公开(公告)号：US11802091B2

公开(公告)日：2023-10-31

申请号：US17971018

申请日：2022-10-21

申请人： The Government of the United States of America, as represented by the Secretary of Homeland Security

发明人： Inho Cho

IPC分类号： C04B41/45 ,  C04B41/00 ,  C04B41/62 ,  B01J19/00 ,  B01J15/00 ,  C04B111/54

CPC分类号： C04B41/4531 ,  B01J15/00 ,  B01J19/0073 ,  C04B41/009 ,  C04B41/455 ,  C04B41/62 ,  B01J2219/00051 ,  B01J2219/00162 ,  C04B2111/542

摘要： Various embodiments of the present invention are directed towards a system and method relating to depositing vapor in a sample. For example, a device includes a vapor source chamber configured to contain a vapor source material to generate vapor. An activation chamber is configured to contain a sample. The activation chamber is in fluid communication with the vapor source chamber to receive the vapor. A permeable separator divides the vapor source chamber and the activation chamber, and isolates the sample in the activation chamber while allowing vapor to pass between the vapor source chamber and the activation chamber. The device is sealable and configured to apply vacuum to the vapor and sample, to cause deposition of the vapor into the pumice stone samples.

公开(公告)号：US09649617B2

公开(公告)日：2017-05-16

申请号：US14902076

申请日：2013-11-21

申请人： Samsung SDI Co., Ltd.

发明人： Sang Kyun Im ,  Ki Yon Lee ,  Shin Hyo Bae ,  Young Jun Kim ,  Kyoung Kyun Park ,  Young Sub Jin ,  Sang Hyun Jeon

IPC分类号： B01J19/28 ,  C08G63/80 ,  C08G64/20 ,  C08G69/06 ,  C08G69/30 ,  B01J19/00 ,  C08G63/78

CPC分类号： B01J19/28 ,  B01J19/0073 ,  B01J2219/00094 ,  B01J2219/00159 ,  B01J2219/00162 ,  B01J2219/0204 ,  B01J2219/0245 ,  C08G63/785 ,  C08G63/80 ,  C08G64/205 ,  C08G69/06 ,  C08G69/30 ,  Y02P20/149

摘要： A continuous solid-state polymerization device according to the present invention comprises: a feeder for injecting a prepolymer continuously; a transverse reactor connected to the feeder via a first connector to receive the prepolymer from the feeder and to perform solid-state polymerization, the reactor itself rotating; and a chamber connected to the transverse reactor via a second connector to receive a polymer, which has been discharged from the transverse reactor, and solid-state polymerization of which has been completed, and to discharge the polymer, wherein the transverse reactor has a demolding coating film formed on the inner wall thereof, and the feeder, the transverse reactor and the chamber are in a vacuum state. The continuous solid-state polymerization device can prevent formation of an interval, in which the prepolymer stagnates, and can perform solid-state polymerization continuously in a vacuum state without using inert gas.

公开(公告)号：US09649616B2

公开(公告)日：2017-05-16

申请号：US14899203

申请日：2013-10-22

申请人： Samsung SDI Co., Ltd.

发明人： Sang Kyun Im ,  Suk Min Jun ,  Shin Hyo Bae ,  So Young Kwon ,  Eun Ju Lee ,  Young Sub Jin ,  Kyoung Kyun Park

IPC分类号： C08F2/00 ,  B01J19/18 ,  B01J19/28 ,  C08F2/01 ,  C08G63/80 ,  C08G69/06 ,  C08G69/30 ,  B01J19/00 ,  B01F9/08 ,  B01F13/06 ,  B01F15/06 ,  B01F7/00 ,  C08G64/20

CPC分类号： B01J19/28 ,  B01F7/00466 ,  B01F9/08 ,  B01F13/06 ,  B01F15/065 ,  B01F2015/061 ,  B01F2015/062 ,  B01F2215/0431 ,  B01J19/0066 ,  B01J19/0073 ,  B01J19/18 ,  B01J2219/00094 ,  B01J2219/00159 ,  B01J2219/00162 ,  B01J2219/00166 ,  B01J2219/00168 ,  B01J2219/00186 ,  B01J2219/00189 ,  B01J2219/0204 ,  B01J2219/182 ,  C08F2/01 ,  C08G63/80 ,  C08G64/205 ,  C08G69/06 ,  C08G69/30 ,  Y02P20/149

