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1.发明申请公开(公告)号：US20170210865A1
公开(公告)日：2017-07-27
申请号：US15478817
申请日：2017-04-04
CPC分类号： C08J5/18 , A61L27/16 , A61L27/26 , A61L27/34 , A61L27/507 , A61L27/56 , A61L29/041 , A61L29/049 , A61L29/085 , A61L31/041 , A61L31/048 , A61L31/10 , A61L31/146 , B29B9/12 , B29C43/003 , B29C43/12 , B29C44/5627 , B29C47/0004 , B29C47/0026 , B29C47/004 , B29C47/0057 , B29C55/005 , B29C55/16 , B29K2027/00 , B29K2027/12 , B29K2027/18 , B29K2105/04 , B29L2007/008 , B32B27/06 , B32B27/322 , B32B2250/00 , B32B2250/24 , B32B2307/72 , B32B2327/18 , B32B2437/00 , B32B2439/00 , B32B2535/00 , B32B2581/00 , C08F214/26 , C08F259/08 , C08J9/00 , C08J2207/02 , C08J2327/18 , Y10T428/1376 , Y10T428/28 , Y10T428/31544 , C08F2/24 , C08L27/18 , C08F214/22 , C08F214/24
摘要： A tetrafluoroethylene (TFE) copolymer film having a first endotherm between about 50° C. and about 300° C., a second endotherm between about 320° C. and about 350° C., and a third endotherm between about 350° C. and about 400° C. is provided. In exemplary embodiments, the third endotherm is approximately 380° C. In some embodiments, the second endotherm is between about 320° C. and about 330° C. or between about 330° C. and about 350° C. TFE copolymer films have a methane permeability less than about 20 μg*micron/cm2/min. In addition, the dense articles have a void volume of less than about 20%. Methods for dense articles from core shell tetrafluoroethylene copolymers are also provided. The dense articles exhibit improved physical and mechanical properties such as adhesion and barrier properties.
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2.发明授权公开(公告)号：US09988506B2
公开(公告)日：2018-06-05
申请号：US15478817
申请日：2017-04-04
IPC分类号： C08J5/18 , B29C43/00 , B29B9/12 , B29C55/16 , B29C55/00 , B29C43/12 , B29C47/00 , C08F259/08 , B29K27/12 , B29L7/00
CPC分类号： C08J5/18 , A61L27/16 , A61L27/26 , A61L27/34 , A61L27/507 , A61L27/56 , A61L29/041 , A61L29/049 , A61L29/085 , A61L31/041 , A61L31/048 , A61L31/10 , A61L31/146 , B29B9/12 , B29C43/003 , B29C43/12 , B29C44/5627 , B29C47/0004 , B29C47/0026 , B29C47/004 , B29C47/0057 , B29C55/005 , B29C55/16 , B29K2027/00 , B29K2027/12 , B29K2027/18 , B29K2105/04 , B29L2007/008 , B32B27/06 , B32B27/322 , B32B2250/00 , B32B2250/24 , B32B2307/72 , B32B2327/18 , B32B2437/00 , B32B2439/00 , B32B2535/00 , B32B2581/00 , C08F214/26 , C08F259/08 , C08J9/00 , C08J2207/02 , C08J2327/18 , Y10T428/1376 , Y10T428/28 , Y10T428/31544 , C08F2/24 , C08L27/18 , C08F214/22 , C08F214/24
摘要： A tetrafluoroethylene (TFE) copolymer film having a first endotherm between about 50° C. and about 300° C., a second endotherm between about 320° C. and about 350° C., and a third endotherm between about 350° C. and about 400° C. is provided. In exemplary embodiments, the third endotherm is approximately 380° C. In some embodiments, the second endotherm is between about 320° C. and about 330° C. or between about 330° C. and about 350° C. TFE copolymer films have a methane permeability less than about 20 μg*micron/cm2/min. In addition, the dense articles have a void volume of less than about 20%. Methods for dense articles from core shell tetrafluoroethylene copolymers are also provided. The dense articles exhibit improved physical and mechanical properties such as adhesion and barrier properties.
