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    Substituted tricyclodecane derivatives, processes for producing same and organoleptic uses thereof
    11.
    发明授权
    Substituted tricyclodecane derivatives, processes for producing same and organoleptic uses thereof 失效
    取代的三环癸烷衍生物，其制备方法和感官用途

    公开(公告)号：US4318863A

    公开(公告)日：1982-03-09

    申请号：US220632

    申请日：1980-12-29

    Applicant: Mark A. Sprecker ,  John B. Hall

    Inventor： Mark A. Sprecker ,  John B. Hall

    IPC: A24B15/34 ,  C07C29/09 ,  C07C29/17 ,  C07C29/70 ,  C07C35/37 ,  C07C35/46 ,  C07C45/29 ,  C07C49/643 ,  C11B9/00 ,  C07C69/96

    CPC classification number: C11B9/0042 ,  A24B15/345 ,  C07C29/095 ,  C07C29/17 ,  C07C29/70 ,  C07C35/37 ,  C07C35/46 ,  C07C45/29 ,  C07C49/643 ,  C07C2103/66

    Abstract: Described are substituted tricyclodecane derivatives having the generic structure: ##STR1## wherein Y is a moiety having a structure selected from the group consisting of: ##STR2## wherein one of the dashed lines represents a carbon-carbon single bond and the other of the dashed lines represents a carbon-carbon double bond; wherein R.sub.1 and R.sub.2 represent hydrogen or methyl with the proviso that one of R.sub.1 and R.sub.2 is hydrogen and the other of R.sub.1 and R.sub.2 is methyl; wherein R.sub.3 is hydrogen, C.sub.1 -C.sub.3 acyl, C.sub.3 or C.sub.4 alkyl or C.sub.3 or C.sub.4 alkenyl; wherein R.sub.4, R.sub.5 and R.sub.6 represent hydrogen or methyl with the additional proviso that one of R.sub.4, R.sub.5 and R.sub.6 is methyl and the other two of R.sub.4, R.sub.5 and R.sub.6 is hydrogen. Also described are processes for preparing such substituted tricyclodecane derivatives and processes for using the above defined substituted tricyclodecane derivatives for their organoleptic properties and compositions containing said substituted tricyclodecane derivatives including perfumes, perfumed articles, such as solid or liquid anionic, cationic, nonionic and zwitterionic detergents, fabric softeners and cosmetic powders; foodstuffs, chewing gums, toothpastes, medicinal products and chewing tobaccos; smoking tobacco compositions and smoking tobacco flavoring compositions and smoking tobacco articles containing such smoking tobacco compositions.

    Abstract translation: 描述了具有以下通用结构的取代的三环癸烷衍生物：其中Y是具有选自以下的结构的部分：其中一条虚线表示碳 - 碳单键，另一条为虚线 线代表碳 - 碳双键; 其中R1和R2表示氢或甲基，条件是R1和R2之一是氢，R1和R2中的另一个是甲基; 其中R3是氢，C1-C3酰基，C3或C4烷基或C3或C4链烯基; 其中R4，R5和R6代表氢或甲基，另外条件是R4，R5和R6之一是甲基，R4，R5和R6中的另外两个是氢。 还描述了制备这种取代的三环癸烷衍生物的方法和使用上述定义的取代的三环癸烷衍生物的感官特性的方法和含有所述取代的三环癸烷衍生物的组合物，包括香料，加香制品如固体或液体阴离子，阳离子，非离子和两性离子洗涤剂 ，织物柔软剂和化妆粉; 食品，口香糖，牙膏，药用产品和咀嚼烟草; 吸烟烟草组合物和吸烟烟草调味组合物和含有烟草烟草组合物的烟草制品。

    Substituted tricyclodecane derivatives, processes for producing same and organoleptic uses thereof
    13.
    发明授权
    Substituted tricyclodecane derivatives, processes for producing same and organoleptic uses thereof 失效

    公开(公告)号：US4410740A

    公开(公告)日：1983-10-18

    申请号：US422461

    申请日：1982-09-23

    Applicant: Mark A. Sprecker ,  John B. Hall

    Inventor： Mark A. Sprecker ,  John B. Hall

    IPC: A24B15/34 ,  C07C29/09 ,  C07C29/17 ,  C07C29/70 ,  C07C35/37 ,  C07C35/46 ,  C07C45/29 ,  C07C49/643 ,  C11B9/00 ,  C07C35/22

    CPC classification number: C11B9/0042 ,  A24B15/345 ,  C07C29/095 ,  C07C29/172 ,  C07C29/70 ,  C07C35/37 ,  C07C35/46 ,  C07C45/29 ,  C07C49/643 ,  C07C2103/60 ,  C07C2103/66

