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    Triphendioxazine compounds, processes for their preparation and their use as dyestuffs
    1.
    发明授权
    Triphendioxazine compounds, processes for their preparation and their use as dyestuffs 失效
    三苯并二恶嗪化合物，其制备方法及其作为染料的用途

    公开(公告)号：US5484458A

    公开(公告)日：1996-01-16

    申请号：US243111

    申请日：1994-05-16

    Applicant: Werner H. Russ ,  Horst Tappe ,  Christian Schumacher

    Inventor： Werner H. Russ ,  Horst Tappe ,  Christian Schumacher

    IPC: C07C317/28 ,  C09B62/44 ,  C09B62/503 ,  C09B67/22 ,  D06P3/24 ,  D06P3/66 ,  C09B62/002 ,  D06P1/38

    CPC classification number: C09B62/503 ,  C07C317/28 ,  C09B62/4403 ,  C09B67/0033 ,  Y10S8/917 ,  Y10S8/918 ,  Y10S8/924

    Abstract: Triphendioxazine compounds corresponding to the formula ##STR1## which are suitable as fiber-reactive dyestuffs for dyeing and printing material, in particular fiber material, containing hydroxy and/or carboxamide groups, such as wool and synthetic polyamide fibers, and especially cellulose fibers, such as cotton, are described. In formula (1), M is hydrogen or an alkali metal and Z is a radical of the formula (2) ##STR2## in which R is hydrogen, sulfo, alkyl having 1 to 4 carbon atoms, alkoxy having 1 to 4 carbon atoms, nitro or cyano, W is alkylene having 3 to 6 carbon atoms and the group --SO.sub.2 --Y is a fiber-reactive group of the vinyl sulfone series.

    Abstract translation: 对应于式（1）的三苯并二恶嗪化合物适合用作染色和印刷材料的纤维反应性染料，特别是含有羟基和/或羧酰胺基团的纤维材料，例如羊毛和合成聚酰胺纤维，特别是纤维素 描述了诸如棉花之类的纤维。 在式（1）中，M是氢或碱金属，Z是式（2）的基团，其中R是氢，磺基，具有1至4个碳原子的烷基，具有1至 4个碳原子，硝基或氰基，W是具有3至6个碳原子的亚烷基，基团-SO 2 -Y是乙烯基砜系列的纤维反应性基团。

    2,4-Diaminophenyl tetrahydrofurfuryl ethers, processes for their preparation and tinting compositions, which contain them for keratinic fibres
    2.
    发明授权
    2,4-Diaminophenyl tetrahydrofurfuryl ethers, processes for their preparation and tinting compositions, which contain them for keratinic fibres 失效
    2,4-二氨基苯基四氢糠醚，它们的制备方法和着色组合物，其含有角蛋白纤维

    公开(公告)号：US4857070A

    公开(公告)日：1989-08-15

    申请号：US154495

    申请日：1988-02-08

    Applicant: Winfried Seidel ,  Horst Tappe

    Inventor： Winfried Seidel ,  Horst Tappe

    IPC: A61K8/00 ,  A61K8/49 ,  A61Q5/10 ,  C07D307/12 ,  C09B53/00 ,  D06P1/32 ,  D06P3/08

    CPC classification number: D06P1/32 ,  A61K8/4973 ,  A61Q5/10 ,  C07D307/12

    Abstract: The invention relates to new 2,4-diaminophenyl tetrahydrofurfuryl ethers of the general formula VIII and to their salts with inorganic or organic acids ##STR1## in which R.sub.1, R.sub.2, R.sub.3 and R.sub.4, independently of one another, each represent a hydrogen atom, a (C.sub.1 -C.sub.4)alkyl group, hydroxy(C.sub.2 -C.sub.4)alkyl group, dihydroxy(C.sub.3 -C.sub.4)alkyl group, halogeno(C.sub.2 -C.sub.4)alkyl group, amino(C.sub.2 -C.sub.4)alkyl group or an amino(C.sub.2 -C.sub.4)alkyl group which is substituted once or twice by methyl, ethyl or hydroxyethyl radicals on the nitrogen, the carbon chain having a straight or branched arrangement, and it being a proviso that at least one of R.sub.1, R.sub.2, R.sub.3 and R.sub.4 represents a hydrogen atom, to processes for their preparation, and to aqueous tinting compositions for keratin fibres such as fur and human hair, containing at least one coupler and at least one developing component together with customary additives and auxiliaries, the coupler corresponding to the general formula VIII or to the acid salts of these compounds.