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3.发明授权公开(公告)号：US09644054B2
公开(公告)日：2017-05-09
申请号：US14577597
申请日：2014-12-19
IPC分类号： C08F214/26 , C08F259/08 , B29C55/00 , B32B15/085 , B32B27/08 , B32B27/32 , C08J9/00 , C09D127/18 , C08J5/18 , B29C55/02 , B29K27/18 , B29L9/00
CPC分类号： C08F214/26 , B29C55/005 , B29C55/023 , B29K2027/18 , B29K2995/0063 , B29L2009/00 , B32B15/085 , B32B27/08 , B32B27/322 , B32B2307/30 , C08F214/262 , C08F259/08 , C08J5/18 , C08J9/00 , C08J2327/18 , C08L51/003 , C08L2207/53 , C09D127/18 , C08F214/22 , C08F214/24 , C08L91/00
摘要： A dense article that includes a dense TFE copolymer film is provided. The dense TFE copolymer film includes a first endotherm between about 50° C. and about 300° C., a second endotherm between about 320° C. and about 350° C., and a third endotherm between about 350° C. and about 400° C. To form the dense article, a core shell TFE copolymer is formed into a pellet, ram extruded into a tape, dried into a dried preform, and then stretched into a dense TFE copolymer film that exhibits improved physical and mechanical properties. The dense TFE copolymer film is produced directly from the dried preform at a deformation temperature less than about 335° C. and without increasing the porosity of the dried preform, as would conventionally be done in expansion processes. The dense TFE copolymer films have a methane permeability less than about 20 μg*micron/cm2/min. The dense articles have a void volume less than about 20%.
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4.发明授权公开(公告)号：US09650479B2
公开(公告)日：2017-05-16
申请号：US14577566
申请日：2014-12-19
IPC分类号： C08F259/08 , C08F214/26 , B32B27/06 , B32B27/32 , C08J5/18 , A61L27/16 , A61L27/50 , A61L27/56 , A61L31/04 , A61L31/14 , B29C55/00 , C08J9/00 , B29C44/56 , A61L27/26 , A61L27/34 , A61L29/04 , A61L29/08 , A61L31/10 , B29K27/12 , B29K27/00 , B29K27/18 , B29K105/04
CPC分类号： C08J5/18 , A61L27/16 , A61L27/26 , A61L27/34 , A61L27/507 , A61L27/56 , A61L29/041 , A61L29/049 , A61L29/085 , A61L31/041 , A61L31/048 , A61L31/10 , A61L31/146 , B29B9/12 , B29C43/003 , B29C43/12 , B29C44/5627 , B29C47/0004 , B29C47/0026 , B29C47/004 , B29C47/0057 , B29C55/005 , B29C55/16 , B29K2027/00 , B29K2027/12 , B29K2027/18 , B29K2105/04 , B29L2007/008 , B32B27/06 , B32B27/322 , B32B2250/00 , B32B2250/24 , B32B2307/72 , B32B2327/18 , B32B2437/00 , B32B2439/00 , B32B2535/00 , B32B2581/00 , C08F214/26 , C08F259/08 , C08J9/00 , C08J2207/02 , C08J2327/18 , Y10T428/1376 , Y10T428/28 , Y10T428/31544 , C08F2/24 , C08L27/18 , C08F214/22 , C08F214/24
摘要： A tetrafluoroethylene (TFE) copolymer film having a first endotherm between about 50° C. and about 300° C., a second endotherm between about 320° C. and about 350° C., and a third endotherm between about 350° C. and about 400° C. is provided. In exemplary embodiments, the third endotherm is approximately 380° C. In some embodiments, the second endotherm is between about 320° C. and about 330° C. or between about 330° C. and about 350° C. TFE copolymer films have a methane permeability less than about 20 μg*micron/cm2/min. In addition, the dense articles have a void volume of less than about 20%. Methods for dense articles from core shell tetrafluoroethylene copolymers are also provided. The dense articles exhibit improved physical and mechanical properties such as adhesion and barrier properties.
