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公开(公告)号：US20240058783A1
公开(公告)日：2024-02-22
申请号：US18260979
申请日：2022-01-11
CPC分类号： B01J19/123 , B01J19/0006 , B01J19/0066 , B01J19/1881 , C08F2/48 , B01J2219/00087
摘要： Apparatuses for polymerizing or devolatilizing a composition, especially one of high melt viscosity, are disclosed. Methods of polymerizing and devolatilizing a composition, especially one of high melt viscosity, are also disclosed.
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公开(公告)号：US20180362424A1
公开(公告)日：2018-12-20
申请号：US16060221
申请日：2016-12-07
申请人： SHELL OIL COMPANY
发明人： Leslie Andrew CHEWTER , Jean Paul Andre Marie Joseph Ghislain LANGE , Duraisamy MUTHUSAMY , Timothy Michael NISBET , Evert VAN DER HEIDE , Pieter HUIZENGA
CPC分类号： C07C29/132 , B01J8/20 , B01J8/22 , B01J10/007 , B01J16/005 , B01J19/1881 , B01J19/2465 , B01J2208/00283 , B01J2219/0011 , C07C29/60 , C07C31/202 , C07C31/205 , C07C2521/06 , C07C2523/22 , C07C2523/26 , C07C2523/28 , C07C2523/30 , Y02P20/582
摘要： The invention provides a continuous process for the preparation of ethylene glycol and 1, 2-propylene glycol from starting material comprising one or more saccharides, said process being carried out in a reactor system comprising a reactor vessel equipped with an external recycle loop and said process comprising the steps of: i) providing the starting material in a solvent, via an inlet, to the external recycle loop and contacting it therein with a retro-aldol catalyst composition to provide an intermediate stream; ii) then contacting said intermediate stream with hydrogen in the presence of a hydrogenation catalyst composition in the reactor vessel; iii) withdrawing a product stream comprising glycols from the reactor vessel; iv) providing a portion of said product stream, via an outlet, for separation and purification of the glycols contained therein; and v) recycling the remainder of said product stream via the external recycle loop.
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3.发明申请公开(公告)号：US20180011024A1
公开(公告)日：2018-01-11
申请号：US15544176
申请日：2016-01-19
申请人： ADVANCED POLYMER MONITORING TECHNOLOGIES, INC. , THE ADMINISTRATORS OF THE TULANE EDUCATIONAL FUND
CPC分类号： E21B41/00 , B01J8/001 , B01J8/006 , B01J8/222 , B01J8/228 , B01J19/0006 , B01J19/18 , B01J19/1881 , B01J2208/00061 , B01J2208/00212 , B01J2208/00362 , B01J2208/00539 , B01J2208/00548 , B01J2208/00575 , B01J2208/00628 , B01J2208/00637 , B01J2208/00725 , B01J2208/00973 , B01J2219/0004 , B01J2219/00063 , B01J2219/00069 , B01J2219/00072 , B01J2219/00094 , B01J2219/00123 , B01J2219/00164 , B01J2219/00168 , B01J2219/00186 , B01J2219/002 , B01J2219/00216 , B01J2219/00218 , B01J2219/00225 , B01J2219/00231 , B01J2219/00236 , B01J2219/00238 , B01J2219/0024 , B01J2219/00243 , B01J2219/00272 , G01N11/08 , G01N21/19 , G01N21/21 , G01N21/23 , G01N21/272 , G01N21/33 , G01N21/35 , G01N21/47 , G01N21/64 , G01N21/65 , G01N21/75 , G01N21/84 , G01N2021/8416 , G01N2201/12
摘要： Devices and methods for controlling the properties of chemical species during time-dependent processes. A device includes a reactor for containing one or more chemical species of a time-dependent process, an extraction pump for automatically and continuously extracting an amount of the one or more chemical species from the reactor, one or more detectors for measuring property changes of the one or more extracted chemical species and generating a continuous stream of data related to the one or more property changes to the one or more chemical species during a time interval, and a process controller configured to fit the continuous stream of data to a mathematical function to predict one or more properties of the one or more chemical species at a future time point and make one or more process decisions based on the prediction of one or more properties at the future time point.
