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1.发明申请公开(公告)号：US20190194029A1
公开(公告)日：2019-06-27
申请号：US16068989
申请日：2017-01-19
申请人： PURAC BIOCHEM BV
IPC分类号： C01F5/30 , C01F5/10 , C01B7/03 , B01D1/26 , B01D1/28 , C12P7/52 , C07C51/02 , C12P7/48 , C12P7/44 , C12P7/40 , C12P7/56 , C12P17/04 , C12P7/42 , C12P7/46
CPC分类号： C01F5/30 , B01D1/26 , B01D1/28 , C01B7/035 , C01F5/10 , C07C51/02 , C12P7/40 , C12P7/42 , C12P7/44 , C12P7/46 , C12P7/48 , C12P7/52 , C12P7/56 , C12P17/04 , C07C55/10 , C07C59/08 , C07C59/06 , C07C59/01
摘要： Magnesium chloride solutions including providing aqueous magnesium chloride solution with magnesium chloride concentration of 10-30 wt. % to concentration step where water is evaporated, resulting in concentrated magnesium chloride solution with magnesium chloride concentration of 30-50 wt. %, wherein concentration step is carried out in one or more stages, wherein at least one of the stages is conducted at elevated pressure, withdrawing concentrated magnesium chloride solution from concentration step, and providing it to thermohydrolysis reactor of at least 300° C., withdrawing MgO from thermohydrolysis reactor in solid form, and withdrawing a HCl containing gas stream of at least 300° C. from thermohydrolysis reactor, providing the HCl-containing gas stream of at least 300° C. to cooling step, where HCl-containing gas stream is contacted with cooling liquid, withdrawing HCl-containing gas stream below 150° C. from cooling step, circulating cooling liquid through heat exchanger where energy is transferred to heating liquid which circulates from heat exchanger to concentration step.
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公开(公告)号：US09550712B2
公开(公告)日：2017-01-24
申请号：US14238686
申请日：2012-08-16
申请人： André Banier De Haan , Jan Van Breugel , Paulus Loduvicus Johannes Van Der Weide , Peter Paul Jansen , José María Vidal Lancis , Augustín Cerdà Baró
发明人： André Banier De Haan , Jan Van Breugel , Paulus Loduvicus Johannes Van Der Weide , Peter Paul Jansen , José María Vidal Lancis , Augustín Cerdà Baró
IPC分类号： C07C51/02 , C07C51/42 , C07C51/43 , C01F5/30 , C01F5/10 , C07D307/60 , C07D307/68 , C01B7/03
CPC分类号： C07C51/02 , C01B7/035 , C01F5/06 , C01F5/10 , C01F5/16 , C01F5/30 , C07C51/42 , C07C51/43 , C07D307/60 , C07D307/68 , C07C55/10
摘要： The invention provides a method for preparing a carboxylic acid, which method includes the steps of providing magnesium carboxylate, wherein the carboxylic acid corresponding with the carboxylate has a solubility in water at 20° C. of 80 g/100 g water or less; acidifying the magnesium carboxylate with HCl, thereby obtaining a solution comprising carboxylic acid and magnesium chloride (MgCl2); optionally a concentration step, wherein the solution comprising carboxylic acid and MgCl2 is concentrated; precipitating the carboxylic acid from the solution comprising the carboxylic acid and MgCl2, thereby obtaining a carboxylic acid precipitate and a MgCl2 solution.
摘要翻译： 本发明提供一种制备羧酸的方法，该方法包括提供羧酸镁的步骤，其中对应于羧酸酯的羧酸在20℃下在水中的溶解度为80g / 100g水或更少; 用HCl酸化羧酸镁，从而得到包含羧酸和氯化镁（MgCl 2）的溶液; 任选的浓缩步骤，其中将包含羧酸和MgCl 2的溶液浓缩; 从包含羧酸和MgCl 2的溶液中沉淀羧酸，由此得到羧酸沉淀和MgCl 2溶液。
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公开(公告)号：US09422217B2
公开(公告)日：2016-08-23
申请号：US14402441
申请日：2013-05-23
申请人： PURAC BIOCHEM BV
发明人： Adriaan Dirk Kon , André Banier De Haan , Paulus Loduvicus Johannes Van Der Weide , Tanja Ðekic Živkovic , Lucien Henri Leander Jozef De Koninck
CPC分类号： C07C51/02 , B01J39/05 , B01J49/53 , C01B7/035 , C01F5/02 , C01F5/10 , C01F5/16 , C01F5/30 , C07C55/10 , C07C59/08 , C07C53/122 , C07C59/01 , C07C59/265 , C07C55/14 , C07C57/15 , C07C57/145 , C07C63/26 , C07C57/04
摘要： The invention is directed to a method for recovering carboyxlic acid from an magnesium carboxylate containing aqueous mixture, including the steps of: contacting the aqueous mixture with an acidic ion exchanger, thereby forming a carboxylic acid mixture and an ion exchanger loaded with magnesium ions; contacting the ion exchanger loaded with magnesium ions with a hydrochloric acid solution, thereby forming a magnesium chloride solution; and thermally decomposing the magnesium chloride solution at a temperature of at least 300° C., thereby forming magnesium oxide (MgO) and hydrogen chloride (HCl).
