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公开(公告)号：US12077635B2
公开(公告)日：2024-09-03
申请号：US17284270
申请日：2019-09-12
Applicant: SABIC GLOBAL TECHNOLOGIES B.V.
Inventor： Ignacio Vic Fernandez
CPC classification number: C08G64/14 , C08G64/307
Abstract: A method for the continuous multi-stage manufacture of an end-capped polycarbonate includes, i) preparing a monomer mixture in a monomer mixing stage by mixing a bisphenol, a diaryl carbonate and optionally a transesterification catalyst in at least one monomer mixing device, ii) preparing a carbonate oligomer in an oligomerisation stage by reacting the monomer mixture in at least one oligomerisation reactor, and iii) preparing the polycarbonate in a polymerisation stage by further reacting the carbonate oligomer of the oligomerisation stage in at least one polymerisation reactor, in which an end-capping agent different from phenol and having a single phenolic hydroxy group is added to the monomer mixture in the monomer mixing stage and/or to at least one oligomerisation reactor in the oligomerisation stage.
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公开(公告)号：US20180022918A1
公开(公告)日：2018-01-25
申请号：US15548822
申请日：2016-02-11
Applicant: SABIC GLOBAL TECHNOLOGIES B.V.
Inventor： Ignacio Vic Fernandez
IPC: C08L69/00
CPC classification number: C08L69/00 , C08G64/40 , C08L2205/025
Abstract: In an embodiment, a process for forming a quenched composition comprises mixing an unquenched melt polycarbonate and a quenched melt polycarbonate to form the quenched composition; wherein the quenched polycarbonate was formed from a first melt polymerization, wherein the first melt polymerization comprises adding a quencher to form the quenched polycarbonate, wherein the unquenched polycarbonate was formed from a second melt polymerization, wherein the unquenched melt polycarbonate comprises an active catalyst used during the second melt polymerization, and wherein the second melt polymerization is free of a quencher addition.
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3.发明授权Polycarbonate composition to produce optical quality products with high quality and good processability 有权聚碳酸酯组合物生产具有高质量和良好加工性能的光学优质产品公开(公告)号：US09390744B2
公开(公告)日：2016-07-12
申请号：US14039604
申请日：2013-09-27
Applicant: SABIC GLOBAL TECHNOLOGIES B.V.
IPC: G11B7/2534 , C08K5/103 , G11B7/253
CPC classification number: G11B7/2534 , C08K5/103 , C08K2201/014 , C08K2201/017 , G11B2007/25304 , C08L69/00
Abstract: The present disclosure relates to thermoplastic compositions, methods of making thermoplastic compositions, and articles made from thermoplastic compositions. The disclosed compositions comprise a polycarbonate polymer, a triacylglyceride release agent, and a monoacylglyceride release agent. In an embodiment, the thermoplastic composition comprises: greater than 90 weight percent based on the total weight of the composition of a melt polycarbonate polymer; a triacylglyceride release agent; and a monoacylglyceride release agent. The total amount of triacylglyceride release agent and the monoacylglyceride release agent is 0.01 to 0.5 weight percent based on the total weight of the composition.
Abstract translation: 本公开涉及热塑性组合物，制备热塑性组合物的方法和由热塑性组合物制成的制品。 所公开的组合物包含聚碳酸酯聚合物，三酰基甘油酯脱模剂和单酰基甘油酯脱模剂。 在一个实施方案中，热塑性组合物包含：基于组合物的熔体聚碳酸酯聚合物的总重量大于90重量％ 三酰基甘油酯脱模剂; 和单酰基甘油酯脱模剂。 三酰基甘油酯脱模剂和单酰基甘油酯脱模剂的总量相对于组合物的总重量为0.01〜0.5重量％。
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4.发明授权公开(公告)号：US12084542B2
公开(公告)日：2024-09-10
申请号：US17297670
申请日：2019-12-05
Applicant: SABIC Global Technologies, B.V.
Inventor： Aaron David Bojarski , Ignacio Vic Fernandez
CPC classification number: C08G64/307 , C08G64/06
Abstract: A method of preparing a polycarbonate composition in a polymerization system that includes a monomer mixing unit, an oligomerization section, and a polymerization section. The method includes melt polymerizing a dihydroxy compound with a diaryl carbonate compound in the presence of a quaternary phosphonium catalyst to produce the polycarbonate composition having a phosphorus-containing byproduct of at least one of the quaternary phosphonium catalyst or of the diaryl carbonate compound. The method further includes recycling the phosphorus-containing byproduct into the monomer mixing unit of the polymerization system and removing the polycarbonate composition from the polymerization system. The recycle stream has a phosphorus concentration of greater than or equal to 40 parts per million by weight.
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公开(公告)号：US10150855B2
公开(公告)日：2018-12-11
申请号：US15111929
申请日：2015-03-04
Applicant: SABIC GLOBAL TECHNOLOGIES B.V.
Inventor： Marco Roncaglia , Ignacio Vic Fernandez , Rein Mollerus Faber , Christianus Johannes Jacobus Maas , Cornelis Jan Maria Rijken
IPC: C08K5/103 , C08K5/11 , C08L69/00 , B29C47/68 , B29C47/00 , B29C47/06 , C08J5/18 , C08K5/3475 , C08K5/00 , C08G64/40 , B29K69/00
Abstract: In an embodiment, a method for making a thermoplastic composition, comprising: melt polymerizing a polycarbonate, extruding and melt filtering the polycarbonate to form a melt filtered polycarbonate; forming the thermoplastic composition comprising the melt filtered polycarbonate, 0.03 to 0.05 wt % of a triacylglyceride release agent; and 0.10 to 0.14 wt % of a UV stabilizer; wherein the weight percentages are based on the total weight of the composition; and extruding the thermoplastic composition.
