公开(公告)号：US20150141253A1

公开(公告)日：2015-05-21

申请号：US14402496

申请日：2013-05-15

Applicant: BASF SE

Inventor： Robert Reinhard ,  Tiziana Chiodo ,  Bernd Wolf ,  Stefan Scherer ,  Matthias Bratz ,  Matthias Witschel ,  Trevor William Newton ,  Thomas Seitz

IPC: C07D413/04 ,  A01N43/84

CPC classification number: C07D413/04 ,  A01N43/84 ,  A01N25/12

Abstract: The present invention relates to a novel crystalline form B of 1,5-dimethyl-6-thioxo-3-(2,2,7-trifluoro-3-oxo-4-(prop-2-ynyl)-3,4-dihydro-2H-benzo[b][1,4]oxazin-6-yl)-1,3,5-triazinane-2,4-dione The invention also relates to a process for the production of this crystalline form and formulations for plant protection which contains the novel crystalline form of 1,5-dimethyl-6-thioxo-3-(2,2,7-trifluoro-3-oxo-4-(prop-2-ynyl)-3,4-dihydro-2H-benzo[b][1,4]oxazin-6-yl)-1,3,5-triazinane-2,4-dione.

Abstract translation: 本发明涉及1,5-二甲基-6-硫代-3-（2,2,7-三氟-3-氧代-4-（丙-2-炔基）-3,4-二氢 - -2,3-二氢-2H-苯并[b] [1,4]恶嗪-6-基）-1,3,5-三氮杂环戊烷-2,4-二酮本发明还涉及制备该结晶形式的方法和用于 其含有新的1,5-二甲基-6-硫代-3-（2,2,7-三氟-3-氧代-4-（丙-2-炔基）-3,4-二氢 - 2H-苯并[b] [1,4]恶嗪-6-基）-1,3,5-三氮杂环戊烷-2,4-二酮。

公开(公告)号：US09451772B2

公开(公告)日：2016-09-27

申请号：US13746868

申请日：2013-01-22

Applicant: BASF SE

Inventor： Heidi Emilia Saxell ,  Peter Erk ,  Claude Taranta ,  Thomas Kroehl ,  Gerhard Cox ,  Martin Sukopp ,  Stefan Scherer ,  Antti Ojala ,  Gautam R. Desiraju ,  Rahul Banerjee ,  Prashant M. Bhatt

IPC: A01N43/56 ,  A01N47/02

CPC classification number: A01N43/56 ,  A01N47/02 ,  A01N2300/00

Abstract: The present invention relates to a novel crystalline modification of fipronil, to a process for the preparation of the same, to pesticidal and parasiticidal mixtures and compositions comprising said crystalline modification and to their use for combating pests and parasites.

Abstract translation: 本发明涉及氟虫腈的新型结晶改性，其制备方法，涉及杀虫剂和杀虫剂混合物，以及包含所述结晶改性的组合物及其用于防治害虫和寄生虫的用途。

公开(公告)号：US09328101B2

公开(公告)日：2016-05-03

申请号：US14402496

申请日：2013-05-15

Applicant: BASF SE

Inventor： Robert Reinhard ,  Tiziana Chiodo ,  Bernd Wolf ,  Stefan Scherer ,  Matthias Bratz ,  Matthias Witschel ,  Trevor William Newton ,  Thomas Seitz

IPC: A01N43/84 ,  C07D413/04

CPC classification number: C07D413/04 ,  A01N43/84 ,  A01N25/12

Abstract: The present invention relates to a novel crystalline form B of 1,5-dimethyl-6-thioxo-3-(2,2,7-trifluoro-3-oxo-4-(prop-2-ynyl)-3,4-dihydro-2H-benzo[b][1,4]oxazin-6-yl)-1,3,5-triazinane-2,4-dione The invention also relates to a process for the production of this crystalline form and formulations for plant protection which contains the novel crystalline form of 1,5-dimethyl-6-thioxo-3-(2,2,7-trifluoro-3-oxo-4-(prop-2-ynyl)-3,4-dihydro-2H-benzo[b][1,4]oxazin-6-yl)-1,3,5-triazinane-2,4-dione.