摘要翻译： 本发明涉及从含羧酸镁的含水混合物中回收羧基甲酸的方法，包括以下步骤：使含水混合物与酸性离子交换剂接触，由此形成羧酸混合物和负载有镁离子的离子交换剂; 使负载有镁离子的离子交换剂与盐酸溶液接触，从而形成氯化镁溶液; 并在至少300℃的温度下热分解氯化镁溶液，从而形成氧化镁（MgO）和氯化氢（HCl）。
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公开(公告)号：US09376364B2
公开(公告)日：2016-06-28
申请号：US14238666
申请日：2012-08-16
申请人： André Banier De Haan , Jan Van Breugel , Paulus Loduvicus Johannes Van Der Weide , Peter Paul Jansen , José María Vidal Lancis , Agustín Cerdà Baró
发明人： André Banier De Haan , Jan Van Breugel , Paulus Loduvicus Johannes Van Der Weide , Peter Paul Jansen , José María Vidal Lancis , Agustín Cerdà Baró
摘要： The invention provides a method for preparing a succinic acid, which method includes the steps of: providing magnesium succinate; acidifying the magnesium succinate with hydrochloric acid (HCl), thereby obtaining a solution including succinic acid and magnesium chloride (MgCl2); optionally a concentration step, wherein the solution including succinic acid and MgCl2 is concentrated; precipitating succinic acid from the solution including succinic acid and MgCl2, thereby obtaining a succinic acid precipitate and a MgCl2 solution. The addition of HCl to a magnesium salt of succinic acid and subsequent precipitation of succinic acid from the solution leads to a very efficient separation of succinic acid from a magnesium succinate solution.
摘要翻译： 本发明提供一种制备琥珀酸的方法，该方法包括以下步骤：提供琥珀酸镁; 用盐酸（HCl）酸化琥珀酸镁，由此得到包含琥珀酸和氯化镁（MgCl 2）的溶液; 任选的浓缩步骤，其中将包含琥珀酸和MgCl 2的溶液浓缩; 从包括琥珀酸和MgCl 2的溶液中沉淀琥珀酸，从而得到琥珀酸沉淀和MgCl 2溶液。 向琥珀酸镁盐中加入HCl，随后从溶液中沉淀琥珀酸导致琥珀酸与琥珀酸镁溶液的非常有效的分离。
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公开(公告)号：US20160016812A1
公开(公告)日：2016-01-21
申请号：US14429588
申请日：2014-03-06
IPC分类号： C01G23/02
CPC分类号： C01G23/024 , B09B3/00 , B09B5/00 , C01B7/035 , C01G23/022 , C01G49/02 , C01G49/10
摘要： A method for producing titanium tetrachloride is provided, in which valuable materials such as unreacted titanium-containing raw material, carbon raw material and chlorine can be recovered from solid recovered material generated in chlorinating process of titanium-containing raw material, and titanium-containing raw material can be efficiently used. The treatment method of titanium-containing raw material includes the steps: separating and removing impurities selectively from the titanium-containing raw material as chlorides so as to obtain high titanium-containing raw material, producing titanium tetrachloride using the high titanium-containing raw material, and performing separating process of impurities from solid recovered material byproduced in the production of titanium tetrachloride, together with selective chlorinating treatment of the titanium-containing raw material. Thus, the high titanium-containing raw material can be produced while recovering chlorine and impure oxides.
