摘要:
The present disclosure provides an apparatus and method for producing a policosanol having a specific chromatographic fingerprint. The apparatus of the present disclosure has a feed tank and receiving tanks which are connected to a vacuum system. The method of the present disclosure is carried out by a high vacuum rectification process and includes: firstly, feeding a saponified crude alkanol into a melting tank in which the material is melted and then flows into the feed tank, and then injecting the material into a rectifying still using a delivery pump, followed by first rectification under vacuum condition and sequential collection of fractions at different phases from the tower top and stillage residue from the tower bottom; and after the completion of the rectification of the first batch crude product, carrying out second feeding on the basis of consistent vacuum in the feed tank and the rectifying tower.
摘要:
A method for rehabilitating coffee beans or brewed coffee, including placing a quantity of coffee solution or roasted coffee beans in a pressure-controllable environment, decreasing the pressure of the pressure-controllable environment to about 75 Torr, holding the pressure of the pressure-controllable environment at about 75 Torr for a first predetermined period of time, removing unwanted congeners, such as ethyl acetate, from the coffee solution or roasted coffee beans to yield a treated coffee, and removing treated coffee from the pressure-controllable environment.
摘要:
A vacuum device, in particular to a vacuum pump, includes a reservoir for an operating medium; an outlet connector arranged at or in the reservoir; and a selection device that selectively closes or opens the outlet connector or an outlet line, which is connected via the outlet connector to the reservoir, in dependence on whether the operating medium or water is present at the outlet connector.
摘要:
An apparatus for extracting contaminants from a contaminated material, such as contaminated soil and animal manure, includes an extraction tank having an interior, a heating element that is adapted heat the contaminated material to a temperature where contaminants in the contaminated material are released therefrom to the interior of the extraction tank, and an agitator that is adapted to agitate the contaminated material as it is being heated by the heating element. The apparatus also includes an air pump that generates a series of positive pressure air pulses at an outlet thereof and a series of negative pressure air pulses at the inlet thereof. The apparatus further includes one or more contaminant retaining mechanisms, such as a sediment holding tank, a fluid holding tank, and a gas filter. The interior of the extraction tank, the air pump, and the contaminant retaining mechanisms are connected in a closed loop air circulation system such that the contaminants that are released from the contaminated material are stored in the contaminant retaining mechanisms.
摘要:
An apparatus for removing dissolved water from a water-containing fluid and a chamber for the same apparatus. The apparatus sprays a water-containing fluid which is a hydrophobic fluid, such as industrial oil in which water is dissolved, into a chamber that maintains a high vacuum pressure of 70 Torr (abs) or lower. The apparatus can effectively remove the dissolved water using a difference in saturated vapor pressure even in a state where a to-be-recycled hydrophobic fluid is heated to a moderate temperature, at which the hydrophobic fluid does not undergo a chemical change. Specifically, the chamber has a dual structure made up of an upper chamber and a lower chamber, thereby maximizing effects of fluid discharge and water removal.
摘要:
A method for preparing a novel aromatic phosphate ester-based compound, including: (a) reacting a compound expressed by chemical formula 1 (i) and a C6-10 aryl compound substituted with hydroxy or C1-6 alkoxy, or a C6-20 arylalkyl compound substituted with hydroxy or C1-6 alkoxy (ii), which are used as reaction materials by gradually heating to the temperature levels of 90-125° C., 125-180° C., 180-210° C. and 210-240° C.; (b) separating an aromatic phosphate ester-based compound from the resultant product in step (a) under the condition of a pressure of 0.01 mmHg-50 mmHg and a temperature of 50° C.-300° C. using fractional distillation; and (c) reacting the aromatic phosphate ester-based compound separated in step (b) (i) and C1-10 alcohol or a nitrogen compound (ii) at a temperature of 10-70° C.
摘要:
This invention relates to a system and method for recycling a high-boiling-point waste photoresist stripper generated in processes of manufacturing LCDs or semiconductor devices, wherein an expensive high-boiling-point stripper solvent can be easily recycled at high yield and high-purity electronic grade. This system includes a first distillation device for removing low-boiling-point impurities, a second distillation device for recycling a stripper solvent composition while removing high-boiling-point impurities, and a third distillation device for removing trace water, thus recovering the stripper solvent composition, and further includes a fourth distillation device for additionally recycling a stripper solvent, thus additionally recovering a high-boiling-point stripper solvent, and this method includes removing low-boiling-point impurities, recycling a stripper solvent composition while removing high-boiling-point impurities, and removing trace water, thus recovering the stripper solvent composition, and further includes additionally recycling a stripper solvent.
摘要:
The present invention relates to an improved method for removing contaminants from a gaseous stream substantially comprising carbon dioxide. More specifically, the method comprises the step of subjecting the gaseous stream to an absorption step in which the absorbent is liquid carbon dioxide wherein the waste of carbon dioxide is minimized by utilizing a compressing means for generating a pressure difference between two streams in a reboiler.
摘要:
Disclosed herein is a distillation purifying system. The device has a section which creates a vacuum pressure that is transmitted throughout the system, a distillation/purification zone in which fluids to be distilled/purified are treated, and a collection zone in which the distilled/purified liquids are transferred. The device is effective for certain liquids, solutions, and the like and can be used for water treatment, petroleum processes, and bodily fluid treatment.
摘要:
A distillation purifying system including a section which creates a vacuum pressure that is transmitted throughout the system, a distillation/purification zone in which fluids to be distilled/purified are treated, and a collection zone in which the distilled/purified liquids are transferred. The system is effective for use with liquids, solutions, fluids and the like and can be used for water treatment as well as bodily fluid treatment.