Abstract translation: 本发明涉及1,5-二甲基-6-硫代-3-（2,2,7-三氟-3-氧代-4-（丙-2-炔基）-3,4-二氢 - -2,3-二氢-2H-苯并[b] [1,4]恶嗪-6-基）-1,3,5-三氮杂环戊烷-2,4-二酮本发明还涉及制备该结晶形式的方法和用于 其含有新的1,5-二甲基-6-硫代-3-（2,2,7-三氟-3-氧代-4-（丙-2-炔基）-3,4-二氢 - 2H-苯并[b] [1,4]恶嗪-6-基）-1,3,5-三氮杂环戊烷-2,4-二酮。

公开(公告)号：US09353095B2

公开(公告)日：2016-05-31

申请号：US14402518

申请日：2013-05-15

Applicant: BASF SE

Inventor： Robert Reinhard ,  Tiziana Chiodo ,  Bernd Wolf ,  Stefan Scherer ,  Matthias Bratz ,  Matthias Witschel ,  Trevor William Newton ,  Thomas Seitz

IPC: A01N43/84 ,  C07D413/04

CPC classification number: C07D413/04 ,  A01N43/84 ,  C07B2200/13 ,  A01N25/12 ,  A01N2300/00

Abstract: The present invention relates to a novel crystalline form A of 1,5-dimethyl-6-thioxo-3-(2,2,7-trifluoro-3-oxo-4-(prop-2-ynyl)-3,4-dihydro-2H-benzo[b][1,4]oxazin-6-yl)-1,3,5-triazinane-2,4-dione. The invention also relates to a process for the production of this crystalline form and formulations for plant protection which contains the novel crystalline form of 1,5-dimethyl-6-thioxo-3-(2,2,7-trifluoro-3-oxo-4-(prop-2-ynyl)-3,4-dihydro-2H-benzo[b][1,4]oxazin-6-yl)-1,3,5-triazinane-2,4-dione.

Abstract translation: 本发明涉及1,5-二甲基-6-硫代-3-（2,2,7-三氟-3-氧代-4-（丙-2-炔基）-3,4-二氢 - -2,3-二氢-2H-苯并[b] [1,4]恶嗪-6-基）-1,3,5-三氮杂环戊烷-2,4-二酮。 本发明还涉及生产该结晶形式的方法和用于植物保护的制剂，其含有1,5-二甲基-6-硫代-3-（2,2,7-三氟-3-氧代 -4-（丙-2-炔基）-3,4-二氢-2H-苯并[b] [1,4]恶嗪-6-基）-1,3,5-三氮杂环戊烷-2,4-二酮。

公开(公告)号：US20150099631A1

公开(公告)日：2015-04-09

申请号：US14402518

申请日：2013-05-15

Applicant: BASF SE

Inventor： Robert Reinhard ,  Tiziana Chiodo ,  Bernd Wolf ,  Stefan Scherer ,  Matthias Bratz ,  Matthias Witschel ,  Trevor William Newton ,  Thomas Seitz

IPC: C07D413/04 ,  A01N43/84

CPC classification number: C07D413/04 ,  A01N43/84 ,  C07B2200/13 ,  A01N25/12 ,  A01N2300/00

Abstract: The present invention relates to a novel crystalline form A of 1,5-dimethyl-6-thioxo-3-(2,2,7-trifluoro-3-oxo-4-(prop-2-ynyl)-3,4-dihydro-2H-benzo[b][1,4]oxazin-6-yl)-1,3,5-triazinane-2,4-dione. The invention also relates to a process for the production of this crystalline form and formulations for plant protection which contains the novel crystalline form of 1,5-dimethyl-6-thioxo-3-(2,2,7-trifluoro-3-oxo-4-(prop-2-ynyl)-3,4-dihydro-2H-benzo[b][1,4]oxazin-6-yl)-1,3,5-triazinane-2,4-dione.

Abstract translation: 本发明涉及1,5-二甲基-6-硫代-3-（2,2,7-三氟-3-氧代-4-（丙-2-炔基）-3,4-二氢 - -2,3-二氢-2H-苯并[b] [1,4]恶嗪-6-基）-1,3,5-三氮杂环戊烷-2,4-二酮。 本发明还涉及生产该结晶形式的方法和用于植物保护的制剂，其含有1,5-二甲基-6-硫代-3-（2,2,7-三氟-3-氧代 -4-（丙-2-炔基）-3,4-二氢-2H-苯并[b] [1,4]恶嗪-6-基）-1,3,5-三氮杂环戊烷-2,4-二酮。