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    Triphendioxazine compounds, processes for their preparation and their use as dyestuffs
    1.
    发明授权
    Triphendioxazine compounds, processes for their preparation and their use as dyestuffs 失效
    三苯并二恶嗪化合物，其制备方法及其作为染料的用途

    公开(公告)号：US5484458A

    公开(公告)日：1996-01-16

    申请号：US243111

    申请日：1994-05-16

    Applicant: Werner H. Russ ,  Horst Tappe ,  Christian Schumacher

    Inventor： Werner H. Russ ,  Horst Tappe ,  Christian Schumacher

    IPC: C07C317/28 ,  C09B62/44 ,  C09B62/503 ,  C09B67/22 ,  D06P3/24 ,  D06P3/66 ,  C09B62/002 ,  D06P1/38

    CPC classification number: C09B62/503 ,  C07C317/28 ,  C09B62/4403 ,  C09B67/0033 ,  Y10S8/917 ,  Y10S8/918 ,  Y10S8/924

    Abstract: Triphendioxazine compounds corresponding to the formula ##STR1## which are suitable as fiber-reactive dyestuffs for dyeing and printing material, in particular fiber material, containing hydroxy and/or carboxamide groups, such as wool and synthetic polyamide fibers, and especially cellulose fibers, such as cotton, are described. In formula (1), M is hydrogen or an alkali metal and Z is a radical of the formula (2) ##STR2## in which R is hydrogen, sulfo, alkyl having 1 to 4 carbon atoms, alkoxy having 1 to 4 carbon atoms, nitro or cyano, W is alkylene having 3 to 6 carbon atoms and the group --SO.sub.2 --Y is a fiber-reactive group of the vinyl sulfone series.

    Abstract translation: 对应于式（1）的三苯并二恶嗪化合物适合用作染色和印刷材料的纤维反应性染料，特别是含有羟基和/或羧酰胺基团的纤维材料，例如羊毛和合成聚酰胺纤维，特别是纤维素 描述了诸如棉花之类的纤维。 在式（1）中，M是氢或碱金属，Z是式（2）的基团，其中R是氢，磺基，具有1至4个碳原子的烷基，具有1至 4个碳原子，硝基或氰基，W是具有3至6个碳原子的亚烷基，基团-SO 2 -Y是乙烯基砜系列的纤维反应性基团。

    Water-soluble azo compounds, containing a diazo component with a heterocyclic moiety, and a coupling component with a fibre-reactive group, suitable as dyestuffs
    2.
    发明授权
    Water-soluble azo compounds, containing a diazo component with a heterocyclic moiety, and a coupling component with a fibre-reactive group, suitable as dyestuffs 失效
    含有杂环部分的重氮组分的水溶性偶氮化合物和与纤维反应性基团的偶合组分，适合作为染料

    公开(公告)号：US5539088A

    公开(公告)日：1996-07-23

    申请号：US382645

    申请日：1995-02-02

    Applicant: Christian Schumacher ,  Werner H. Russ

    Inventor： Christian Schumacher ,  Werner H. Russ

    IPC: C09B62/085 ,  C07D401/12 ,  C07D403/12 ,  C07D413/12 ,  C07D417/12 ,  C09B62/08 ,  C09B62/44 ,  C09B62/507 ,  C09B62/51 ,  D06P1/38 ,  C09B62/006

    CPC classification number: C07D417/12 ,  C07D401/12 ,  C07D403/12 ,  C07D413/12 ,  C09B62/08 ,  C09B62/4411 ,  C09B62/507 ,  D06P1/38

    Abstract: Water-soluble azo compounds are described which possess fiber-reactive properties and which are suitable as dyes for the dyeing of material, in particular fiber material, which contains hydroxy and/or carboxamido groups, examples being cellulosic fiber materials such as cotton, wool and nylon, and which compounds possess, as the radical of a diazo component, a radical of the formula ##STR1## in which R is hydrogen, alkyl of 1 to 4 carbon atoms, alkoxy of 1 to 4 carbon atoms, halogen or sulfo and G forms to the benzene ring the radical of a heterocycle which is free from olefinic double bonds and which contains at least one carboxamide group of the formula --CO--N(R.sup.10)-- in which R.sup.10 is hydrogen, alkyl of 1 to 4 carbon atoms or aryl of 6 to 10 carbon atoms which maybe substituted by from 1 to 3 substituents from the group consisting of sulfo, carboxy, alkoxy of 1 to 4 carbon atoms, alkyl of 1 to 4 carbon atoms, halogen, cyano, nitro and amino, and which if desired possesses 1 or 2 further hetero-groups from the series consisting of --O--, --S-- and --N(R.sup.10)-- where R.sup.10 is as defined, and which compounds contain a fiber-reactive radical which is attached to the coupling component by an amino group.