摘要： The continuous solid-state polymerization device of the present invention comprises: a feeder for continuously introducing a prepolymer; a horizontal reactor which is connected via a first connecting part to the feeder and receives the prepolymer from the feeder so as to subject same to solid-state polymerization, wherein the reactor itself is rotated; a stirring device which comprises a stirring shaft rotating inside the horizontal reactor, in the direction opposite to that of the rotational axis of the horizontal reactor, and comprises stirring blades joined vertically to the stirring shaft; and a chamber which is connected via a second connecting part to the horizontal reactor and, once the solid-state polymerization has been completed, receives the resulting polymer discharged from the horizontal reactor, and, here, the feeder, the horizontal reactor and the chamber are in a vacuum state. The continuous solid-state polymerization device prevents the formation of prepolymer stagnation zones, and allows solid-state polymerization to take place continuously in the vacuum state without any inert gas.

公开(公告)号：US09567235B2

公开(公告)日：2017-02-14

申请号：US14380575

申请日：2013-02-25

申请人： Inje University Industry-Academic Cooperation Foundation

发明人： Hyuk Hyun Ryu ,  Jin Tak Jang ,  Tae Hyun Lee ,  Hee Bong Oh

IPC分类号： B01J4/00 ,  B01J19/00 ,  B01J19/02 ,  B01J19/24 ,  C01G3/00 ,  C01G3/02 ,  C01G9/00 ,  C01G9/02

CPC分类号： C01G9/02 ,  B01J4/001 ,  B01J19/0073 ,  B01J19/02 ,  B01J19/24 ,  B01J2219/00761 ,  B01J2219/025 ,  B01J2219/0254 ,  B01J2219/0263 ,  B01J2219/0277 ,  B01J2219/0281 ,  B01J2219/0295 ,  B01J2219/182 ,  B01J2219/1923 ,  B01J2219/1943 ,  C01G3/02 ,  C01P2004/03 ,  C01P2004/16 ,  C01P2004/54 ,  C01P2004/62 ,  Y02P20/149

摘要： The present invention relates to a solution reaction apparatus and solution reaction method using the same, and more particularly a solution reaction apparatus and a solution reaction method using the same, wherein a reaction vessel is made by using a sealing member, a reaction vessel forming member, and a substrate serving as the bottom part of the reaction vessel so as to cause one side of a reaction solution only to contact the solution, thereby adjusting the temperature of the substrate differently from the temperature of the solution. The solution reaction apparatus of the present invention can control temperature of the substrate and temperature of the reaction solution separately, thereby it can control the temperature of the solution above the boiling point of the solution, and can react the solution while constantly maintaining the concentration of the solution by the solution circulatory device. Accordingly, it has an effect of freely forming various nanostructures on the substrate.

摘要翻译： 本发明涉及使用该溶液反应装置和溶液反应方法的溶液反应装置，更具体地说，涉及一种溶液反应装置和使用该反应装置的溶液反应方法，其中通过使用密封构件制成反应容器，反应容器形成构件 和作为反应容器的底部的基板，使反应液的一侧仅与溶液接触，从而不同于溶液的温度调节基板的温度。 本发明的溶液反应装置可以分别控制基板的温度和反应溶液的温度，从而可以将溶液的温度控制在溶液的沸点以上，并且可以使溶液反应，同时保持反应溶液的浓度 溶液循环装置解决。 因此，其具有在基板上自由形成各种纳米结构的效果。