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Patent Agency Ranking
6.发明授权公开(公告)号：US09732028B2
公开(公告)日：2017-08-15
申请号：US14206692
申请日：2014-03-12
Applicant: SABIC GLOBAL TECHNOLOGIES B.V.
Inventor： Ignacio Vic Fernandez , Mykhaylo Lyakhovych , Sergio Ferrer Nadal
IPC: B01D11/00 , C02F1/26 , C07C69/96 , C02F1/52 , B01D21/01 , B03D3/00 , C07C68/08 , C07C68/02 , C07C68/04 , C07C68/06 , C08G64/04 , C02F1/62 , C02F1/64 , C02F1/02 , C02F1/04 , B01D11/04 , C02F1/00 , C02F1/68 , B01D21/00 , B01D37/00 , C02F101/22 , C02F101/20 , C02F103/36
CPC classification number: C07C68/08 , C02F1/02 , C02F1/04 , C02F1/52 , C02F1/62 , C02F1/64 , C02F2101/20 , C02F2101/203 , C02F2101/206 , C02F2101/22 , C02F2103/36 , C07C68/02 , C07C68/04 , C07C68/06 , C07C69/96 , C08G64/04
Abstract: A process for purifying a diaryl carbonate, comprises introducing an aqueous stream to a diaryl carbonate stream that comprises a metal contaminant, wherein the aqueous stream reacts with the metal contaminant to form a precipitate; wherein introducing the aqueous stream to the diaryl carbonate stream results in introducing 100 to 10,000 ppm water based on the total composition of the diaryl carbonate stream and the aqueous stream; removing the precipitate via one or both of a separation column and a filter to result in a purified diaryl carbonate.
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公开(公告)号：US10544302B2
公开(公告)日：2020-01-28
申请号：US15553196
申请日：2016-02-25
Applicant: SABIC Global Technologies B.V.
Inventor： Helena Varela Rizo , Ignacio Vic Fernandez , David Del Agua Hernandez
Abstract: The disclosure concerns a polymer blend derived from transesterification of (i) 69.9 to 95 weight percent polycarbonate; and (ii) 4.9 to 30 weight percent liquid crystal polymer; in the presence of 0.01 to 0.1 weight percent catalyst; wherein the polymer is transparent.
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公开(公告)号：US10155845B2
公开(公告)日：2018-12-18
申请号：US15573431
申请日：2016-05-26
Applicant: SABIC GLOBAL TECHNOLOGIES B.V.
Inventor： Helena Varela Rizo , Ignacio Vic Fernandez , David Del Agua Hernandez
Abstract: The disclosure concerns a polymer derived from melt extrusion of (i) 80 to 95 wt % polycarbonate; said polycarbonate having and endcap level of 45% to 80% and a branching level of 300-5,000 m comprising the following branching structures: (ii) 4.9 to 20 wt % polymethyl methacrylate; and (iii) 0.1 to 1.5 wt % of catalyst; wherein the polymer is transparent, and wherein transesterification occurs with at least a portion of the polycarbonate and the polymethyl methacrylate during melt extrusion.
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公开(公告)号：US20170321004A1
公开(公告)日：2017-11-09
申请号：US15522858
申请日：2015-10-30
Applicant: SABIC GLOBAL TECHNOLOGIES B.V.
Inventor： Ignacio Vic Fernandez , William E. Hollar, Jr. , Donald E. Owens, III
CPC classification number: C08G64/226 , C08G64/40 , C08G64/403 , C08G64/406 , C08G64/42
Abstract: In an embodiment, a polycarbonate polymerization process comprises interfacially polymerizing a carbonate compound and dihydroxy compound in the presence of an interfacial catalyst to form a polycarbonate and adding a viscosity reducing agent and a transesterification catalyst to polycarbonate upstream of a first filter to form an adjusted polycarbonate. The first filter can be replaced with a replacement filter and the adjusted polycarbonate can be introduced to the replacement filter. The flow can be diverted to a replacement filter. The process further comprises reducing the addition rate of the viscosity reducing agent and the transesterification catalyst until the addition rate is 0 mol/hr.
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10.发明申请公开(公告)号：US20170313815A1
公开(公告)日：2017-11-02
申请号：US15520541
申请日：2015-11-19
Applicant: SABIC GLOBAL TECHNOLOGIES B.V.
Inventor： Ignacio Vic Fernandez
CPC classification number: C08G64/14 , C08G64/307 , C08G64/42
Abstract: In an embodiment, a melt polymerization process comprises melt polymerizing a carbonate compound and a dihydroxy compound in the presence of a catalyst composition to form a polycarbonate; and adding an end-capping agent comprising a mono-phenolic compound to the polycarbonate, wherein the adding of the end-capping agent comprises at least one of adding the end-capping agent just upstream of a final polymerization unit, adding the end-capping agent directly into the final polymerization unit, and adding the end-capping agent downstream of the final polymerization unit; wherein a molecular weight of the polycarbonate increases by less than 10% downstream of the final polymerization unit.
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