摘要:
The present invention includes a reactor main body (4) that is formed into a tubular shape having an axis (O) as the center and accumulates a slurry (S); a gas supply line (10) for incorporating a synthesis gas (G) into the reactor main body (4), and a sparger part (5) that is disposed in a lower portion within the reactor main body (4), communicates with the gas supply line (10), and sprays the synthesis gas (G). The sparger part (5) includes a header tube (15) in which a plurality of openings are formed so as to be separated from each other in a first direction and which sprays the synthesis gas (G) from the openings, and a pair of wall surface parts that protrude from the header tube (15), on opposing sides of the plurality of openings and in a direction orthogonal to the first direction.
摘要:
Herein disclosed is a system for producing an organic, the system including at least one high shear mixing device having at least one rotor and at least one stator separated by a shear gap, wherein the shear gap is the minimum distance between the at least one rotor and the at least one stator; a pump configured for delivering a fluid stream comprising liquid medium and light gas to the at least one high shear mixing device, wherein the at least one high shear mixing device is configured to form a dispersion of the light gas in the liquid medium; and a reactor comprising at least one inlet and at least one outlet, wherein the at least one inlet of the reactor is fluidly connected to the at least one high shear mixing device, and wherein the at least one outlet is configured for extracting the organic therefrom.
摘要:
The present invention includes a reactor main body (4) that is formed into a tubular shape having an axis (O) as the center and accumulates a slurry (S); a gas supply line (10) for incorporating a synthesis gas (G) into the reactor main body (4), and a sparger part (5) that is disposed in a lower portion within the reactor main body (4), communicates with the gas supply line (10), and sprays the synthesis gas (G). The sparger part (5) includes a header tube (15) in which a plurality of openings are formed so as to be separated from each other in a first direction and which sprays the synthesis gas (G) from the openings, and a pair of wall surface parts that protrude from the header tube (15), on opposing sides of the plurality of openings and in a direction orthogonal to the first direction.
摘要:
A process for producing at least one product from at least one gaseous reactant includes feeding the gaseous reactant, as a gaseous feed or as part of a gaseous feed which is at an inlet superficial gas velocity of at least 0.5 m/s, into a vessel holding an expanded slurry bed of solid catalyst particles suspended in a suspension liquid so that the gaseous reactant can bubble upwardly through the slurry bed. The slurry bed has a catalyst loading of less than 14% by volume of degassed slurry. The gaseous reactant is allowed to react catalytically at a pressure above atmospheric pressure as the gaseous reactant bubbles upwardly through the slurry bed to produce at least one product. The product and any unreacted gaseous reactant are withdrawn from the vessel.
摘要:
A method for estimating a particulate content in a slurry of the present invention is a method for estimating a content of particulates having a predetermined particle size or less in a slurry with solid particles dispersed in hydrocarbons including a wax, the method including, based on a correlation between a visible light transmittance and a content of solid particles having the predetermined particle size or less at a temperature at which hydrocarbons including a wax are liquefied when the solid particles having the predetermined particle size or less are dispersed in the hydrocarbons, estimating a content of particulates having the predetermined particle size or less in the slurry from a visible light transmittance of a supernatant part when the slurry is left to stand at the temperature.
摘要:
A fluidized-bed reactor for carrying out a gas-phase reaction, in which a gaseous reaction mixture flows from the bottom upward through a heterogeneous particulate catalyst forming a fluidized bed and internals are arranged in the fluidized bed, wherein the internals divide the fluidized bed into a plurality of cells arranged horizontally in the fluidized-bed reactor and a plurality of cells arranged vertically in the fluidized-bed reactor, with the cells having cell walls which are permeable to gas and have openings which ensure an exchange number of the heterogeneous particulate catalyst in the vertical direction in the range from 1 to 100 liters/hour per liter of reactor volume, is proposed.
摘要:
There is provided a bubble column type hydrocarbon synthesis reactor which synthesizes a hydrocarbon compound by a chemical reaction of a synthesis gas including hydrogen and carbon monoxide as main components, and a slurry having solid catalyst particles suspended in liquid. The hydrocarbon synthesis reactor includes a reactor main body which accommodates the slurry, a synthesis gas supplying section which supplies the synthesis gas to the slurry, and an introducing portion which introduces a cooling fluid having a lower temperature than the slurry into the reactor main body.
摘要:
Method of operating a three-phase slurry reactor includes feeding at a low level at least one gaseous reactant into a vertically extending slurry body of solid particles suspended in a suspension liquid, the slurry body being contained in at least two vertically extending shafts housed within a common reactor shell, each shaft being divided into a plurality of vertically extending channels at least some of which are in slurry flow communication and the slurry body being present in at least some of the channels. The gaseous reactant is allowed to react as it passes upwardly through the slurry body present in at least some of the channels of the shafts, thereby to form a non-gaseous and/or a gaseous product. Gaseous product, if present, and/or unreacted gaseous reactant is allowed to disengage from the slurry body in a head space above the slurry body.
摘要:
The invention relates to methods for prevention of and recovery from a catalyst bed slumping in a gas-agitated multiphase hydrocarbon synthesis reactor, while the reactor is either under non-reactive conditions or under reaction promoting conditions when syngas is converted to products. The reactor contains a catalyst bed comprising catalyst particles and a gas injection zone suitable for injecting a reactor gas feed. A method for preventing bed slumping comprises supplying a supplemental gas to the gas-agitated multiphase reactor to prevent the catalyst bed from slumping due to insufficient reactor gas feed flow. The method may include recycling some or all of the supplemental gas to the reactor. The method may further comprise separating the gas injection zone from the catalyst bed with a porous plate so as to prevent migration of catalyst particles into the gas injection zone and to minimize plugging of gas distributor(s) present in said zone.
摘要:
The present invention relates to a method for gas-solid contacting in a bubbling fluidized bed reactor by: (a) introducing into a reactor with bed length to bed diameter ratio below about 5.0, a primary gas consisting essentially of reactant(s) of the reaction to be carried out in the bed of solid particles through a primary gas distributor located at the reactor bottom at a superficial gas velocity Up, which is very close or equivalent to the minimum fluidization velocity Umf, required for achieving the incipient fluidization of the solid particles in the bed to obtain an emulsion phase consisting essentially of the solid particles and the primary gas with little or no formation of gas bubbles to achieve incipient fluidization or liquid-like behaviour of fluidizable solid particles; (b) forming gas bubbles in the incipiently fluidized bed by introducing through a secondary gas distributor located immediately above the primary gas distributor a secondary gas, selected from one of the reactants which is used in excess of that required for the reaction stoichiometry, steam, an inert or a mixture of two or more thereof at a superficial gas velocity, Us, which is related to the superficial velocity of the primary gas such that a ratio of the superficial velocity of the secondary gas to the superficial velocity of the primary gas Us/Up, is in the range from about 0.5 to about 10.0, preferably from about 1 to about 5.
摘要翻译:本发明涉及通过以下步骤在鼓泡流化床反应器中气 - 固接触的方法:(a)将床长至床直径比低于约5.0引入反应器中,主要气体基本上由 在固体颗粒床上通过位于反应器底部的初级气体分布器以表面气体速度U P p P进行反应,该气体速度非常接近或等于最小流化速度U