    Abstract translation: 本发明涉及通式VIII的新的2,4-二氨基苯基四氢糠基醚及其与无机或有机酸（VIII）的盐，其中R 1，R 2，R 3和R 4彼此独立地表示 氢原子，（C1-C4）烷基，羟基（C2-C4）烷基，二羟基（C3-C4）烷基，卤代（C2-C4）烷基，氨基（C2-C4）烷基或氨基 （C 2 -C 4）烷基，其被氮上的甲基，乙基或羟乙基取代一次或两次，所述碳链具有直链或支链排列，条件是R1，R2，R3和 R4代表氢原子，其制备方法，以及含有至少一种偶联剂和至少一种显影组分以及常规添加剂和助剂的角蛋白纤维如毛皮和人发的水性着色组合物，所述成色剂对应于 通式VIII或这些化合物的酸式盐。

    Process for the production of resist effects on polyester/cellulose mixed fiber textiles
    5.
    发明授权
    Process for the production of resist effects on polyester/cellulose mixed fiber textiles 失效
    生产聚酯/纤维素混纺纤维织物的抗皱效果的方法

    公开(公告)号：US4265629A

    公开(公告)日：1981-05-05

    申请号：US105204

    申请日：1979-12-19

    Applicant: Joachim Ribka ,  Horst Tappe ,  Kurt Roth ,  Hans-Jurgen Weyer

    Inventor： Joachim Ribka ,  Horst Tappe ,  Kurt Roth ,  Hans-Jurgen Weyer

    IPC: D06P5/12 ,  D06P5/15

    CPC classification number: D06P5/15 ,  D06P5/12

    Abstract: In the process for production of resist effects on textile materials of mixed fibers of polyester and cellulose comprising impregnating the materials with a dye liquor containing disperse dyestuffs and reactive dyestuffs which react with the resisting agents, drying or partially drying the padded materials and subsequently printing a resist paste on the material, and heat-treating the materials the improvement comprises the dischargeable disperse dyestuffs being of a class of dyestuffs of which an exemplary species is ##STR1## one of the tautomeric forms of a class of dyestuffs of which an exemplary species is ##STR2## or disperse dyestuffs which are free from groups conferring solubility in water and which contain at least two carboxylic acid ester moieties.

    Abstract translation: 在对聚酯和纤维素的混合纤维的纺织材料的抗蚀剂效果的生产过程中，包括用含有分散染料的染液和与抗蚀剂反应的活性染料浸渍材料，干燥或部分干燥填充材料并随后印刷 在材料上抵抗糊料，并且对材料进行热处理，改进包括可排放的分散染料是一类染料，其示例性物质是一类染料的互变异构体之一，其示例性物质是 或分散不含赋予在水中溶解度且含有至少两个羧酸酯部分的基团的染料。

    3-Formyl-pyridines and process for making them
    6.
    发明授权
    3-Formyl-pyridines and process for making them 失效
    3-甲酰基吡啶类及其制备方法

    公开(公告)号：US4157446A

    公开(公告)日：1979-06-05

    申请号：US819756

    申请日：1977-07-29

    Applicant: Horst Tappe

    Inventor： Horst Tappe

    IPC: C07D213/69 ,  C07D213/71 ,  C07D213/76

    CPC classification number: C07D213/69 ,  C07D213/71

    Abstract: A .beta.,.beta.,.beta.-trihalo-.alpha.-hydroxyethyl (e.g. --CHOH--CCl.sub.3) group is introduced into a 2,6-dihydroxy pyridine. The 3-formyl-4-methyl-2,6-dihydroxy pyridine produced by splitting off haloform from the trihalohydroxyethyl product, is a desirable intermediate for the making of dyes and other products, and the alkali metal or alkaline earth metal salts of the formyl compound are more stable forms of this intermediate.

    Abstract translation: 将β，β，β-三卤-α-羟乙基（例如-CHOH-CCl 3）基团引入2,6-二羟基吡啶中。 通过从三卤羟乙基产物中分离卤代衍生的3-甲酰基-4-甲基-2,6-二羟基吡啶是制备染料和其它产物的理想中间体，以及甲酰基的碱金属或碱土金属盐 化合物是该中间体的更稳定的形式。

    Mixtures of blue mono-azo disperse dyestuffs and their use for dyeing polyester
    7.
    再颁专利
    Mixtures of blue mono-azo disperse dyestuffs and their use for dyeing polyester 失效

    公开(公告)号：USRE33908E

    公开(公告)日：1992-05-05

    申请号：US658720

    申请日：1991-02-19

    Applicant: Horst Tappe ,  Hubert Kruse ,  Reinhard Kuhn ,  Albert Bode ,  Margareta Boos

    Inventor： Horst Tappe ,  Hubert Kruse ,  Reinhard Kuhn ,  Albert Bode ,  Margareta Boos

