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    Process for the preparation of triphendioxazine dyestuffs amidated on both sides, and novel triphendioxazine dyestuffs
    2.
    发明授权
    Process for the preparation of triphendioxazine dyestuffs amidated on both sides, and novel triphendioxazine dyestuffs 失效
    双面酰胺化三苯并二恶嗪染料的制备方法，新型三苯并二恶嗪染料

    公开(公告)号：US5944854A

    公开(公告)日：1999-08-31

    申请号：US893924

    申请日：1997-07-15

    Applicant: Christian Schumacher ,  Karl-Josef Herd

    Inventor： Christian Schumacher ,  Karl-Josef Herd

    IPC: C07D498/04 ,  C09B19/02 ,  C09B62/002 ,  C09B62/04 ,  C09B62/503

    CPC classification number: C07D498/04 ,  C09B19/02 ,  C09B62/0025

    Abstract: According to the invention, a process for the preparation of triphendioxazines systemetrically or asymmetrically amidated on both sides comprises reducing a triphendioxazine chromophore, which is optionally already amidated on one side, to give the leuco form end amidating and re-oxidizing the leuco form. Products amidated on both sides are obtained in this manner with a high yield and product quality. Novel triphendioxazine dyestuffs are furthermore prepared in this manner.

    Abstract translation: 根据本发明，制备在两侧系统地或不对称地酰胺化的三苯基二恶嗪的方法包括减少任选在一侧已经酰胺化的三苯并二恶嗪发色团，得到无色形式末端酰胺化和再氧化无色形式。 以这种方式获得两面的酰胺化产物，产率和产品质量高。 此外，以这种方式制备新型的三苯并二恶嗪染料。

    Monoazo reactive dyes and solutions thereof
    4.
    发明授权
    Monoazo reactive dyes and solutions thereof 失效
    单偶氮染料及其溶液

    公开(公告)号：US5516897A

    公开(公告)日：1996-05-14

    申请号：US400450

    申请日：1995-03-07

    Applicant: Brian Lamble ,  Aiden Lavery ,  John A. Taylor

    Inventor： Brian Lamble ,  Aiden Lavery ,  John A. Taylor

    IPC: C09B62/085 ,  C09B67/22 ,  C09B67/26 ,  D06P3/66 ,  C09B62/002 ,  C09B62/028 ,  D06P1/382 ,  D06P3/87

    CPC classification number: C09B62/085 ,  C09B67/0053 ,  C09B67/0073

    Abstract: A high strength aqueous solution comprising a first and second dye each of which, in the free acid form, is of Formula (1): ##STR1## wherein: R.sup.1 is NH.sub.2 or alkyl;W is H, alkyl or alkoxy;X is a labile atom or group;A is ##STR2## Y is H or alkyl; Z is an optionally substituted phenyl group; andn has a value of 1 to 3;provided that(i) the groups defined by A in the first and second dye are different to one another; and(ii) the solution contains less than 5% by weight of inorganic compounds.Also claimed are compositions and dyes of Formula (1).

    Abstract translation: 一种高强度水溶液，其包含第一和第二种染料，每种染料以游离酸形式具有式（1）：其中：R1是NH2或烷基; W是H，烷基或烷氧基; X是不稳定的原子或组; A是H或烷基; Z是任选取代的苯基; n为1〜3的值。 条件是（i）由第一和第二染料中的A定义的基团彼此不同; 和（ii）该溶液含有小于5重量％的无机化合物。 还要求的是式（1）的组合物和染料。

    Single-step printing of cellulose fibers with triphen-dioxazine reactive dyes and with sodium acetate or sodium trichloro-acetate as alkali
    6.
    发明授权
    Single-step printing of cellulose fibers with triphen-dioxazine reactive dyes and with sodium acetate or sodium trichloro-acetate as alkali 失效
    使用三聚二氧化物反应性染料和乙酸钠或三氯三乙酸酯作为碱性物质的纤维素纤维的单步打印