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5.发明申请Dense Articles Formed From Tetrafluoroethylene Core Shell Copolymers and Methods of Making The Same 有权由四氟乙烯芯壳共聚物形成的稠密物品及其制造方法公开(公告)号：US20160177001A1
公开(公告)日：2016-06-23
申请号：US14577597
申请日：2014-12-19
IPC分类号： C08F214/26 , C08J9/00 , B29C55/02 , B32B27/08 , B32B15/085 , B29C55/00 , C09D127/18 , B32B27/32
CPC分类号： C08F214/26 , B29C55/005 , B29C55/023 , B29K2027/18 , B29K2995/0063 , B29L2009/00 , B32B15/085 , B32B27/08 , B32B27/322 , B32B2307/30 , C08F214/262 , C08F259/08 , C08J5/18 , C08J9/00 , C08J2327/18 , C08L51/003 , C08L2207/53 , C09D127/18 , C08F214/22 , C08F214/24 , C08L91/00
摘要： A dense article that includes a dense TFE copolymer film is provided. The dense TFE copolymer film includes a first endotherm between about 50° C. and about 300° C., a second endotherm between about 320° C. and about 350° C., and a third endotherm between about 350° C. and about 400° C. To form the dense article, a core shell TFE copolymer is formed into a pellet, ram extruded into a tape, dried into a dried preform, and then stretched into a dense TFE copolymer film that exhibits improved physical and mechanical properties. The dense TFE copolymer film is produced directly from the dried preform at a deformation temperature less than about 335° C. and without increasing the porosity of the dried preform, as would conventionally be done in expansion processes. The dense TFE copolymer films have a methane permeability less than about 20 μg*micron/cm2/min. The dense articles have a void volume less than about 20%.
摘要翻译： 提供包含致密的TFE共聚物膜的致密制品。 致密的TFE共聚物膜包括在约50℃和约300℃之间的第一吸热，约320℃至约350℃之间的第二吸热，以及约350℃至约350℃之间的第三吸热 为了形成致密制品，将芯壳TFE共聚物形成为颗粒，挤压成胶带的柱塞，干燥成干燥的预制件，然后拉伸成具有改善的物理和机械性能的致密的TFE共聚物膜。 密实的TFE共聚物膜直接从干燥的预制件中以低于约335℃的变形温度生产，并且不增加干燥的预成型件的孔隙率，如在扩展过程中通常所做的那样。 致密的TFE共聚物膜的甲烷渗透率小于约20μg*微米/ cm 2 / min。 致密制品的空隙体积小于约20％。
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公开(公告)号：US20240360286A1
公开(公告)日：2024-10-31
申请号：US18687513
申请日：2021-08-30
IPC分类号： C08J5/18
CPC分类号： C08J5/18 , C08J2327/24
摘要： Dense polytetrafluoroethylene films as well as methods for preparing the present materials are provided having superior optical properties (highly transmissive, low haze, low yellowness) in combination with desirable mechanical properties (such as flexibility, strength, and durability). The highly transmissive dense films are suitable for use in a variety of optical applications, such as a cover layer for a screen in a portable electronic device.
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公开(公告)号：US20240218136A1
公开(公告)日：2024-07-04
申请号：US18605514
申请日：2024-03-14
发明人： Michael E. Kennedy , Shaofeng Ran
CPC分类号： C08J5/18 , B32B3/28 , B32B27/08 , B32B27/322 , B32B37/182 , B32B38/0012 , C08L27/18 , B32B2307/518 , B32B2307/7246 , C08J2327/18
摘要： A structured fluoropolymer film including a plurality of structures having a height at least two times a thickness of a corresponding unstructured fluoropolymer film and at least a 20% increase in displacement induction period when compared to the corresponding unstructured fluoropolymer film when measured in a biaxial tensile curve at a temperature of about 125° C. In addition, the structured fluoropolymer film has a methane permeability of less than 500 μg*μm/cm2/min. The structured fluoropolymer film exhibits a higher resistance to strain and retain barrier properties during manufacture and/or use.
