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公开(公告)号：US09150493B2
公开(公告)日：2015-10-06
申请号：US13521523
申请日：2011-01-10
申请人： Wolfgang Lorenz , Bernd Pennemann
发明人： Wolfgang Lorenz , Bernd Pennemann
IPC分类号： C07C211/00 , C07C209/36
CPC分类号： C07C209/36 , C07C211/51
摘要： The invention relates to a process for the preparation of aromatic amines in the liquid phase by catalytic hydrogenation of the corresponding nitroaromatic compounds in at least two reaction spaces connected in series, wherein at least one reaction space is operated isothermally and at least the reaction space connected downstream thereof is operated adiabatically, and in preferred embodiments the sudden adiabatic temperature change is used for monitoring the reaction.
摘要翻译： 本发明涉及通过在至少两个串联连接的反应空间中对相应的硝基芳族化合物进行催化氢化在液相中制备芳族胺的方法，其中至少一个反应空间是等温运行的，并且至少连接的反应空间 其下游绝热操作，在优选的实施方案中，突然的绝热温度变化用于监测反应。
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公开(公告)号：US09102594B2
公开(公告)日：2015-08-11
申请号：US13696195
申请日：2011-04-29
IPC分类号： C07C263/10
CPC分类号： C07C263/10 , C07C265/14
摘要： The invention relates to a process for the preparation of isocyanates by reaction of the corresponding amines with phosgene in the gas phase, wherein a diluent containing between 90.0000% by weight and 99.9999% by weight of substances which are inert in the phosgenation process and between 0.0001% by weight and 10.0000% by weight of oxygen is present during the conversion of the amine into the gas phase and the molar ratio of amine to oxygen (O2) is ≧1,000:1.
摘要翻译： 本发明涉及一种通过相应的胺与气相中的光气反应来制备异氰酸酯的方法，其中包含在光气化过程中为惰性的物质的90.0000重量％至99.9999重量％的稀释剂和0.0001 在胺转化为气相期间存在重量％和10.0000％重量的氧，胺与氧（O 2）的摩尔比为≧1,000:1。
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公开(公告)号：US20130131377A1
公开(公告)日：2013-05-23
申请号：US13696195
申请日：2011-04-29
IPC分类号： C07C263/10
CPC分类号： C07C263/10 , C07C265/14
摘要： The invention relates to a process for the preparation of isocyanates by reaction of the corresponding amines with phosgene in the gas phase, wherein a diluent containing between 90.0000% by weight and 99.9999% by weight of substances which are inert in the phosgenation process and between 0.0001% by weight and 10.0000% by weight of oxygen is present during the conversion of the amine into the gas phase and the molar ratio of amine to oxygen (O2) is ≧1,000:1.
摘要翻译： 本发明涉及一种通过相应的胺与气相中的光气反应来制备异氰酸酯的方法，其中包含在光气化过程中为惰性的物质的90.0000重量％至99.9999重量％的稀释剂和0.0001 在胺转化为气相期间存在重量％和10.0000％（重量）的氧，胺与氧（O 2）的摩尔比≥1000:1。
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公开(公告)号：US20090209784A1
公开(公告)日：2009-08-20
申请号：US12378508
申请日：2009-02-17
IPC分类号： C07C263/10
CPC分类号： C01B7/035 , C07C263/10 , C07C263/20 , C07C265/14 , C07C265/12
摘要： The present invention relates to a process for the preparation of isocyanates by reacting the appropriate amines with phosgene, condensing the gas mixture thereby obtained, stripping the liquid phase thereby obtained and returning the solvent so retained in liquid form to the reaction stage. The gaseous constituents are then purified further in an absorption process.