公开(公告)号：US09500631B2

公开(公告)日：2016-11-22

申请号：US14277845

申请日：2014-05-15

申请人： Extundo Incorporated

发明人： Clifford L. Johns ,  Daniel D. Sympson

IPC分类号： B08B9/093 ,  G01N33/00 ,  B01J8/00 ,  B01J8/06 ,  B01J19/00 ,  G01L19/08

CPC分类号： G01N33/0004 ,  B01J8/001 ,  B01J8/008 ,  B01J8/06 ,  B01J19/0073 ,  B01J2208/0007 ,  B01J2208/00539 ,  B01J2208/00584 ,  B01J2208/00654 ,  B01J2208/00769 ,  B01J2208/00805 ,  B01J2219/002 ,  B01J2219/00213 ,  B01J2219/0024 ,  G01L19/083 ,  G01L19/086

摘要： Method for calibrating a device for measuring back pressure in open-ended chemical reactor tubes, comprising the steps of: providing a device for measuring back pressure in open-ended chemical reactor tubes, including a frame member and a plurality of injector tubes mounted on the frame member with a spacing between the injector tubes; providing a test stand, comprising a frame member; a base supporting said frame member; and a plurality of calibration tubes mounted on the frame member, each of said calibration tubes having an open top and a dosed bottom, with a precision orifice in the dosed bottom to simulate the chemical reactor tubes to be tested; inserting the plurality of injector tubes into the respective calibration tubes; sealing between the injector tubes and the calibration tubes; sending gas through the injector tubes and taking a back pressure reading for each of the injector tubes; and generating correction factors for each injector tube to correct for variations in the back pressure readings.

摘要翻译： 用于校准用于测量开放式化学反应器管中的背压的装置的方法，包括以下步骤：提供用于测量开放式化学反应器管中的背压的装置，包括框架构件和安装在所述壳体上的多个注射器管 框架构件，其在注射器管之间具有间隔; 提供测试台，包括框架构件; 支撑所述框架构件的基座; 以及安装在所述框架构件上的多个校准管，每个所述校准管具有敞开的顶部和定量的底部，在所述定量的底部具有精确的孔，以模拟待测试的化学反应器管; 将多个注射器管插入相应的校准管中; 注射器管和校准管之间的密封; 通过注射管输送气体并对每个注射器管采取背压读数; 并产生每个注射管的校正因子，以校正背压读数的变化。

公开(公告)号：US20160144337A1

公开(公告)日：2016-05-26

申请号：US14899203

申请日：2013-10-22

申请人： Samsung SDI Co., Ltd..

发明人： Sang Kyun IM ,  Suk Min JUN ,  Shin Hyo BAE ,  So Young KWON ,  Eun Ju LEE ,  Young Sub JIN ,  Kyoung Kyun PARK

IPC分类号： B01J19/28 ,  C08G64/20 ,  C08G63/80 ,  C08G69/06

CPC分类号： B01J19/28 ,  B01F7/00466 ,  B01F9/08 ,  B01F13/06 ,  B01F15/065 ,  B01F2015/061 ,  B01F2015/062 ,  B01F2215/0431 ,  B01J19/0066 ,  B01J19/0073 ,  B01J19/18 ,  B01J2219/00094 ,  B01J2219/00159 ,  B01J2219/00162 ,  B01J2219/00166 ,  B01J2219/00168 ,  B01J2219/00186 ,  B01J2219/00189 ,  B01J2219/0204 ,  B01J2219/182 ,  C08F2/01 ,  C08G63/80 ,  C08G64/205 ,  C08G69/06 ,  C08G69/30 ,  Y02P20/149

摘要： The continuous solid-state polymerisation device of the present invention comprises: a feeder for continuously introducing a prepolymer; a horizontal reactor which is connected via a first connecting part to the feeder and receives the prepolymer from the feeder so as to subject same to solid-state polymerisation, wherein the reactor itself is rotated; a stirring device which comprises a stirring shaft rotating inside the horizontal reactor, in the direction opposite to that of the rotational axis of the horizontal reactor, and comprises stirring blades joined vertically to the stirring shaft; and a chamber which is connected via a second connecting part to the horizontal reactor and, once the solid-state polymerisation has been completed, receives the resulting polymer discharged from the horizontal reactor, and, here, the feeder, the horizontal reactor and the chamber are in a vacuum state. The continuous solid-state polymerisation device prevents the formation of prepolymer stagnation zones, and allows solid-state polymerisation to take place continuously in the vacuum state without any inert gas.