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8.发明申请Dense Articles Formed Tetrafluoroethylene Core Shell Copolymers and Methods of Making The Same 有权形成四氟乙烯核壳共聚物的密集制品及其制备方法公开(公告)号：US20150111031A1
公开(公告)日：2015-04-23
申请号：US14577566
申请日：2014-12-19
CPC分类号： C08J5/18 , A61L27/16 , A61L27/26 , A61L27/34 , A61L27/507 , A61L27/56 , A61L29/041 , A61L29/049 , A61L29/085 , A61L31/041 , A61L31/048 , A61L31/10 , A61L31/146 , B29B9/12 , B29C43/003 , B29C43/12 , B29C44/5627 , B29C47/0004 , B29C47/0026 , B29C47/004 , B29C47/0057 , B29C55/005 , B29C55/16 , B29K2027/00 , B29K2027/12 , B29K2027/18 , B29K2105/04 , B29L2007/008 , B32B27/06 , B32B27/322 , B32B2250/00 , B32B2250/24 , B32B2307/72 , B32B2327/18 , B32B2437/00 , B32B2439/00 , B32B2535/00 , B32B2581/00 , C08F214/26 , C08F259/08 , C08J9/00 , C08J2207/02 , C08J2327/18 , Y10T428/1376 , Y10T428/28 , Y10T428/31544 , C08F2/24 , C08L27/18 , C08F214/22 , C08F214/24
摘要： A tetrafluoroethylene (TFE) copolymer film having a first endotherm between about 50° C. and about 300° C., a second endotherm between about 320° C. and about 350° C., and a third endotherm between about 350° C. and about 400° C. is provided. In exemplary embodiments, the third endotherm is approximately 380° C. In some embodiments, the second endotherm is between about 320° C. and about 330° C. or between about 330° C. and about 350° C. TFE copolymer films have a methane permeability less than about 20 μg*micron/cm2/min. In addition, the dense articles have a void volume of less than about 20%. Methods for dense articles from core shell tetrafluoroethylene copolymers are also provided. The dense articles exhibit improved physical and mechanical properties such as adhesion and barrier properties.
摘要翻译： 一种四氟乙烯（TFE）共聚物膜，其具有约50℃至约300℃之间的第一吸热，约320℃至约350℃之间的第二吸热和约350℃之间的第三吸热。 并提供约400℃。 在示例性实施方案中，第三吸热约为380℃。在一些实施方案中，第二吸热温度为约320℃至约330℃，或约330℃至约350℃.TFE共聚物膜具有 甲烷渗透率小于约20μg*微米/ cm 2 / min。 此外，致密制品具有小于约20％的空隙体积。 还提供了来自核心壳四氟乙烯共聚物的致密制品的方法。 致密制品表现出改善的物理和机械性能，例如粘附性和阻隔性。
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公开(公告)号：US12031001B2
公开(公告)日：2024-07-09
申请号：US17277776
申请日：2018-10-05
发明人： Michael E. Kennedy , Shaofeng Ran
CPC分类号： C08J5/18 , B32B3/28 , B32B27/08 , B32B27/322 , B32B37/182 , B32B38/0012 , C08L27/18 , B32B2307/518 , B32B2307/7246 , C08J2327/18
摘要： A structured fluoropolymer film including a plurality of structures having a height at least two times a thickness of a corresponding unstructured fluoropolymer film and at least a 20% increase in displacement induction period when compared to the corresponding unstructured fluoropolymer film when measured in a biaxial tensile curve at a temperature of about 125° C. In addition, the structured fluoropolymer film has a methane permeability of less than 500 μg*μm/cm2/min. The structured fluoropolymer film exhibits a higher resistance to strain and retain barrier properties during manufacture and/or use.
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