23C16/48 ,  C23C16/20 ,  C23C16/08 ,  D01F8/18 ,  C23C16/50 ,  C23C16/52

    CPC分类号： C23C16/483 ,  C04B35/58 ,  C04B35/58007 ,  C04B35/58028 ,  C04B35/62272 ,  C04B35/62277 ,  C04B35/62286 ,  C04B2235/5296 ,  C23C16/08 ,  C23C16/20 ,  C23C16/4418 ,  C23C16/486 ,  C23C16/50 ,  C23C16/52 ,  D01F8/18 ,  D01F9/127 ,  D04H1/4242

    摘要： The disclosed methods and apparatus improve the fabrication of solid fibers and microstructures. In many embodiments, the fabrication is from gaseous, solid, semi-solid, liquid, critical, and supercritical mixtures using one or more low molar mass precursor(s), in combination with one or more high molar mass precursor(s). The methods and systems generally employ the thermal diffusion/Soret effect to concentrate the low molar mass precursor at a reaction zone, where the presence of the high molar mass precursor contributes to this concentration, and may also contribute to the reaction and insulate the reaction zone, thereby achieving higher fiber growth rates and/or reduced energy/heat expenditures together with reduced homogeneous nucleation. In some embodiments, the invention also relates to the permanent or semi-permanent recording and/or reading of information on or within fabricated fibers and microstructures. In some embodiments, the invention also relates to the fabrication of certain functionally-shaped fibers and microstructures. In some embodiments, the invention may also utilize laser beam profiling to enhance fiber and microstructure fabrication.

    摘要翻译： 所公开的方法和装置改善了固体纤维和微结构的制造。 在许多实施方案中，制造是使用一种或多种低摩尔质量前体与一种或多种高摩尔质量前体组合从气态，固体，半固体，液体，临界和超临界混合物。 所述方法和系统通常采用热扩散/反应效应将低摩尔质量前体浓缩在反应区，其中高摩尔质量前体的存在有助于该浓度，并且还可以有助于反应并使反应区绝缘 ，从而实现更高的纤维生长速率和/或降低的能量/热量支出以及减少的均匀成核。 在一些实施例中，本发明还涉及在制造的纤维和微结构之上或之内的信息的永久或半永久性记录和/或读取。 在一些实施例中，本发明还涉及某些功能形状的纤维和微结构的制造。 在一些实施例中，本发明还可以利用激光束轮廓来增强光纤和微结构的制造。

    METHOD OF MANUFACTURING CARBON NANOTUBES AND FIBERS USING CATALYTIC METAL OXIDE NANOPARTICLES
    10.
    发明申请
    METHOD OF MANUFACTURING CARBON NANOTUBES AND FIBERS USING CATALYTIC METAL OXIDE NANOPARTICLES 有权
    使用催化金属氧化物纳米粒子制造碳纳米管和纤维的方法

    公开(公告)号：US20160280546A1

    公开(公告)日：2016-09-29

    申请号：US15177085

    申请日：2016-06-08

    申请人： BAKER HUGHES INCORPORATED

    发明人： CORINA L. SANDU

    IPC分类号： C01B31/02

    CPC分类号： C01B32/158 ,  B82Y40/00 ,  C01B32/16 ,  C01B32/162 ,  C01B32/166 ,  C01B32/18 ,  D01F9/127 ,  Y10S977/842

    摘要： A method for producing carbon nanotubes and/or fibers, such as carbon nanotubes, involves sparging a gas (such as carbon dioxide) through a liquid hydrocarbon (such as crude oil) in the presence of an effective amount of metal oxide particles (such as MgO, Al2O3, CeO2, and/or SiO2 nanoparticles having a size in the range from about 2 nm to about 10 microns, and which may have a bimodal particle size distribution) at a temperature in a range of between about 70 to about 350° C. to produce carbon nanotubes and fibers having a size range of from about 50 nm to about 20 microns.

    摘要翻译： 碳纳米管等碳纳米管和/或纤维的制造方法包括在有效量的金属氧化物粒子（例如，原料油）的存在下，通过液态烃（如原油）喷射气体（如二氧化碳） MgO，Al 2 O 3，CeO 2和/或SiO 2纳米颗粒，其尺寸在约2nm至约10微米的范围内，并且其可具有双峰粒径分布）在约70至约350° 以产生尺寸范围为约50nm至约20微米的碳纳米管和纤维。