摘要翻译： 本发明的连续固态聚合装置包括：用于连续引入预聚物的进料器; 水平反应器，其经由第一连接部分连接到进料器并且接收来自进料器的预聚物以便同时进行固相聚合，其中反应器本身旋转; 搅拌装置，包括在水平反应器内沿与水平反应器的旋转轴线相反的方向旋转的搅拌轴，并包括垂直于搅拌轴连接的搅拌叶片; 以及经由第二连接部分连接到水平反应器的室，并且一旦固态聚合已经完成，则接收从水平反应器排出的所得聚合物，并且在这里，进料器，水平反应器和室 处于真空状态。 连续固态聚合装置防止预聚物停滞区的形成，并且允许固态聚合在真空状态下连续发生而没有任何惰性气体。

公开(公告)号：US20160030905A1

公开(公告)日：2016-02-04

申请号：US14448146

申请日：2014-07-31

申请人： UOP LLC

发明人： Michael S. Sandacz ,  Michael A. Stine ,  Mark A. La Vine ,  Melvin Paden ,  Patrick D. Walker ,  James W. Althoff

IPC分类号： B01J8/24 ,  B01J38/12

CPC分类号： B01J8/24 ,  B01J8/003 ,  B01J8/0055 ,  B01J8/008 ,  B01J8/1863 ,  B01J8/26 ,  B01J19/0073 ,  B01J2208/00495 ,  B01J2208/0084 ,  B01J2208/00867 ,  B01J2208/00884 ,  B01J2208/00911 ,  B01J2208/00938 ,  B01J2208/00991 ,  F27D99/0073

摘要： A regenerator for an FCC apparatus. The regenerator includes a riser inside of a shell. The riser includes a cone and a cone skirt. An annulus is formed between the riser and the shell. A sealing system for keeping catalyst out of a portion of the annulus comprises a first sealing element and a second sealing element disposed above the second sealing element. The second sealing element comprises a ring having one or more plates being movable to accommodate the thermal expansion of the riser.

摘要翻译： FCC设备的再生器。 再生器包括壳内的提升管。 提升器包括锥体和锥形裙部。 在提升管和壳体之间形成一个环。 用于将催化剂保持在环形空间的一部分之外的密封系统包括设置在第二密封元件上方的第一密封元件和第二密封元件。 第二密封元件包括具有一个或多个板的环可移动以适应提升管的热膨胀。

公开(公告)号：US09233354B1

公开(公告)日：2016-01-12

申请号：US14448146

申请日：2014-07-31

申请人： UOP LLC

发明人： Michael S. Sandacz ,  Michael A. Stine ,  Mark A. La Vine ,  Melvin Paden ,  Patrick D. Walker ,  James W. Althoff

IPC分类号： B01J8/08 ,  B01J19/00 ,  B01J8/24 ,  B01J38/12 ,  B01J8/00 ,  F27D99/00

CPC分类号： B01J8/24 ,  B01J8/003 ,  B01J8/0055 ,  B01J8/008 ,  B01J8/1863 ,  B01J8/26 ,  B01J19/0073 ,  B01J2208/00495 ,  B01J2208/0084 ,  B01J2208/00867 ,  B01J2208/00884 ,  B01J2208/00911 ,  B01J2208/00938 ,  B01J2208/00991 ,  F27D99/0073

摘要： A regenerator for an FCC apparatus. The regenerator includes a riser inside of a shell. The riser includes a cone and a cone skirt. An annulus is formed between the riser and the shell. A sealing system for keeping catalyst out of a portion of the annulus comprises a first sealing element and a second sealing element disposed above the second sealing element. The second sealing element comprises a ring having one or more plates being movable to accommodate the thermal expansion of the riser.

摘要翻译： FCC设备的再生器。 再生器包括壳内的提升管。 提升器包括锥体和锥形裙部。 在提升管和壳体之间形成一个环。 用于将催化剂保持在环形空间的一部分之外的密封系统包括设置在第二密封元件上方的第一密封元件和第二密封元件。 第二密封元件包括具有一个或多个板的环可移动以适应提升管的热膨胀。

公开(公告)号：US20150196887A1

公开(公告)日：2015-07-16

申请号：US14669463

申请日：2015-03-26

申请人： Honeywell International Inc.