摘要翻译： 本发明涉及通过使适当的胺与光气反应制备异氰酸酯的方法，将由此得到的气体混合物冷凝，将由此获得的液相汽提，并使溶剂保持液态返回到反应阶段。 然后在吸收过程中进一步纯化气态成分。
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公开(公告)号：US20070249859A1
公开(公告)日：2007-10-25
申请号：US11409940
申请日：2006-04-24
申请人： Matthias Bohm , Wolfgang Lorenz , Bill Brady , Donald Pferdehirt
发明人： Matthias Bohm , Wolfgang Lorenz , Bill Brady , Donald Pferdehirt
IPC分类号： C07C263/10
CPC分类号： C07C263/10 , C01B7/0706 , C01B7/0731 , C07C263/20 , C07C265/14
摘要： Isocyanates are produced by a) reacting at least one amine with phosgene, optionally in the presence of a solvent to produce the corresponding isocyanate and a stream containing hydrogen chloride, phosgene and optionally solvent, low-boiling compounds and inert substances is obtained, b) separating the stream containing hydrogen chloride, phosgene and optionally solvent, low-boiling compounds and inert substances in an at least two-stage sequence of absorption steps that includes (1) at least one isothermal absorption step and (2) at least one adiabatic absorption step, to obtain (i) a hydrogen chloride stream containing phosgene in concentrations of at most 0.5 wt. % (based on the weight of the hydrogen chloride stream) and (ii) a liquid phosgene stream, and c) recycling the liquid phosgene stream (ii) to the reaction of amine with phosgene.
摘要翻译： 异氰酸酯通过以下方法制备：a）任选地在溶剂存在下使至少一种胺与光气反应以产生相应的异氰酸酯，并且获得含有氯化氢，光气和任选溶剂的低沸点化合物和惰性物质的流，b） 在至少两级的吸收步骤序列中分离含有氯化氢，光气和任选溶剂的低沸点化合物和惰性物质，其包括（1）至少一个等温吸收步骤和（2）至少一个绝热吸收 步骤，以获得（i）含有至多0.5重量％浓度的光气的氯化氢料流。 ％（基于氯化氢流的重量）和（ii）液体光气流，和c）将液体光气流（ii）再循环到胺与光气的反应中。
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公开(公告)号：US20070128365A1
公开(公告)日：2007-06-07
申请号：US11611812
申请日：2006-12-15
申请人： Matthias Koch , Kerstin Unger , Wolfgang Lorenz , Andreas Kunz , Eva Wilke
发明人： Matthias Koch , Kerstin Unger , Wolfgang Lorenz , Andreas Kunz , Eva Wilke
CPC分类号： C09D5/24 , C09D5/084 , Y10T428/12569
摘要： The present invention relates to electrically conductive and electrically weldable anti-corrosion compositions for coating metal surfaces, a process for coating metal surfaces with electrically conductive organic coatings, as well as the correspondingly coated and optionally painted metal strips, sheets or parts, the coatings comprising: an organic binder, an anti-corrosion pigment, at least one conductive pigment with a density of at least 3 g/cm3 and optionally at least one conductive pigment with a density of less than 3 g/cm3.
摘要翻译： 本发明涉及用于涂覆金属表面的导电和可电焊接的防腐蚀组合物，用导电有机涂层涂覆金属表面的方法，以及相应地涂覆和任选涂漆的金属条，片或部分，所述涂层包括 ：有机粘合剂，防腐蚀颜料，至少一种密度为至少3g / cm 3的导电颜料和任选的至少一种导电颜料，密度小于3g / cm 3。
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公开(公告)号：US06835459B2
公开(公告)日：2004-12-28
申请号：US10275538
申请日：2002-11-06
申请人： Wolfgang Lorenz , Andreas Kunz , Eva Wilke
发明人： Wolfgang Lorenz , Andreas Kunz , Eva Wilke
IPC分类号： B32B1504
CPC分类号： C09D5/24 , C09D163/00 , C23C28/00 , Y10S428/931 , Y10T428/12014 , Y10T428/12569 , Y10T428/26 , Y10T428/30 , Y10T428/31504 , Y10T428/31678 , C08L2666/54
摘要： A conductive and weldable anti-corrosion composition for coating metal surfaces which contains: (a) 5 to 40 wt. % of an organic binder containing: (aa) at least one epoxide resin (ab) at least one hardener selected from cyanoguanidine, benzoguanamine and plasticised urea resin (ac) at least one amine adduct selected from polyoxyalkylenetriamine and epoxide resin/amine adducts (b) 0 to 15 wt. % of an anti-corrosion pigment (c) 40 to 70 wt. % of a conductive pigment selected from powdered zinc, aluminum, graphite, molybdenum sulfide, carbon black and iron phosphide (d) 0 to 45 wt. % of a solvent; and a lacquered metal structural part which has a conductive organic layer.
