Ring Opening Of Oxazolines At High Temperature In A Continuous Process
    10.
    发明申请
    Ring Opening Of Oxazolines At High Temperature In A Continuous Process 审中-公开
    在连续过程中高温下恶唑啉的开环

    公开(公告)号:US20160017094A1

    公开(公告)日:2016-01-21

    申请号:US14774043

    申请日:2014-03-12

    申请人: BASF SE

    IPC分类号: C08G69/00

    CPC分类号: C08G69/00 C08G73/0233

    摘要: A process for preparing a polyoxazoline includes feeding continuously an oxazoline, a solvent, and a catalyst to a continuous stirred tank reactor at a rate which provides for a residence time sufficient to achieve ring opening of the oxazoline and polymerize the oxazoline; exiting a polyoxazoline solution from the continuous stirred reactor, the polyoxazoline solution including polyoxazoline, solvent, and, optionally, unreacted oxazoline, low molecular weight oligomeric oxazoline, or a mixture thereof; removing the solvent, and, optionally, unreacted oxazoline, low molecular weight oligomeric oxazoline, or a mixture thereof from the polyoxazoline solution; and recovering the polyoxazoline.

    摘要翻译: 制备聚恶唑啉的方法包括以连续的搅拌釜反应器连续进料恶唑啉,溶剂和催化剂,其速率为提供足以实现恶唑啉的开环并使恶唑啉聚合的停留时间; 从连续搅拌反应器中排出聚恶唑啉溶液,包括聚恶唑啉,溶剂和任选未反应的恶唑啉,低分子量低聚恶唑啉或其混合物的聚恶唑啉溶液; 从所述聚恶唑啉溶液中除去溶剂和任选的未反应的恶唑啉,低分子量低聚恶唑啉或其混合物; 并回收聚恶唑啉。