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    PROCESS FOR THE PREPARATION OF A POWDER COMPRISING ONE OR MORE DERIVATIVES OF GLYCINE-N,N DIACETIC ACID AND /OR ONE OR MORE DERIVATIVES OF GLUTAMINE-N,N DIACETIC ACID AND METHYLGLYCINE-N,N DIACETIC ACID TRISODIUM SALT POWDER
    1.
    发明申请
    PROCESS FOR THE PREPARATION OF A POWDER COMPRISING ONE OR MORE DERIVATIVES OF GLYCINE-N,N DIACETIC ACID AND /OR ONE OR MORE DERIVATIVES OF GLUTAMINE-N,N DIACETIC ACID AND METHYLGLYCINE-N,N DIACETIC ACID TRISODIUM SALT POWDER 审中-公开
    制备含有GLYCINE-N，N二酸和/或一种或多种谷氨酰胺-N，N二酸和甲基甘氨酸-N，N二酸三钠盐粉末的一种或多种衍生物的粉末的制备方法

    公开(公告)号：US20140155646A1

    公开(公告)日：2014-06-05

    申请号：US14090285

    申请日：2013-11-26

    Applicant: BASF SE

    Inventor： Frank Mrzena ,  Hans-Juergen Kinder ,  Michael Schoenherr ,  Gerhard Cox ,  Thomas Schmidt ,  Volker Huett

    IPC: C07C229/24

    CPC classification number: C07C229/24 ,  C07B2200/13 ,  C07C227/42 ,  C07C229/16

    Abstract: A process is proposed for the preparation of a powder comprising one or more derivatives of glycine-N,N-diacetic acid and/or one or more derivatives of glutamine-N,N-diacetic acid with a degree of crystallinity of a ≧30%, starting from an aqueous solution comprising the one or more derivatives of glycine-N,N-diacetic acid and/or the one or more derivatives of glutamine-N,N-diacetic acid in a concentration range from 20 to 60% by weight, based on the total weight of the aqueous solution, where the aqueous solution is concentrated in a first process step in an evaporator with rotating internals, which are arranged at a distance relative to the inside wall of the evaporator of ≦1% of the diameter of the evaporator, to give a crystal slurry with a solids concentration in the range from 60 to 85% by weight, based on the total weight of the crystal slurry, and where in a second process step the crystal slurry is left to ripen in a paste bunker and then in a thin-film contact dryer, and where the residence time in the paste bunker and in the thin-film contact dryer is in total a ≧15 minutes.

    Abstract translation: 提出一种制备包含一种或多种甘氨酸-N，N-二乙酸衍生物和/或一种或多种结晶度为≥30％的谷氨酰胺-N，N-二乙酸衍生物的粉末的方法， 从包含甘氨酸-N，N-二乙酸的一种或多种衍生物和/或浓度为20至60重量％的谷氨酰胺-N，N-二乙酸的一种或多种衍生物的水溶液开始， 基于水溶液的总重量，其中在具有旋转内部件的蒸发器中的第一工艺步骤中浓缩水溶液，所述蒸发器相对于蒸发器的内壁设置一定距离; 1％的直径 ，得到基于晶体浆料的总重量的固体浓度为60至85重量％的晶体浆料，并且在第二工艺步骤中，将晶体浆料在 然后在薄膜接触式干燥机中， 其中在糊状掩模和薄膜接触式干燥器中的停留时间总共为≥15分钟。

    PROCESS FOR PRODUCING COMPOSITE MATERIALS
    2.
    发明申请
    PROCESS FOR PRODUCING COMPOSITE MATERIALS 审中-公开
    生产复合材料的方法

    公开(公告)号：US20140017411A1

    公开(公告)日：2014-01-16

    申请号：US13940835

    申请日：2013-07-12

    Applicant: BASF SE

    Inventor： Arno Lange ,  Theo Smit ,  Rainer Dyllick-Brenzinger ,  Gerhard Cox ,  Oliver Gronwald ,  Judith Christine Bräuer ,  Stefan Spange ,  Tina Löschner ,  Patrick Kempe

    IPC: C09D183/04

    CPC classification number: C09D183/04 ,  C08G77/50

    Abstract: The present invention relates to a process for producing composite materials formed from a) at least one inorganic or organometallic phase; and b) at least one organic polymer phase with aromatic or heteroaromatic structural units; comprising the homo- or copolymerization of at least one monomer of the formula I in which M is a metal or semimetal; R1, R2 may be the same or different and are each an Ar—C(Ra,Rb)— radical in which Ar is as defined in claim 1, or the R1Q and R2G radicals together are a radical of the formula A in which A is an aromatic or heteroaromatic ring fused to the double bond, m is 0, 1 or 2, and the R radicals may be the same or different and are as defined in claim 1; G, Q are each O, S or NH; Q is O, S or NH; and in which q, X, Y, R1′, R2′ are each as defined in claim 1; which comprises performing the polymerization of the monomers of the general formula I thermally in the absence or substantial absence of added catalysts.