    Abstract: Described are substituted tricyclodecane derivatives having the generic structure: ##STR1## wherein Y is a moiety having a structure selected from the group consisting of: ##STR2## wherein one of the dashed lines represents a carbon-carbon single bond and the other of the dashed lines represents a carbon-carbon double bond; wherein R.sub.1 and R.sub.2 represent hydrogen or methyl with the proviso that one of R.sub.1 and R.sub.2 is hydrogen and the other of R.sub.1 and R.sub.2 is methyl; wherein R.sub.3 is hydrogen, C.sub.1 -C.sub.3 acyl, C.sub.3 or C.sub.4 alkyl or C.sub.3 or C.sub.4 alkenyl; wherein R.sub.4, R.sub.5 and R.sub.6 represent hydrogen or methyl with the additional proviso that one of R.sub.4, R.sub.5 and R.sub.6 is methyl and the other two of R.sub.4, R.sub.5 and R.sub.6 is hydrogen. Also described are processes for preparing such substituted tricyclodecane derivatives and processes for using the above defined substituted tricyclodecane derivatives for their organoleptic properties and compositions containing said substituted tricyclodecane derivatives including perfumes, perfumed articles, such as solid or liquid anionic, cationic, nonionic and zwitterionic detergents, fabric softeners and cosmetic powders; foodstuffs, chewing gums, toothpastes, medicinal products and chewing tobaccos; smoking tobacco compositions and smoking tobacco flavoring compositions and smoking tobacco articles containing such smoking tobacco compositions.

    Substituted tricyclodecane derivatives, processes for producing same and organoleptic uses thereof
    14.
    发明授权
    Substituted tricyclodecane derivatives, processes for producing same and organoleptic uses thereof 失效

    公开(公告)号：US4358617A

    公开(公告)日：1982-11-09

    申请号：US305534

    申请日：1981-09-25

    Applicant: Mark A. Sprecker ,  John B. Hall

    Inventor： Mark A. Sprecker ,  John B. Hall

    IPC: A24B15/34 ,  C07C29/09 ,  C07C29/17 ,  C07C29/70 ,  C07C35/37 ,  C07C35/46 ,  C07C45/29 ,  C07C49/643 ,  C11B9/00

    CPC classification number: C11B9/0042 ,  A24B15/345 ,  C07C29/095 ,  C07C29/17 ,  C07C29/70 ,  C07C35/37 ,  C07C35/46 ,  C07C45/29 ,  C07C49/643 ,  C07B2200/07 ,  C07C2103/68

    Abstract: Described are substituted tricyclodecane derivatives having the generic structure: ##STR1## wherein Y is a moiety having a structure selected from the group consisting of: ##STR2## wherein one of the dashed lines represents a carbon-carbon single bond and the other of the dashed lines represents a carbon-carbon double bond; wherein R.sub.1 and R.sub.2 represent hydrogen or methyl with the proviso that one of R.sub.1 and R.sub.2 is hydrogen and the other of R.sub.1 and R.sub.2 is methyl; wherein R.sub.3 is hydrogen, C.sub.1 -C.sub.3 acyl, C.sub.3 or C.sub.4 alkyl or C.sub.3 or C.sub.4 alkenyl; wherein R.sub.4, R.sub.5 and R.sub.6 represent hydrogen or methyl with the additional proviso that one of R.sub.4, R.sub.5 and R.sub.6 is methyl and the other two of R.sub.4, R.sub.5 and R.sub.6 is hydrogen. Also described are processes for preparing such substituted tricyclodecane derivatives and processes for using the above defined substituted tricyclodecane derivatives for their organoleptic properties and compositions containing said substituted tricyclodecane derivatives including perfumes, perfumed articles, such as solid or liquid anionic, cationic, nonionic and zwitterionic detergents, fabric softeners and cosmetic powders; foodstuffs, chewing gums, toothpastes, medicinal products and chewing tobaccos; smoking tobacco compositions and smoking tobacco flavoring compositions and smoking tobacco articles containing such smoking tobacco compositions.

    Substituted tricyclodecane derivatives
    15.
    发明授权
    Substituted tricyclodecane derivatives 失效
    取代三环癸烷衍生物

    公开(公告)号：US4346245A

    公开(公告)日：1982-08-24

    申请号：US305531

    申请日：1981-09-25

    Applicant: Mark A. Sprecker ,  John B. Hall

    Inventor： Mark A. Sprecker ,  John B. Hall

    IPC: A24B15/34 ,  C07C29/09 ,  C07C29/17 ,  C07C29/70 ,  C07C35/37 ,  C07C35/46 ,  C07C45/29 ,  C07C49/643 ,  C11B9/00 ,  C07C43/162