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公开(公告)号：US20170081257A1
公开(公告)日：2017-03-23
申请号：US14858526
申请日：2015-09-18
发明人： Bruce E. KREISCHER
CPC分类号： C07C2/32 , B01J4/004 , B01J4/02 , B01J8/22 , B01J8/222 , B01J19/1806 , B01J19/1818 , B01J19/1825 , B01J19/1856 , B01J19/1862 , B01J19/1881 , B01J2208/00044 , B01J2208/00141 , B01J2208/00176 , B01J2208/00212 , B01J2208/00265 , B01J2208/00274 , B01J2208/00283 , B01J2208/00911 , B01J2219/00056 , B01J2219/00083 , B01J2219/00094 , B01J2219/00108 , B01J2219/0011 , B01J2219/00195 , B01J2219/00211 , B01J2219/00229 , B01J2219/00238 , C07C2/30 , C07C2/88 , C07C2523/26 , C07C2523/755 , C07C2527/135 , C07C2531/12 , C07C2531/14 , C07C2531/24 , C07C11/02 , C07C11/107
摘要： A process includes periodically or continuously introducing an olefin monomer and periodically or continuously introducing a catalyst system or catalyst system components into a reaction mixture within a reaction system, oligomerizing the olefin monomer within the reaction mixture to form an oligomer product, and periodically or continuously discharging a reaction system effluent comprising the oligomer product from the reaction system. The reaction system includes a total reaction mixture volume and a heat exchanged portion of the reaction system comprising a heat exchanged reaction mixture volume and a total heat exchanged surface area providing indirect contact between the reaction mixture and a heat exchange medium. A ratio of the total heat exchanged surface area to the total reaction mixture volume within the reaction system is in a range from 0.75 in−1 to 5 in−1, and an oligomer product discharge rate from the reaction system is between 1.0 (lb)(hr−1)(gal−1) to 6.0 (lb)(hr−1)(gal−1).
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5.发明授权Dispersed bubble reactor for enhanced gas-liquid-solids contact and mass transfer 有权分散气泡反应器，用于增强气 - 液 - 固体接触和传质公开(公告)号：US09242220B2
公开(公告)日：2016-01-26
申请号：US13402908
申请日：2012-02-23
申请人： Pannalal Vimalchand , Guohai Liu , WanWang Peng , Alexander Bonsu
发明人： Pannalal Vimalchand , Guohai Liu , WanWang Peng , Alexander Bonsu
CPC分类号： B01J8/228 , B01D53/1475 , B01D53/18 , B01D53/62 , B01D2251/206 , B01J8/1827 , B01J8/1836 , B01J8/1872 , B01J19/1881 , B01J2208/00141 , B01J2208/00548 , B01J2219/00083 , B01J2219/00164 , B01J2219/00182 , B01J2219/00247 , Y02A50/2342 , Y02C10/04 , Y02C10/06 , Y02P20/152
摘要： An apparatus to promote gas-liquid contact and facilitate enhanced mass transfer. The dispersed bubble reactor (DBR) operates in the dispersed bubble flow regime to selectively absorb gas phase constituents into the liquid phase. The dispersion is achieved by shearing the large inlet gas bubbles into fine bubbles with circulating liquid and additional pumped liquid solvent when necessary. The DBR is capable of handling precipitates that may form during absorption or fine catalysts that may be necessary to promote liquid phase reactions. The DBR can be configured with multistage counter current flow sections by inserting concentric cylindrical sections into the riser to facilitate annular flow. While the DBR can absorb CO2 in liquid solvents that may lead to precipitates at high loadings, it is equally capable of handling many different types of chemical processes involving solids (precipitates/catalysts) along with gas and liquid phases.
摘要翻译： 促进气液接触并促进增强传质的装置。 分散的气泡反应器（DBR）以分散的气泡流动方式操作，以选择性地吸收气相成分进入液相。 通过在需要时将大的入口气泡剪切成具有循环液体的细小气泡和附加的泵送液体溶剂来实现分散。 DBR能够处理可能在吸收过程中形成的沉淀物或可能促进液相反应所需的细小催化剂。 DBR可以通过将同心圆柱形部分插入提升管中以便于环形流动而配置多级逆流部分。 虽然DBR可以在可能导致高负载下沉淀的液体溶剂中吸收二氧化碳，但同样能够处理涉及固体（沉淀物/催化剂）以及气相和液相的许多不同类型的化学过程。
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公开(公告)号：US20160010851A1
公开(公告)日：2016-01-14
申请号：US14854815
申请日：2015-09-15
发明人： Robert Edward NEATE , Clive Alexander Hamilton , Robert E. Stilson , George Malcolm Williamson , Jonathan D. Runnacles
CPC分类号： F22B1/16 , B01J8/0015 , B01J8/0065 , B01J8/20 , B01J19/1881 , B01J2208/00176 , B01J2219/00103 , C07C67/08 , C07C69/82
摘要： The invention relates to recycling steam at elevated temperature and/or pressure generated within a thermosiphon esterifier design comprising a riser baffle in the vapor separator. Advantageously, the thermosiphon esterifier design can provide steam that can be employed in various additional processes and can thus provide an overall energy savings in operating the thermosiphon esterifier. Methods of using the steam are also described.