    Abstract translation: 本发明涉及由a）至少一种无机或有机金属相形成的复合材料的制造方法。 和b）至少一个具有芳族或杂芳族结构单元的有机聚合物相; 包括其中M是金属或半金属的至少一种式I的单体的均聚或共聚合; R 1，R 2可以相同或不同，并且各自为Ar-C（Ra，Rb） - 基团，其中Ar如权利要求1所定义，或者R1Q和R2G基团一起是式A的基团，其中A 是与双键稠合的芳族或杂芳族环，m是0,1或2，R基可以相同或不同，如权利要求1所定义; G，Q各自为O，S或NH; Q是O，S或NH; 并且其中q，X，Y，R 1'，R 2'各自如权利要求1所定义; 其包括在不存在或基本不存在添加的催化剂的情况下热分解通式I的单体。

    PROCESS FOR PRODUCING A COMPOSITE MATERIAL
    5.
    发明申请
    PROCESS FOR PRODUCING A COMPOSITE MATERIAL 有权
    生产复合材料的方法

    公开(公告)号：US20130345385A1

    公开(公告)日：2013-12-26

    申请号：US13926364

    申请日：2013-06-25

    Applicant: BASF SE

    Inventor： Arno Lange ,  Gerhard Cox ,  Hannes Wolf ,  Szilard Csihony

    IPC: C08G77/06

    CPC classification number: C08G77/06 ,  C08G16/0218 ,  C08G77/48

    Abstract: The present invention relates to a process for producing a composite material composed of a) at least one oxidic phase and b) an organic polymer phase. The copolymerization of at least one compound of the formula I [(ArO)mMOnRrHp]q  (I) in which M is B, Al, Ga, In, Si, Ge, Sn, P, As or Sb, Ar is phenyl or naphthyl, R is alkyl, alkenyl, cycloalkyl or aryl, where aryl is unsubstituted or may have one or more substituents, with formaldehyde or formaldehyde equivalents, in a reaction medium which is essentially anhydrous, to obtain a composite material having an arrangement of phase domains similar to those nanocomposite materials obtainable by twin polymerization, and to the use of the composite material for production of gas storage materials, rubber mixtures, low-K dielectrics and electrode materials for lithium ion batteries.

    Abstract translation: 本发明涉及一种由a）至少一个氧化相和b）有机聚合物相组成的复合材料的制造方法。 其中M为B，Al，Ga，In，Si，Ge，Sn，P，As或Sb的至少一种式I [（ArO）mMOnRrHp] q（I）的化合物的共聚合是Ar是苯基或萘基 R是烷基，链烯基，环烷基或芳基，其中芳基是未取代的或可以具有一个或多个取代基，与甲醛或甲醛当量在基本上是无水的反应介质中，以获得具有类似相位排列的复合材料 可以通过双聚合获得的那些纳米复合材料，以及用于制备气体储存材料，橡胶混合物，低K电介质和用于锂离子电池的电极材料的复合材料的使用。

    COMPOSITE MATERIALS AND PROCESS FOR PRODUCTION THEREOF
    6.
    发明申请
    COMPOSITE MATERIALS AND PROCESS FOR PRODUCTION THEREOF 审中-公开
    复合材料及其生产方法

    公开(公告)号：US20130341559A1

    公开(公告)日：2013-12-26

    申请号：US13923715

    申请日：2013-06-21

    Applicant: BASF SE

    Inventor： Arno LANGE ,  Gerhard Cox ,  Hannes Wolf ,  Szilard Csihony

    IPC: H01M4/36

    CPC classification number: H01M4/364 ,  C04B35/52 ,  C04B2235/80 ,  H01M4/13

    Abstract: A process for producing a composite material comprising a) at least one (semi)metallic phase and b) at least one organic polymer phase, comprising the copolymerization of at least one aryloxy (semi)metallate and/or aryloxy ester of a nonmetal which forms oxo acids, the nonmetal being different than carbon and nitrogen, (compound I) with at least one ketone, formaldehyde and/or formaldehyde equivalent (compound II) in the presence of at least one (semi)metal compound which is not an aryloxy (semi)metallate, (compound III), where the weight of (semi)metal in compound III is at least 5% by weight based on the weight of compound I.