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公开(公告)号：US4658635A
公开(公告)日：1987-04-21
申请号：US838612
申请日：1986-03-11
CPC分类号： G01M9/04
摘要： The simulator is equipped with a multipartite support comprising a part for the accommodation of a model. The parts of the support are arranged telescopically in the form of an approximate semicircle. Hydrostatic bearings are used as mountings.
摘要翻译： 该模拟器配备有一个多部分支持，其中包括用于模拟模型的部件。 支撑件的部分以大致半圆的形式可伸缩地布置。 静压轴承用作安装座。
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公开(公告)号：US09365503B2
公开(公告)日：2016-06-14
申请号：US12636925
申请日：2009-12-14
申请人： Klaus Biskup , Rainer Bruns , Wolfgang Lorenz , Lars Padeken , Bernd Pennemann , Fritz Pohl , Andreas Rausch , Friedhelm Steffens
发明人： Klaus Biskup , Rainer Bruns , Wolfgang Lorenz , Lars Padeken , Bernd Pennemann , Fritz Pohl , Andreas Rausch , Friedhelm Steffens
IPC分类号： C07C263/10
CPC分类号： C07C263/10 , C07C265/14
摘要： Meta-toluene-diisocyanate is produced by reacting meta-toluenediamine with phosgene in the gas phase. The meta-toluenediamine to be vaporized for use in this phosgenation process must contain less than 0.5 wt. % of toluenediamine residue, a total of less than 0.2 wt. % of ammonia and cycloaliphatic amines, and less than 20 ppm of heavy metals. At least 0.1 wt. % of the liquid meta-toluenediamine being to be vaporized must not be vaporized. This non-vaporized content of the meta-toluenediamine must not be fed to the phosgenation reactor.
摘要翻译： 甲基 - 甲苯二异氰酸酯是通过间苯二甲胺与光气在气相中反应制得的。 要在该光气化过程中使用的待蒸发的间甲苯二胺必须含有小于0.5wt。 ％的甲苯二胺残留物，总计小于0.2wt。 ％的氨和脂环族胺，以及小于20ppm的重金属。 至少0.1wt。 待蒸发的液体间甲苯二胺的％不得蒸发。 间甲苯二胺的这种非汽化含量不得进料到光气化反应器中。
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公开(公告)号：US09051243B2
公开(公告)日：2015-06-09
申请号：US13383936
申请日：2010-07-06
IPC分类号： C07C263/10
CPC分类号： C07C263/10 , C07C265/14
摘要： Isocyanates are produced by reacting a primary amine with phosgene in the gas phase. In this process, the amine is vaporized and then superheated prior to introduction into the reactor. The amine is superheated to a temperature at least 10° C. above dew point before entry into the reactor. A pressure difference between the vaporizer and entry into the reactor of from 1 to 500 mbar is maintained.
摘要翻译： 异氰酸酯是通过在气相中使伯胺与光气反应来制备的。 在该方法中，胺被蒸发，然后在引入反应器之前过热。 胺在进入反应器之前过热至高于露点至少10℃的温度。 蒸发器和进入反应器的压差保持在1至500毫巴之间。
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