    Abstract translation: 描述了具有纤维反应性的水溶性偶氮化合物，其适合作为用于染色含有羟基和/或甲酰胺基的材料，特别是纤维材料的染料，例如纤维素纤维材料如棉，羊毛和 尼龙，并且哪些化合物具有作为重氮组分的基团的式为“IMAGE”的基团，其中R为氢，1至4个碳原子的烷基，1至4个碳原子的烷氧基，卤素或磺基，G 向苯环形成不含烯属双键的杂环基团，其含有至少一个式-CO-N（R 10） - 的羧酰胺基，其中R 10是氢，1-4个碳原子的烷基或 可以被1至3个由1至3个碳原子的磺基，羧基，烷氧基，1至4个碳原子的烷基，卤素，氰基，硝基和氨基取代的6至10个碳原子的芳基和 如果需要，其还具有1或2个更高的h 由-O - ， - S-和-N（R 10）组成的系列中的杂原子 - 其中R 10如所定义，哪些化合物含有通过氨基连接到偶联组分上的纤维反应性基团。

    Water-soluble triphendioxazine compounds and their use as dyestuffs
    4.
    发明授权
    Water-soluble triphendioxazine compounds and their use as dyestuffs 失效
    水溶性三苯并二恶嗪化合物及其作为染料的用途

    公开(公告)号：US5585489A

    公开(公告)日：1996-12-17

    申请号：US434682

    申请日：1995-05-04

    Applicant: Werner H. Russ ,  Christian Schumacher

    Inventor： Werner H. Russ ,  Christian Schumacher

    IPC: C09B62/503 ,  C07D498/04 ,  C09B62/44 ,  C09B19/00 ,  C09B62/04

    CPC classification number: C07D498/04 ,  C09B62/4405

    Abstract: Triphendioxazine compounds corresponding to the formula (1) ##STR1## in which Z is a radical of the formula (2) ##STR2## in which Y.sup.1 and Y.sup.2 each vinyl .beta.-hydroxyethyl or an ethyl radical which contains a substituent which can be eliminated under alkaline conditions in the .beta.-position, and in which Y.sup.1 and Y.sup.2 are not simultaneously .beta.-hydroxyethyl, W.sup.1 and W.sup.2 are both allyene having 2 to 6 carbon atoms, A is a covalent bond of a group of the formula --B.sup.1 --N(R.sup.3)--, in which R.sup.3 has one of the meanings of R.sup.1 and B.sup.1 is an aliphatic or aromatic bridge member, and in which the group--N(R.sup.1) --B.sup.1 --N(R.sup.3)-- can also be in total a bivalent saturated heterocyclic radical, and Z.sup.0 is hydrogen or a group of the formula (4) ##STR3## in which A.sup.0 is a covalent bond or a radical or the formula --N(R.sup.4)--B.sup.2 -- having the meaning corresponding to the above formula --B.sup.1 (NR.sup.3)-- are described. The triphendioxazine compounds of the formula (1) are used as fiber-reactive dyestuffs for dyeing material containing hydroxy, amino and/or carboxamide groups.

    Abstract translation: 对应于式（1）的三苯并二恶嗪化合物其中Z是式（2）的基团，其中Y1和Y2各自是乙烯基的β-羟乙基或乙基，其含有 取代基，其可以在碱性条件下在β-位上被去除，并且其中Y1和Y2不同时是β-羟乙基，W1和W2都是具有2至6个碳原子的烯丙烯，A是一组的共价键 式（B-N（R 3） - ）其中R 3具有R 1和R 1之一的含义是脂族或芳族桥连，其中-N（R 1）-B 1 -N（R 3） - 基团也可以 总共为二价饱和杂环基，Z 0为氢或式（4）的基团（4）其中A0为共价键或基团，或式-N（R4）-B2-具有 描述对应于上述式-B1（NR3）的含义。 式（1）的三苯并二恶嗪化合物用作用于含有羟基，氨基和/或羧酰胺基团的染色材料的纤维反应性染料。

    Individual temperature-control of aircraft cabin regions by heating and evaporative cooling
    6.
    发明授权
    Individual temperature-control of aircraft cabin regions by heating and evaporative cooling 有权
    通过加热和蒸发冷却对飞机机舱区域进行个别温度控制

    公开(公告)号：US09540111B2

    公开(公告)日：2017-01-10

    申请号：US12812831

    申请日：2009-01-12

    Applicant: Jan Dittmar ,  Christian Schumacher

    Inventor： Jan Dittmar ,  Christian Schumacher

    IPC: F25D17/06 ,  B64D13/06 ,  B64D11/06

    CPC classification number: B64D13/06 ,  B64D11/0626 ,  B64D2013/0662 ,  B64D2013/0674 ,  Y02T50/44 ,  Y02T50/46 ,  Y02T50/56

    Abstract: An air conditioning system for an aircraft for the individual air conditioning of regions of a cabin of an aircraft includes a central air conditioning device, which provides a pressurized and temperature-controlled central air flow. A part of the central air flow is supplied to a first cabin region. Another part of the central air flow is heated in a heating device or cooled in a cooling device and supplied to another cabin region. Water evaporates in the cooling device, in order to cool the air flow to be supplied to the cabin region.