    Abstract translation: 一种制备复合材料的方法，包括a）至少一种（半）金属相和b）至少一种有机聚合物相，其包含至少一种形成非金属的非金属的芳氧基（半）金属化物和/或芳氧基酯的共聚合 在至少一种不是芳氧基的（半）金属化合物的存在下，非金属与碳和氮不同，（化合物I）与至少一种酮，甲醛和/或甲醛当量（化合物II） 半）金属化合物（化合物III），其中化合物III中（半）金属的重量为至少5重量％，基于化合物I的重量。

    Nickel hexaaluminate-containing catalyst for reforming hydrocarbons in the presence of carbon dioxide
    9.
    发明授权
    Nickel hexaaluminate-containing catalyst for reforming hydrocarbons in the presence of carbon dioxide 有权
    在二氧化碳存在下重整碳氢化镍的含六铝酸盐的催化剂

    公开(公告)号：US09475037B2

    公开(公告)日：2016-10-25

    申请号：US14771888

    申请日：2014-03-06

    Applicant: BASF SE

    Inventor： Stephan Schunk ,  Ekkehard Schwab ,  Andrian Milanov ,  Guido Wasserschaff ,  Thomas Roussiere ,  Gerhard Cox ,  Bernd Hinrichsen ,  Ulrich Floerchinger

    IPC: C01B3/38 ,  C07C1/02 ,  B01J23/00 ,  B01J23/02 ,  B01J23/08 ,  B01J21/04 ,  B01J23/83 ,  B01J37/03 ,  B01J37/04 ,  B01J37/08 ,  B01J23/755 ,  B01J23/78 ,  B01J35/00 ,  B01J35/02 ,  B01J35/10 ,  B01J37/02 ,  C01B3/40

    CPC classification number: B01J23/83 ,  B01J21/04 ,  B01J23/002 ,  B01J23/02 ,  B01J23/755 ,  B01J23/78 ,  B01J35/002 ,  B01J35/006 ,  B01J35/023 ,  B01J35/1004 ,  B01J37/0236 ,  B01J37/031 ,  B01J37/036 ,  B01J37/04 ,  B01J37/08 ,  B01J37/088 ,  C01B3/40 ,  C01B2203/0227 ,  C01B2203/0805 ,  C01B2203/1058 ,  C01B2203/1082 ,  Y02E60/324

    Abstract: The invention relates to a nickel hexaaluminate-comprising catalyst for reforming hydrocarbons, preferably methane, in the presence of carbon dioxide, which comprises hexaaluminate in a proportion in the range from 65 to 95% by weight, preferably from 70 to 90% by weight, and a crystalline, oxidic secondary phase selected from the group consisting of LaAlO3, SrAl2O4 and BaAl2O4 in the range from 5 to 35% by weight, preferably from 10 to 30% by weight. The BET surface area of the catalyst is ≧5 m2/g, preferably ≧10 m2/g. The molar nickel content of the catalyst is ≦3 mol %, preferably ≦2.5 mol % and more preferably ≦2 mol %. The interlayer cations are preferably Ba and/or Sr. The process for producing the catalyst comprises the steps: (i) production of a mixture of metal salts, preferably nitrate salts of Ni and also Sr and/or La, and a nanoparticulate aluminum source, (ii) molding and (iii) calcination. The catalyst of the invention is brought into contact with hydrocarbons, preferably methane, and CO2 in a reforming process, preferably at a temperature of >800° C. The catalyst is also distinguished by structural and preferred properties of the nickel, namely that the nickel particles mostly have a tetragonal form and the particles have a size of ≦50 nm, preferably ≦40 nm and particularly preferably ≦30 nm, and are present finely dispersed as grown-on hexaaluminate particles. The catalyst has only a very low tendency for carbonaceous deposits to be formed.

    Abstract translation: 本发明涉及一种在二氧化碳存在下重整碳氢化合物（优选甲烷）的含六铝酸镍催化剂，其包含65重量％至95重量％，优选70至90重量％的六铝酸盐， 以及选自5至35重量％，优选10至30重量％范围内的LaAlO 3，SrAl 2 O 4和BaAl 2 O 4的结晶，氧化的第二相。 催化剂的BET表面积为≥5m2 / g，优选≥10m2 / g。 催化剂的摩尔镍含量为≤3mol％，优选≤2.5mol％，更优选≤2mol％。 层间阳离子优选为Ba和/或Sr.制备催化剂的方法包括以下步骤：（i）制备金属盐，优选Ni和Sr和/或La的硝酸盐以及纳米颗粒铝源的混合物 ，（ii）成型和（iii）煅烧。 本发明的催化剂在重整过程中优选与烃，优选甲烷和CO 2接触，优选在800℃以上的温度下。催化剂的特征还在于镍的结构和优选性质，即镍 颗粒大多具有四方晶格，并且颗粒的尺寸为≤50nm，优选≤40nm，特别优选≤30nm，并且作为生长六铝酸盐颗粒细分散存在。 催化剂仅形成碳沉积物的非常低的趋势。

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