摘要翻译： 提供一种生产四氯化钛的方法，其中可从含钛原料的氯化过程中产生的固体回收材料中回收诸如未反应的含钛原料，碳原料和氯的有价值的材料，以及含钛原料 材料可以有效地使用。 含钛原料的处理方法包括以下步骤：从含钛原料中选择性地分离和除去杂质为氯化物，以获得高含钛原料，使用高含钛原料生产四氯化钛， 并且通过在生产四氯化钛中产生的固体回收材料进行杂质的分离处理以及含钛原料的选择性氯化处理。 因此，可以在回收氯和不纯的氧化物的同时制备高含钛原料。
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公开(公告)号：US09061986B2
公开(公告)日：2015-06-23
申请号：US14238633
申请日：2012-08-16
申请人： André Banier De Haan , Jan Van Breugel , Paulus Loduvicus Johannes Van Der Weide , Peter Paul Jansen , José María Vidal Lancis , Agustín Cerdà Baró
发明人： André Banier De Haan , Jan Van Breugel , Paulus Loduvicus Johannes Van Der Weide , Peter Paul Jansen , José María Vidal Lancis , Agustín Cerdà Baró
摘要： A method for preparing a carboxylic acid, includes the steps of: providing magnesium carboxylate, wherein the carboxylic acid corresponding with the carboxylate is selected from the group made of 2,5-furandicarboxylic acid, fumaric acid, adipic acid, itaconic acid, citric acid, glutaric acid, maleic acid, malonic acid, oxalic acid and fatty acids having more than 10 carbon atoms; acidifying the magnesium carboxylate with hydrogen chloride (HCl), thereby obtaining a solution including carboxylic acid and magnesium chloride (MgCl2); optionally a concentration step, wherein the solution including carboxylic acid and MgCl2 is concentrated; and precipitating the carboxylic acid from the solution including the carboxylic acid and MgCl2, thereby obtaining a carboxylic acid precipitate and a MgCl2 solution.
摘要翻译： 一种制备羧酸的方法，包括以下步骤：提供羧酸镁，其中对应于羧酸酯的羧酸选自2,5-呋喃二羧酸，富马酸，己二酸，衣康酸，柠檬酸 戊二酸，马来酸，丙二酸，草酸和具有多于10个碳原子的脂肪酸; 用氯化氢（HCl）酸化羧酸镁，从而得到包括羧酸和氯化镁（MgCl 2）的溶液; 任选的浓缩步骤，其中将包含羧酸和MgCl 2的溶液浓缩; 并从包括羧酸和MgCl 2的溶液中沉淀出羧酸，从而得到羧酸沉淀和MgCl 2溶液。
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公开(公告)号：US20150159239A1
公开(公告)日：2015-06-11
申请号：US14413940
申请日：2013-07-12
申请人： ORBITE ALUMINAE INC.
IPC分类号： C22B21/00 , C22B34/12 , C01B33/193 , C22B26/22 , C22B59/00 , C22B3/44 , C22B3/10 , C01G49/06
CPC分类号： C22B21/0015 , C01B7/035 , C01B33/193 , C01F7/22 , C01F7/306 , C01F7/56 , C01G23/02 , C01G23/047 , C01G49/06 , C01G53/04 , C22B3/10 , C22B3/44 , C22B26/22 , C22B34/1245 , C22B34/1259 , C22B59/00
摘要： There are provided processes for preparing various products from various materials. For example, such processes are effective for extracting titanium and various other metals from various materials, thereby allowing for preparing products such as titanium chloride and titanium oxide. These processes can comprise leaching the starting material with HCl so as to obtain a leachate and a solid. The solid can be treated so as to substantially selectively extract titanium therefrom while the leachate can be treated so as to substantially selectively recover a first metal chloride therefrom.
摘要翻译： 提供了从各种材料制备各种产品的方法。 例如，这些方法对从各种材料中提取钛和各种其它金属是有效的，从而允许制备诸如氯化钛和氧化钛的产物。 这些方法可以包括用HCl浸出原料以获得渗滤液和固体。 可以处理固体以便基本上选择性地从其中提取钛，同时处理渗滤液以便基本上选择性地从其中回收第一金属氯化物。
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8.发明授权公开(公告)号：US08173005B2
公开(公告)日：2012-05-08
申请号：US12184423
申请日：2008-08-01
申请人： Greg F. Naterer , Richard Marceau
发明人： Greg F. Naterer , Richard Marceau
CPC分类号： C25C1/12 , C01B3/08 , C01B7/035 , C01B13/0203 , C25C5/02 , Y02E60/36 , Y02P20/129
摘要： This invention relates to hydrogen production using combined heat pumps and a thermochemical cycle. Low grade waste heat can be upgraded to higher temperatures via salt/ammonia and/or MgO/vapor chemical heat pumps, which release heat at successively higher temperatures through exothermic reactions, or vapor compression heat pumps that upgrade thermal energy with phase change fluids. Using this new approach, low grade heat or waste heat from nuclear or other industrial sources can be transformed to a useful energy supply for thermochemical hydrogen production.