    IPC: C09B29/01 ,  C09B29/085 ,  C09B67/22 ,  D06P1/18

    CPC classification number: C09B67/0051 ,  C09B29/0003 ,  Y10S8/921 ,  Y10S8/922 ,  Y10S8/924

    Abstract: Synthetic fiber materials are effectively colored by dyeing or printing with a dyestuff mixture containing at least two separate dyestuffs (I) and (II) in a weight ratio of (I):(II) of from (20 to 99):(80 to 1) wherein:(I) is at least one dyestuff of the formula ##STR1## and (II) is at least one dyestuff of the formula ##STR2## in which X and Y are the same or different and each is independently chloro and bromo:R.sup.1 and R.sup.2 are the same or different and each independently denotes hydrogen, alkoxy having 1 to 4 carbon atoms, alkenyl having 3 or 4 carbon atoms, cyclohexyl, benzyl, chlorobenzyl, bromobenzyl, nitrobenzyl, cyanobenzyl, alkylbenzyl having 1 to 4 carbon atoms in the alkyl moiety, alkoxybenzyl having 1 to 4 alkoxy carbon atoms, alkyl having 1 to 11 carbon atoms, alkyl having 1 to 11 carbon atoms interrupted by 1 to 3 oxygen atoms or substituted alkyl having 1 to 11 carbon atoms wherein the substituent is one selected from the group consisting of chloro, bromo, cyano, phenyl, phenoxy, hydroxy, (C.sub.1 -to-C.sub.4 -alkyl)-carbonyloxy, (C.sub.1 -to-C.sub.4 -alkoxy)-carbonyl, phenylcarbonyloxy, (C.sub.3 -to-C.sub.5 -alkenyloxy)-carbonyloxy, (C.sub.1 -to-C.sub.4 -alkoxy)-carbonyloxy, phenoxycarbonyloxy, tetrahydrofurfuryl, (C.sub.1 -to-C.sub.4 -alkyl)-tetrahydrofurfuryl, tetrahydropyronyl and (C.sub.1 -to-C.sub.4 -alkyl)-tetrahydropyronyl;R.sup.3 and R.sup.4 are the same or different and each is independently methyl, ethyl, n-propyl or i-propyl;R.sup.5 and R.sup.6 are the same or different and each is independently one of the definitions of R.sup.1 and R.sup.2 excepting hydrogen.

    Water soluble naphthylazopyrazolone dyestuffs having fiber-reactive groups of the vinylsulfone series
    8.
    发明授权
    Water soluble naphthylazopyrazolone dyestuffs having fiber-reactive groups of the vinylsulfone series 失效
    具有乙烯基砜系列纤维反应性基团的水溶性萘基吡唑啉酮染料

    公开(公告)号：US4963661A

    公开(公告)日：1990-10-16

    申请号：US198136

    申请日：1988-05-24

    Applicant: Horst Tappe ,  Dieter Oehme ,  Ludwig Schlafer ,  Werner H. Russ

    Inventor： Horst Tappe ,  Dieter Oehme ,  Ludwig Schlafer ,  Werner H. Russ

    IPC: D06P1/384 ,  C09B62/51

    CPC classification number: C09B62/51

    Abstract: Water-soluble monoazo compounds according to the general formula (1) below having valuable fiber-reactive dyestuff properties which dye carboxamido- and/or hydroxy-containing materials, in particular cellulose fibers, in fast yellow to orange hues. ##STR1## in which the symbols denote: M is hydrogen or an alkali metal,R.sup.1 is hydrogen, methyl, ethyl, methoxy, ethoxy, chlorine, bromine, carboxy or sulfo,R.sup.2 is hydrogen, methyl, ethyl, methoxy, ethoxy, chlorine, or bromine,R is carboxy or lower carbalkoxy,n is the number zero or 1,X and Y independently of each other are each .beta.-thiosulfatoethyl or .beta.-sulfatoethyl or vinyl, however, in the case of X and/or Y being equal to vinyl the index n must be 1.