发明人： Stephen A. Cottrell

IPC分类号： B01J19/02 ,  C07C21/185 ,  B01J19/18

CPC分类号： B01J19/02 ,  B01F7/00033 ,  B01J3/08 ,  B01J19/006 ,  B01J19/0066 ,  B01J19/0073 ,  B01J19/18 ,  B01J19/26 ,  B01J2219/00006 ,  B01J2219/0004 ,  B01J2219/00094 ,  B01J2219/00123 ,  B01J2219/00162 ,  B01J2219/0218 ,  B01J2219/0263 ,  B01J2219/0277 ,  C07C17/093 ,  C07C17/25 ,  C07C17/38 ,  C07C17/383 ,  C07C21/185 ,  Y02P20/149 ,  C07C21/18

摘要： Disclosed are a reactor and agitator useful in a high pressure process for making 1-chloro-3,3,3-trifluoropropene (1233zd) from the reaction of 1,1,1,3,3-pentachloropropane (240fa) and HF, wherein the agitator includes one or more of the following design improvements: (a) double mechanical seals with an inert barrier fluid or a single seal; (b) ceramics on the rotating faces of the seal; (c) ceramics on the static faces of seal; (d) wetted o-rings constructed of spring-energized Teflon and PTFE wedge or dynamic o-ring designs; and (e) wetted metal surfaces of the agitator constructed of a corrosion resistant alloy.

摘要翻译： 公开了用于从1,1,1,3,3-五氯丙烷（240fa）和HF的反应制备1-氯-3,3,3-三氟丙烯（1233zd）的高压法中的反应器和搅拌器，其中 搅拌器包括以下设计改进中的一个或多个：（a）具有惰性阻隔流体或单个密封件的双重机械密封; （b）密封件旋转面上的陶瓷; （c）在密封的静态面上的陶瓷; （d）由弹簧通电的Teflon和PTFE楔形或动态O形圈设计构成的润湿O型圈; 和（e）由耐腐蚀合金构成的搅拌器的润湿金属表面。

公开(公告)号：US08977114B2

公开(公告)日：2015-03-10

申请号：US13489442

申请日：2012-06-05

申请人： Norbert Ellinger ,  Josef Wiesbauer ,  Robert Ring

发明人： Norbert Ellinger ,  Josef Wiesbauer ,  Robert Ring

IPC分类号： H05B3/60 ,  B01J19/02 ,  B01J19/00 ,  B01J19/08

CPC分类号： B01J19/02 ,  B01J19/002 ,  B01J19/0073 ,  B01J19/087 ,  B01J2219/00135 ,  B01J2219/00268 ,  B01J2219/0813 ,  B01J2219/0815 ,  B01J2219/0828

摘要： A device for thermal treatment of corrosive gases includes a chamber for heating gases in which there are at least four heating elements or four groups of heating elements including an electrically conductive material, wherein each heating element or group is connected to a separately regulatable and/or controllable subsystem of an electrical energy network and can thereby be heated by direct current flow, wherein each heating element or group can be controlled or regulated with respect to at least one either identical or different value of a parameter selected from the group consisting of temperature, heating power, current, voltage and resistance, or with respect to another heating element process variable, which can be influenced by the device, and wherein at least four regulatable and/or controllable subsystems are DC-isolated from ground potential. The invention also relates to a corresponding method for the thermal treatment of corrosive gases.

摘要翻译： 用于热处理腐蚀性气体的装置包括用于加热气体的室，其中存在至少四个加热元件或包括导电材料的四组加热元件，其中每个加热元件或组连接到单独可调节的和/或 电能网络的可控子系统，并且因此可以通过直流电流加热，其中每个加热元件或组可以相对于选自温度， 加热功率，电流，电压和电阻，或者相对于可受设备影响的另一个加热元件工艺变量，并且其中至少四个可调节和/或可控子系统与地电势DC隔离。 本发明还涉及用于热处理腐蚀性气体的相应方法。