摘要翻译： 本发明涉及使用组合热泵和热化学循环的氢气生产。 通过盐/氨和/或MgO /蒸汽化学热泵可以将低等级的余热升级到更高的温度，这些热泵通过放热反应在连续更高的温度下释放热量，或者通过相变流体升级热能的蒸气压缩热泵。 使用这种新方法，来自核或其他工业来源的低等级的热或废热可以转化为用于热化学氢生产的有用的能量供应。
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公开(公告)号：US08058486B2
公开(公告)日：2011-11-15
申请号：US12404130
申请日：2009-03-13
申请人： Daniel C. Merkel , Hsueh Sung Tung , Konstantin A. Pokrovski , Selma Bektesevic , Robert C. Johnson , Haiyou Wang
发明人： Daniel C. Merkel , Hsueh Sung Tung , Konstantin A. Pokrovski , Selma Bektesevic , Robert C. Johnson , Haiyou Wang
IPC分类号： C07C17/25
CPC分类号： C07C21/18 , C01B7/035 , C01B7/0706 , C01B7/195 , C07C17/087 , C07C17/10 , C07C17/206 , C07C17/25 , C07C17/383 , Y02P20/125 , Y02P20/582 , C07C19/10
摘要： A method for preparing 2,3,3,3-tetrafluoroprop-1-ene comprising (a) providing a starting composition comprising at least one compound having a structure selected from Formulae I, II and III: CX2═CCl—CH2X (Formula I) CX3—CCl═CH2 (Formula II) CX3—CHCl—CH2X (Formula III) wherein X is independently selected from F, Cl, Br, and I, provided that at least one X is not fluorine; (b) contacting said starting composition with a first fluorinating agent to produce a first intermediate composition comprising 2-chloro-3,3,3-trifluoropropene and a first chlorine-containing byproduct; (c) contacting said first intermediate composition with a second fluorinating agent to produce a second intermediate composition comprising 2-chloro-1,1,1,2-tetrafluoropropane and a second chlorine-containing byproduct; and (d) catalytically dehydrochlorinating at least a portion of said 2-chloro-1,1,1,2-tetrafluoropropane to produce a reaction product comprising 2,3,3,3-tetrafluoroprop-1-ene.
摘要翻译： 一种制备2,3,3,3-四氟丙-1-烯的方法，包括（a）提供起始组合物，其包含至少一种具有选自式I，II和III的结构的化合物：CX2 = CCl-CH2X（式I ）CX3-CCl = CH2（式II）CX3-CHCl-CH2X（式III）其中X独立地选自F，Cl，Br和I，条件是至少一个X不是氟; （b）使所述起始组合物与第一氟化剂接触以产生包含2-氯-3,3,3-三氟丙烯和第一含氯副产物的第一中间体组合物; （c）使所述第一中间体组合物与第二氟化剂接触以产生包含2-氯-1,1,1,2-四氟丙烷和第二含氯副产物的第二中间体组合物; 和（d）将至少一部分所述2-氯-1,1,1,2-四氟丙烷催化脱氯化氢以产生包含2,3,3,3-四氟丙-1-烯的反应产物。
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公开(公告)号：US20090209784A1
公开(公告)日：2009-08-20
申请号：US12378508
申请日：2009-02-17
IPC分类号： C07C263/10
CPC分类号： C01B7/035 , C07C263/10 , C07C263/20 , C07C265/14 , C07C265/12
摘要： The present invention relates to a process for the preparation of isocyanates by reacting the appropriate amines with phosgene, condensing the gas mixture thereby obtained, stripping the liquid phase thereby obtained and returning the solvent so retained in liquid form to the reaction stage. The gaseous constituents are then purified further in an absorption process.
摘要翻译： 本发明涉及通过使适当的胺与光气反应制备异氰酸酯的方法，将由此得到的气体混合物冷凝，将由此获得的液相汽提，并使溶剂保持液态返回到反应阶段。 然后在吸收过程中进一步纯化气态成分。
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