    Abstract translation: 用于飞行器机舱区域的各个空调的飞机的空调系统包括中央空调装置，其提供加压和温度控制的中央空气流。 中央空气流的一部分被供应到第一舱区域。 中央空气流的另一部分在加热装置中加热或在冷却装置中冷却并供应到另一个舱区。 水在冷却装置中蒸发，以便冷却要供应到舱区的空气流。

    Dye mixture comprising water-soluble fiber-reactive azo dyes, preparation thereof and use thereof
    9.
    发明授权
    Dye mixture comprising water-soluble fiber-reactive azo dyes, preparation thereof and use thereof 失效
    包含水溶性纤维反应性偶氮染料的染料混合物，其制备及其用途

    公开(公告)号：US6136045A

    公开(公告)日：2000-10-24

    申请号：US372123

    申请日：1999-08-11

    Applicant: Ronald P. Pedemonte ,  Werner Russ ,  Joachim Steckelberg ,  Christian Schumacher

    Inventor： Ronald P. Pedemonte ,  Werner Russ ,  Joachim Steckelberg ,  Christian Schumacher

    IPC: C09B62/51 ,  C09B62/44 ,  C09B67/22 ,  D06P1/38 ,  D06P3/04 ,  D06P3/10 ,  D06P3/58 ,  D06P3/66 ,  C09B67/24 ,  D06P1/382 ,  D06P1/384

    CPC classification number: C09B62/4413 ,  C09B67/0052 ,  D06P1/38 ,  Y10S8/918

    Abstract: The present invention relates to dye mixtures comprising one or more azo dyes of the general formula (1) and one or more azo dyes of the general formula (2) ##STR1## where p is 1 or 2,R.sub.1, R.sup.1' and R.sup.2 are independently hydrogen or a group of the general formula SO.sub.3 M or OCH.sub.3,R.sup.5 and R.sup.6 are independently hydrogen or C.sub.1 -C.sub.4 alkyl,X.sup.1 and X.sup.2 are independently fluorine or chlorine or a grouping of the general formula NR.sup.3 R.sup.4 or OR.sup.3,R.sup.3 is hydrogen, C.sub.1 -C.sub.4 alkyl or optionally substituted aryl,R.sup.4 has one of the meanings of R.sup.3 or is aryl or alkyl (which may be substituted by SO.sub.2 Y, SO.sub.3 M or OCH.sub.3), optionally substituted morpholino or pyrimidino or NHCN,Y, Y.sup.1 and Y.sup.2 are independently vinyl or a grouping of the general formula CH.sub.2 CH.sub.2 Z,Z is a grouping which can be eliminated by the action of alkali, andM is a hydrogen atom, an ammonium ion or the equivalent of an alkali or alkaline earth metal,their preparation and their use for dyeing or printing hydroxyl- and/or carboxamido-containing material.

    Abstract translation: 本发明涉及包含一种或多种通式（1）的偶氮染料和一种或多种通式（2）的偶氮染料的染料混合物，其中p为1或2，R 1，R 1'和R 2独立地为氢或 通式为SO 3 M或OCH 3，R 5和R 6的基团独立地为氢或C 1 -C 4烷基，X 1和X 2独立地为氟或氯或通式为NR 3 R 4或OR 3的基团，R 3为氢，C 1 -C 4烷基或 任选取代的芳基，R 4具有R 3的含义之一，或者是芳基或烷基（其可以被SO 2 Y，SO 3 M或OCH 3取代），任选取代的吗啉代或嘧啶基或NHCN，Y，Y 1和Y 2分别是乙烯基或 通式为CH 2 CH 2 Z，Z为可通过碱作用而除去的基团，M为氢原子，铵离子或碱金属或碱土金属当量，它们的制备及其用于染色或印刷羟基的用途 - 和/或含甲酰氨基的材料。

    Process for the preparation of triphendioxazine dyestuffs amidated on both sides
    10.
    发明授权
    Process for the preparation of triphendioxazine dyestuffs amidated on both sides 失效
    制备三苯并二恶嗪染料的方法在两侧酰胺化

    公开(公告)号：US5696258A

    公开(公告)日：1997-12-09

    申请号：US744422

    申请日：1996-11-08

    Applicant: Christian Schumacher ,  Karl-Josef Herd

    Inventor： Christian Schumacher ,  Karl-Josef Herd

    IPC: C07D498/04 ,  C09B19/02 ,  C09B62/002 ,  C09B62/04 ,  C09B62/503

    CPC classification number: C07D498/04 ,  C09B19/02 ,  C09B62/0025

    Abstract: According to the invention, a process for the preparation of triphendioxazines symmetrically or asymmetrically amidated on both sides comprises reducing a triphendioxazine chromophore, which is optionally already amidated on one side, to give the leuco form and amidating and re-oxidizing the leuco form. Products amidated on both sides are obtained in this manner with a high yield and product quality. Novel triphendioxazine dyestuffs are furthermore prepared in this manner.

    Abstract translation: 根据本发明，制备在两侧对称或不对称酰胺化的三苯二恶嗪的方法包括减少任选在一侧已经酰胺化的三苯并二恶嗪发色团，得到无色形式并酰胺化和再氧化无色形式。 以这种方式获得两面的酰胺化产物，产率和产品质量高。 此外，以这种方式制备新型的三苯并二恶嗪染料。

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