    CPC classification number: C11B9/0042 ,  A24B15/345 ,  C07C29/095 ,  C07C29/17 ,  C07C29/70 ,  C07C35/37 ,  C07C35/46 ,  C07C45/29 ,  C07C49/643 ,  C07C2103/66

    Abstract: Described are substituted tricyclodecane derivatives having the generic structure: ##STR1## wherein Y is a moiety having a structure selected from the group consisting of: ##STR2## wherein one of the dashed lines represents a carbon-carbon single bond and the other of the dashed lines represents a carbon-carbon double bond; wherein R.sub.1 and R.sub.2 represent hydrogen or methyl with the proviso that one of R.sub.1 and R.sub.2 is hydrogen and the other of R.sub.1 and R.sub.2 is methyl; wherein R.sub.3 is hydrogen, C.sub.1 -C.sub.3 acyl, C.sub.3 or C.sub.4 alkyl or C.sub.3 or C.sub.4 alkenyl; wherein R.sub.4, R.sub.5 and R.sub.6 represent hydrogen or methyl with the additional proviso that one of R.sub.4, R.sub.5 and R.sub.6 is methyl and the other two of R.sub.4, R.sub.5 and R.sub.6 is hydrogen. Also described are processes for preparing such substituted tricyclodecane derivatives and processes for using the above defined substituted tricyclodecane derivatives for their organoleptic properties and compositions containing said substituted tricyclodecane derivatives including perfumes, perfumed articles, such as solid or liquid anionic, cationic, nonionic and zwitterionic detergents, fabric softeners and cosmetic powders; foodstuffs, chewing gums, toothpastes, medicinal products and chewing tobaccos; smoking tobacco compositions and smoking tobacco flavoring compositions and smoking tobacco articles containing such smoking tobacco compositions.

    Abstract translation: 描述了具有以下通用结构的取代的三环癸烷衍生物：其中Y是具有选自以下的结构的部分：其中一条虚线表示碳 - 碳单键，另一条为虚线 线代表碳 - 碳双键; 其中R1和R2表示氢或甲基，条件是R1和R2之一是氢，R1和R2中的另一个是甲基; 其中R3是氢，C1-C3酰基，C3或C4烷基或C3或C4链烯基; 其中R4，R5和R6代表氢或甲基，另外条件是R4，R5和R6之一是甲基，R4，R5和R6中的另外两个是氢。 还描述了制备这种取代的三环癸烷衍生物的方法和使用上述定义的取代的三环癸烷衍生物的感官特性的方法和含有所述取代的三环癸烷衍生物的组合物，包括香料，加香制品如固体或液体阴离子，阳离子，非离子和两性离子洗涤剂 ，织物柔软剂和化妆粉; 食品，口香糖，牙膏，药用产品和咀嚼烟草; 吸烟烟草组合物和吸烟烟草调味组合物和含有烟草烟草组合物的烟草制品。

    Methyl substituted oxobicyclo-4,4,0-decane derivatives, process for preparing same and organoleptic uses thereof
    16.
    发明授权
    Methyl substituted oxobicyclo-4,4,0-decane derivatives, process for preparing same and organoleptic uses thereof 失效
    甲基取代的氧代二环-4,4,0癸烷衍生物，其制备方法和感官用途

    公开(公告)号：US4320772A

    公开(公告)日：1982-03-23

    申请号：US182451

    申请日：1980-08-29

    Applicant: Takao Yoshida

    Inventor： Takao Yoshida

    IPC: A23L27/20 ,  A61K8/34 ,  A61K8/35 ,  A61Q13/00 ,  C07C27/00 ,  C07C29/143 ,  C07C29/145 ,  C07C29/17 ,  C07C29/40 ,  C07C29/68 ,  C07C35/36 ,  C07C35/46 ,  C07C45/00 ,  C07C49/447 ,  C07C49/637 ,  C07C67/00 ,  C07F3/02 ,  C11B9/00

    CPC classification number: C11B9/0053 ,  C07C29/17 ,  C07C29/40 ,  C07C29/68 ,  C07C35/36 ,  C07F3/02 ,  C07C2102/28

    Abstract: Described are compounds having the generic structure: ##STR1## wherein the dashed line represents a carbon-carbon single bond or a carbon-carbon double bond; wherein X represents the moieties: ##STR2## wherein R.sub.1, R.sub.2, R.sub.3 and R.sub.4 represent hydrogen or methyl with the proviso that (i) at least three of R.sub.1, R.sub.2, R.sub.3 and R.sub.4 represent hydrogen and (ii) when the dashed line is a carbon-carbon single bond and X is: ##STR3## then one of R.sub.1, R.sub.2, R.sub.3 or R.sub.4 is methyl and the other represents hydrogen; wherein R.sub.5 represents hydrogen, MgX, MgR.sub.7, CdR.sub.7, ZnR.sub.7, Na, K or Li; wherein X represents Chloro, Bromo or Iodo; wherein R.sub.6 represents hydrogen or methyl; and wherein R.sub.7 represents lower alkyl; and uses thereof for their organoleptic properties in augmenting or enhancing or enhancing the aromas or tastes of perfumes, perfumed articles, foodstuffs, chewing gums, smoking tobaccos, toothpastes, medicinal products, chewing tobacco and smoking tobacco articles, as well as processes for preparing same.