摘要翻译： 本发明涉及在高温和/或压力下回收蒸汽，所述高温和/或压力在热虹吸酯设计中产生，包括在所述蒸汽分离器中的提升管挡板。 有利地，热虹吸酯化器设计可以提供可以用于各种附加过程的蒸汽，因此可以在操作热虹吸酯化器时提供总体能量节省。 还描述了使用蒸汽的方法。
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公开(公告)号：US20150197584A1
公开(公告)日：2015-07-16
申请号：US14565577
申请日：2014-12-10
申请人： TPC Group LLC
IPC分类号： C08F10/10
CPC分类号： C08F10/10 , B01J8/00 , B01J19/1837 , B01J19/1881 , B01J2219/00065 , B01J2219/00081 , B01J2219/00094 , B01J2219/00162 , B01J2219/0022 , B01J2219/00231 , C08F2/01 , C08F110/10 , C08F2500/03 , C08F2500/17 , C08F2/00
摘要： A method of making a polyisobutylene polymer in a recirculating loop reactor with one or more reaction tubes in contact with a heat transfer medium includes controlling the delta P and polymerization reaction to provide a linear velocity of the reaction mixture of at least 11 ft/sec in the one or more tubes of the loop reactor and/or controlling the delta P and polymerization reaction of steps (b) and (c) to provide a recirculation ratio of the recirculation rate to the feed rate of at least 30:1. Typically, the process utilizes a recirculating pump operating at a at a pressure differential of from 35 psi to 70 psi.
摘要翻译： 在具有与传热介质接触的一个或多个反应管的再循环回路反应器中制备聚异丁烯聚合物的方法包括控制δP和聚合反应以提供至少11ft / sec的反应混合物的线速度 环流反应器的一个或多个管和/或控制步骤（b）和（c）的δP和聚合反应，以提供再循环速率与至少30:1的进料速率的再循环比。 通常，该方法利用在35psi至70psi的压力差下工作的循环泵。
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公开(公告)号：US20140162064A1
公开(公告)日：2014-06-12
申请号：US13940961
申请日：2013-07-12
申请人： Cabot Corporation
CPC分类号： C09C1/56 , B01J19/1881 , B01J19/26 , B01J2219/00177 , C01P2004/51 , C01P2004/62 , C01P2006/12 , C01P2006/19 , C01P2006/22 , C01P2006/40 , C08K3/04 , C08K5/175 , C08K5/5317 , C08K9/04 , C09C1/48 , C09C1/50 , C09C1/565 , C09D11/324 , Y10T428/2982
摘要： Disclosed herein are high structured carbon blacks, methods of synthesis and treatment, and dispersions and inkjet ink formulations prepared therefrom. The carbon black can have the following properties: OAN≧170 mL/100 g; and STSA ranging from 160 to 220 m2/g. The carbon black can also have the following properties: OAN≧170 mL/100 g; and a ratio of STSA/BET surface area ranging from 0.7 to 1.
摘要翻译： 本文公开了高度结构化的炭黑，合成和处理方法，以及由其制备的分散体和喷墨油墨配方。 炭黑可以具有以下性能：OAN≥170mL/ 100g; 和STSA范围从160到220 m2 / g。 炭黑还可以具有以下性质：OAN≥170mL/ 100g; 和STSA / BET表面积的比例为0.7〜1。
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9.发明授权Polyester production system employing horizontally elongated esterification vessel 有权采用水平伸长酯化容器的涤纶生产系统公开(公告)号：US08470250B2
公开(公告)日：2013-06-25
申请号：US13079380
申请日：2011-04-04
申请人： Bruce Roger DeBruin
发明人： Bruce Roger DeBruin
IPC分类号： B01J19/00
CPC分类号： B01J19/2465 , B01D3/14 , B01D19/0036 , B01J4/002 , B01J19/006 , B01J19/18 , B01J19/1812 , B01J19/1881 , B01J19/24 , B01J19/2415 , B01J19/245 , B01J19/26 , B01J2219/00006 , B01J2219/00081 , B01J2219/00085 , B01J2219/00092 , B01J2219/00094 , B01J2219/00103 , B01J2219/00166 , B01J2219/00184 , B01J2219/00186 , B01J2219/0077 , B01J2219/182 , B01J2219/1943 , C08G63/785
摘要： A polyester production process employing an esterification system that utilizes a horizontally elongated esterification vessel as an esterification reactor and/or a vapor-liquid disengagement vessel.
摘要翻译： 使用利用水平伸长的酯化容器作为酯化反应器和/或气液分离容器的酯化体系的聚酯制备方法。
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公开(公告)号：US08178054B2
公开(公告)日：2012-05-15
申请号：US12702725
申请日：2010-02-09
CPC分类号： B01J19/1881 , B01J4/002 , B01J10/002 , B01J19/1806 , B01J19/1862 , B01J19/1875 , B01J19/2405 , B01J19/245 , B01J19/246 , B01J19/2465 , B01J19/26 , B01J2219/00006 , B01J2219/0004 , B01J2219/00105 , B01J2219/00182 , B01J2219/00186 , C07C51/265 , C07C63/26
摘要： Disclosed is an optimized process and apparatus for more efficiently and economically carrying out the liquid-phase oxidation of an oxidizable compound. Such liquid-phase oxidation is carried out in a bubble column reactor that provides for a highly efficient reaction at relatively low temperatures. When the oxidized compound is para-xylene and the product from the oxidation reaction is crude terephthalic acid (CTA), such CTA product can be purified and separated by more economical techniques than could be employed if the CTA were formed by a conventional high-temperature oxidation process.
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