    Abstract translation: 根据下述通式（1）的水溶性单偶氮化合物具有有价值的纤维反应性染料性质，它以快速的黄色至橙色的色调染色甲酰氨基和/或羟基的材料，特别是纤维素纤维。 其中符号表示：M为氢或碱金属，R1为氢，甲基，乙基，甲氧基，乙氧基，氯，溴，羧基或磺基，R2为氢，甲基，乙基，甲氧基， 乙氧基，氯或溴，R是羧基或低级烷氧羰基，n是数字0或1，X和Y彼此独立地各自是β-硫代硫代乙基或β-磺基乙基或乙烯基，然而，在X和/ 或Y等于乙烯基，索引n必须为1。

    Mixtures of blue mono-azo disperse dyestuffs and their use for dyeing polyester
    9.
    发明授权
    Mixtures of blue mono-azo disperse dyestuffs and their use for dyeing polyester 失效
    蓝色单偶氮分散染料的混合物及其用于染色聚酯的用途

    公开(公告)号：US4678476A

    公开(公告)日：1987-07-07

    申请号：US911746

    申请日：1986-09-26

    Applicant: Horst Tappe ,  Hubert Kruse ,  Reinhard Kuhn ,  Albert Bode ,  Margareta Boos

    Inventor： Horst Tappe ,  Hubert Kruse ,  Reinhard Kuhn ,  Albert Bode ,  Margareta Boos

    IPC: C09B29/01 ,  C09B29/085 ,  C09B67/22 ,  D06P1/18 ,  C09B29/00 ,  D06P1/04

    CPC classification number: C09B67/0051 ,  C09B29/0003 ,  Y10S8/921 ,  Y10S8/922 ,  Y10S8/924

    Abstract: Synthetic fiber materials are effectively colored by dyeing or printing with a dyestuff mixture containing at least two separate dyestuffs (I) and (II) in a weight ratio of (I):(II) of from (20 to 99):(80 to 1) wherein:(I) is at least one dyestuff of the formula ##STR1## and (II) is at least one dyestuff of the formula ##STR2## in which X and Y are the same or different and each is independently chloro and bromo:R.sup.1 and R.sup.2 are the same or different and each independently denotes hydrogen, alkoxy having 1 to 4 carbon atoms, alkenyl having 3 or 4 carbon atoms, cyclohexyl, benzyl, chlorobenzyl, bromobenzyl, nitrobenzyl, cyanobenzyl, alkylbenzyl having 1 to 4 carbon atoms in the alkyl moiety, alkoxybenzyl having 1 to 4 alkoxy carbon atoms, alkyl having 1 to 11 carbon atoms, alkyl having 1 to 11 carbon atoms interrupted by 1 to 3 oxygen atoms or substituted alkyl having 1 to 11 carbon atoms wherein the substituent is one selected from the group consisting of chloro, bromo, cyano, phenyl, phenoxy, hydroxy, (C.sub.1 -to-C.sub.4 -alkyl)-carbonyloxy, (C.sub.1 -to-C.sub.4 -alkoxy)-carbonyl, phenylcarbonyloxy, (C.sub.3 -to-C.sub.5 -alkenyloxy)-carbonyloxy, (C.sub.1 -to-C.sub.4 -alkoxy)-carbonyloxy, phenoxycarbonyloxy, tetrahydrofurfuryl, (C.sub.1 -to-C.sub.4 -alkyl)-tetrahydrofurfuryl, tetrahydrophyronyl and (C.sub.1 -to-C.sub.4 -alkyl)-tetrahydropyronyl;R.sup.3 and R.sup.4 are the same or different and each is independently methyl, ethyl, n-propyl or i-propyl;R.sup.5 and R.sup.6 are the same or different and each is independently one of the definitions of R.sup.1 and R.sup.2 excepting hydrogen.

    Abstract translation: 合成纤维材料通过用含有至少两种分开的染料（I）和（II）的染料混合物以（20〜99）:( 80〜（80〜 1）其中：（I）是至少一种式IMA的染料，（II）是至少一种式“IMAGE”的染料，其中X和Y相同或不同，并且各自独立地是氯和溴 ：R1和R2相同或不同，各自独立地表示氢，具有1-4个碳原子的烷氧基，具有3或4个碳原子的链烯基，环己基，苄基，氯苄基，溴苄基，硝基苄基，氰基苄基，具有1-4个碳原子的烷基苄基 在烷基部分中，具有1-4个烷氧基碳原子的烷氧基苄基，具有1至11个碳原子的烷基，具有1至3个碳原子的1至11个碳原子的烷基或被取代的具有1至11个碳原子的烷基，其中取代基是1 选自氯，溴，氰基，苯基，杂环基 羟基，（C 1 -C 4 - 烷基） - 羰基氧基，（C 1 -C 4 - 烷氧基） - 羰基，苯基羰氧基，（C 3 -C 5 - 烯氧基） - 羰基氧基，（C 1 -C 4 - ） - 羰基氧基，苯氧基羰基氧基，四氢糠基，（C 1 -C 4 - 烷基） - 四氢糠基，四氢化芴基和（C 1 -C 4烷基） - 四氢吡喃基; R 3和R 4相同或不同，各自独立地为甲基，乙基，正丙基或异丙​​基; R 5和R 6相同或不同，并且各自独立地是除氢之外的R 1和R 2的定义之一。

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