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    CONTINUOUS PROCESS OF OXIDATIVE CLEAVAGE OF VEGETABLE OILS
    6.
    发明申请
    CONTINUOUS PROCESS OF OXIDATIVE CLEAVAGE OF VEGETABLE OILS 审中-公开

    公开(公告)号：US20160244394A1

    公开(公告)日：2016-08-25

    申请号：US15143838

    申请日：2016-05-02

    申请人： Novamont S.p.A.

    发明人： Arno Bieser ,  Giampietro Borsotti ,  Francesca Digioia ,  Adriano Ferrari ,  Alessandro Pirocco

    IPC分类号： C07C51/285 ,  C07C51/347

    CPC分类号： C07C51/285 ,  C07C51/09 ,  C07C51/16 ,  C07C51/245 ,  C07C51/347 ,  C07C51/353 ,  C11C1/04 ,  C07C55/02 ,  C07C55/18 ,  C07C53/126

    摘要： A continuous process for the oxidative cleavage of vegetable oils containing triglycerides of unsaturated carboxylic acids, to obtain saturated carboxylic acids, comprising feeding to a first continuous reactor a vegetable oil, an oxidizing compound and catalyst capable of catalyzing the oxidation reaction of the olefinic double bond to obtain an intermediate compound containing vicinal diols: feeding to a second continuous reactor said intermediate compound, a compound containing oxygen and a catalyst capable of catalyzing the oxidation reaction of the vicinal diols to carboxylic groups, to obtain saturated monocarboxylic acids (i) and triglycerides containing saturated carboxylic acids with more than one acid function (ii); separating the saturated monocarboxylic acids (i) from the triglycerides (ii); hydrolyzing in a third reactor the triglycerides (ii) to obtain glycerol and saturated carboxylic acids with more than one acid function; and purifying said saturated carboxylic acids by fractioned crystallization by means of wash column (melt crystallization).

    Liquid phase oxidation of aromatic feedstocks with manganate recycling to produce carboxylic acids
    8.
    发明授权
    Liquid phase oxidation of aromatic feedstocks with manganate recycling to produce carboxylic acids 有权
    芳烃原料的液相氧化与锰酸盐再循环以产生羧酸

    公开(公告)号：US09388110B2

    公开(公告)日：2016-07-12

    申请号：US14104571

    申请日：2013-12-12

    申请人： Saudi Arabian Oil Company

    发明人： Veera Venkata Ramakrishna Tammana ,  Kareemuddin M. Shaik ,  Guillaume Robert Jean-Francois Raynel

    IPC分类号： C07C227/00 ,  C07C51/295 ,  C07C51/285

    CPC分类号： C07C51/295 ,  B01J8/006 ,  B01J8/085 ,  B01J19/0046 ,  B01J2219/0059 ,  B01J2219/00599 ,  B01J2219/0072 ,  B01J2219/00759 ,  C07C51/285 ,  C07C63/06 ,  C07C63/16 ,  C07C63/24 ,  C07C63/26

    摘要： Systems and methods for liquid-phase oxidation of an aromatic feedstock containing at least one oxidizable aromatic compound may incorporate an oxidation reactor, a separation apparatus in fluidic communication with the oxidation reactor, a solids treatment unit, and a product recovery unit in fluidic communication with the separation apparatus. The oxidation reactor may conduct liquid-phase oxidation of the oxidizable aromatic compound in the aromatic feedstock in the presence of a manganate salt to form a slurry containing liquid product and solid manganese dioxide. The separation apparatus may accept the slurry from the oxidation reactor and separate the liquid component from the solid component. The solids treatment unit accepts the solid component from the separation apparatus, treats the solid component with a basic liquid to oxidize the manganese dioxide in the solid component and form a regenerated manganate salt, which may be recycled back to the oxidation reactor.

    摘要翻译： 含有至少一种可氧化芳族化合物的芳族原料的液相氧化的系统和方法可以包括氧化反应器，与氧化反应器流体连通的分离装置，固体处理单元和与 分离装置。 氧化反应器可以在锰酸盐存在下在芳族原料中进行可氧化芳族化合物的液相氧化，形成含有液体产物和固体二氧化锰的浆料。 分离装置可以接受来自氧化反应器的浆料并将液体组分与固体组分分离。 固体处理单元接受来自分离装置的固体组分，用碱性液体处理固体组分以氧化固体组分中的二氧化锰，并形成可再循环回氧化反应器的再生锰酸盐。

    Process for the preparation of a benzene derivative
    9.
    发明授权
    Process for the preparation of a benzene derivative 有权
    制备苯衍生物的方法

    公开(公告)号：US09162960B2

    公开(公告)日：2015-10-20

    申请号：US14346380

    申请日：2012-09-28

    申请人： Furanix Technologies B.V. ,  Stichting Dienst Landbouwkunding Onderzoek

    发明人： Matheus Adrianus Dam ,  Edserd de Jong ,  Jacco van Haveren ,  Aliaksei Pukin

    IPC分类号： C07C51/16 ,  C07C51/41 ,  C07C51/285 ,  C07D493/18 ,  C07C51/275 ,  C07D307/42

    CPC分类号： C07C51/41 ,  C07C51/16 ,  C07C51/275 ,  C07C51/285 ,  C07C51/412 ,  C07D307/42 ,  C07D493/18 ,  C07C65/21 ,  C07C63/307

    摘要： A substituted benzene derivative is prepared in a process, which includes reacting a furan derivative of formula (I): wherein R is an alkyl group, with an olefin of formula (II): R1—CH═CH—R2  (II) wherein R1 and R2 are the same or different and independently are selected from the group consisting of hydrogen, —CN, —CHO and —COOR3, wherein R3 is selected from hydrogen or an alkyl group, or R1 and R2 together form a —C(O)—O—(O)C— group, with the proviso that R1 and R2 are not both hydrogen, to produce a bicyclic ether; and dehydrating the bicyclic ether to obtain a benzene derivative. The benzene derivative thus obtained can suitably be converted to a benzene carboxylic acid compound by oxidation.

    摘要翻译： 在一种方法中制备取代的苯衍生物，其包括使式（I）的呋喃衍生物（其中R是烷基）与式（II）的烯烃反应：其中R 1为-CH 和R 2相同或不同且独立地选自氢，-CN，-CHO和-COOR 3，其中R 3选自氢或烷基，或者R 1和R 2一起形成-C（O） -O-（O）C-基团，条件是R1和R2不同时为氢，以产生双环醚; 并使双环醚脱水得到苯衍生物。 由此获得的苯衍生物可以通过氧化适当地转化成苯羧酸化合物。