    Abstract translation: 描述的是具有通用结构的化合物：其中虚线表示碳 - 碳单键或碳 - 碳双键; 其中X表示部分：其中R 1，R 2，R 3和R 4表示氢或甲基，条件是（i）R 1，R 2，R 3和R 4中的至少3个表示氢，和（ii） 虚线是碳 - 碳单键，X是：其中R1，R2，R3或R4之一是甲基，另一个代表氢; 其中R5表示氢，MgX，MgR7，CdR7，ZnR7，Na，K或Li; 其中X表示氯，溴或碘; 其中R6表示氢或甲基; 并且其中R 7表示低级烷基; 以及其用于增强或增强香料，香料，食品，口香糖，吸烟烟草，牙膏，药用产品，咀嚼烟草和烟草制品的香气或口味的感官特性，以及其制备方法 。

    Process for preparing lithium polyhydric alkoxides
    18.
    发明授权
    Process for preparing lithium polyhydric alkoxides 失效
    制备锂多羟基烷氧基化物的方法

    公开(公告)号：US3520940A

    公开(公告)日：1970-07-21

    申请号：US3520940D

    申请日：1968-12-16

    Applicant: FOOT MINERAL CO

    Inventor： SMITH WILLIAM NOVIS JR

    IPC: C07C29/70 ,  C07C31/30 ,  C07C33/044 ,  C07C33/26 ,  C07C35/04 ,  C07C35/46 ,  C07C37/66 ,  C07C39/235 ,  C07C35/02 ,  C08G17/06

    CPC classification number: C07C29/70 ,  C07C29/705 ,  C07C37/66 ,  C07C2601/14 ,  C07C31/30 ,  C07C35/46 ,  C07C33/044 ,  C07C39/235 ,  C07C33/26

    Abstract: 1,143,897. Alkali metal polyhydric alcoholates and phenolates. METALLGESELLSCHAFT A.G. 8 Feb., 1968 [17 Feb., 1967], No. 6336/68. Heading C2C. Alkali metal polyhydric alcoholates and phenolates are prepared by reacting under anhydrous conditions an alkali metal alcoholate of a monohydric alcohol containing 1-8 carbon atoms with a polyhydric alcohol or phenol containing up to 6 hydroxy groups and from 2-18 carbon atoms in a liquid reaction medium which is a monohydric alkyl alcohol containing 1-8 carbon atoms, a liquid hydrocarbon containing 5-12 carbon atoms or a mixture thereof and recovering the product from the reaction medium. The concentration of the alkali metal alcoholate may be at least 0À1 molar and the amount of polyhydric alcohol reacted per mole of said alkali metal alcoholate is OÀ5-1 molethereof. The alkali metal employed is sodium, potassium or lithium. In most cases the product of the reaction will be a monoalkali metal derivative although in some cases a dialkali metal derivative can be prepared. The alkali metal alcoholate of the monohydric alkyl alcohol may be formed in situ in the liquid reaction medium by reacting 1 mole of the alkali metal or the hydride thereof with 1 mole of the monohydric alkyl alcohol. Both the reaction between the monohydric alkyl alcohol and the alkali metal and the reaction between the monohydric alkyl alkoxide and the polyhydric alcohol preferably take place in an atmosphere substantially free of oxygen, carbon dioxide and moisture such as under an atmosphere of an inert gas such as argon, helium or nitrogen and at elevated temperatures of at least 50‹ C. although the reaction will proceed at room temperature. Examples prepared are the monolithium derivatives of ethylene glycol, 2,2,4,4 - tetramethyl - 1,3 - cyclobutanediol, trimethylol - propane, 2,2 - dimethyl - 1,3 - propanediol, pentaerythritol, 1,2 - propane diol, 1,4 - butanediol, glycerine, 1,2 - cyclohexanediol, 1,12 - octadodecanediol, 2,21 - dihydroxybiphenyl, resorcinol, mannitol, 2,5 - dimethyl - 2,5 - hexanediol, 2,5 -dihydroxy- 2,5 - dimethyl - hexyne, the monosodium derivative of ethylene glycol and the diluthium derivatives of 1,4 - butanediol and 1,3 - propanediol.

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