CONTINUOUS PRODUCTION DEVICE FOR ORGANOPHOSPHORUS NITRILE-CATALYZED HIGH-MOLECULAR-WEIGHT POLYSILOXANE

    公开(公告)号:US20250001388A1

    公开(公告)日:2025-01-02

    申请号:US18827839

    申请日:2024-09-08

    Abstract: This disclosure belongs to the field of organic silicon polymer material preparation, particularly relating to a continuous production device for organophosphorus nitrile-catalyzed high-molecular-weight polysiloxane. It includes a reaction device with a horizontal configuration and dual-axis stirring, where the diameters of the dual axes decrease gradually from the feed port to the discharge outlet, and the corresponding nominal diameters of the paddles increase gradually from the feed port to the discharge outlet. The stirring shaft and paddles are hollow and can be externally heated or cooled. The dual-axis engagement provides mass transfer, heat transfer, and axial propelling force. This reaction device exhibits excellent mass transfer and heat transfer effects, resulting in uniform products with narrow molecular weight distribution and low volatile content. It is particularly suitable for the continuous production of high-viscosity, high-molecular-weight polysiloxanes catalyzed by organophosphorus nitrile. This production device can be adapted to various traditional chemical reaction equipment.

    Silicone emulsion composition
    4.
    发明授权

    公开(公告)号:US12173155B2

    公开(公告)日:2024-12-24

    申请号:US17284666

    申请日:2019-08-28

    Abstract: An addition reaction-curable silicone emulsion composition containing a water-soluble silane coupling agent (I) and an organopolysiloxane (II) having at least two alkenyl groups in one molecule thereof, where the water-soluble silane coupling agent (I) has at least one group selected from among a succinic anhydride group, a quaternary ammonium group, and a ureido group, and 1 part by mass or more of the water-soluble silane coupling agent (I) is contained relative to 100 parts by mass of the organopolysiloxane (II). This provides: a silicone emulsion composition that gives a cured film adhering well to plastic film substrates regardless of the type, while having suitable release properties regarding adhesives; and a delamination film made by forming a cured film of the silicone emulsion composition.

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