    公开(公告)号：US5085668A

    公开(公告)日：1992-02-04

    申请号：US602754

    申请日：1990-10-24

    Applicant: Gerhard Pelster ,  Wolfram Schidlo

    Inventor： Gerhard Pelster ,  Wolfram Schidlo

    IPC: C09B62/002 ,  D06P3/66

    CPC classification number: D06P3/66 ,  C09B62/0025 ,  Y10S8/918

    Abstract: On testing triphendioxazine reactive dyes it was found that they are unsuitable for almost all conventional single-step printing processes since they are not stable under these conditions.In the course of the development of an uncomplicated single-step printing process for these dyes, it has been found according to the invention, then, that by replacing the customary fixing alkali (NaHCO.sub.3) by stoichiometrically specific amounts of sodium acetate or sodium trichloroacetate or certain mixtures of sodium trichloroacetate and sodium acetate it is possible to fix triphendioxazine reactive dyes in full yields without change in hue. In addition, it is possible to print conventional print pastes.

    Abstract translation: 在测试三苯并二恶嗪活性染料时，发现它们不适用于几乎所有常规的单步印刷方法，因为它们在这些条件下不稳定。 在为这些染料开发不复杂的单步印刷方法的过程中，根据本发明已经发现，通过用化学计量比特定量的乙酸钠或三氯乙酸钠代替常规固定碱（NaHCO 3），或 某些三氯乙酸钠和乙酸钠的混合物可能以完全收率固定三苯并二恶嗪活性染料而不改变色调。 此外，可以打印常规的印刷浆料。

    Aminoalkoxytriphendioxazine dyestuffs useful for dyeing and printing hydroxyl- and amino-containing materials
    7.
    发明授权
    Aminoalkoxytriphendioxazine dyestuffs useful for dyeing and printing hydroxyl- and amino-containing materials 失效
    用于染色和印刷含羟基和氨基的材料的氨基烷氧基三苯并二恶嗪染料

    公开(公告)号：US4874857A

    公开(公告)日：1989-10-17

    申请号：US102460

    申请日：1987-09-29

    Applicant: Wolfgang Harms

    Inventor： Wolfgang Harms

    IPC: C09B62/004 ,  C09B19/02 ,  C09B62/002 ,  C09B62/04 ,  C09B62/12 ,  C09B62/20 ,  C09B62/503

    CPC classification number: C09B19/02 ,  C09B62/0025

    Abstract: Dyestuffs of the formula ##STR1## in which R.sub.1, R.sub.2 =H, Cl, Br, optionally substituted C.sub.1 -C.sub.4 -alkyl or C.sub.1 -C.sub.4 -alkoxy, carbonyl, aryloxy optionally substituted carboxamide or acylamino,R.sub.3 =H, optionally substituted C.sub.1 -C.sub.4 -alkyl or C.sub.1 -C.sub.4 -alkoxy, Cl or Br,R.sub.4 =H or alkyl,B=an aliphatic or arylene bridge member,Z=H or fiber-reactive radical,n=0 or 1.These dyestuffs are highly suitable for dyeing and printing hydroxyl- and amides-containing materials and produce red dyeings and prints having good wet- and light-fastness properties.

    Abstract translation: 式中，R 1，R 2 = H，Cl，Br，任选取代的C 1 -C 4 - 烷基或C 1 -C 4 - 烷氧基，羰基，芳氧基任选取代的酰胺或酰基氨基，R3 = H，任选取代的C1- C 1 -C 4烷基或C 1 -C 4 - 烷氧基，Cl或Br，R 4 = H或烷基，B =脂族或亚芳基桥构件，Z = H或纤维反应性基团，n = 0或1.这些染料高度适用于 染色和印刷含羟基和酰胺的材料，并产生具有良好耐湿和耐光性能的红色染色和印花。

    Triphendioxazine reactive dyestuffs
    9.
    发明授权
    Triphendioxazine reactive dyestuffs 失效
    三苯并二恶嗪活性染料

    公开(公告)号：US4591643A

    公开(公告)日：1986-05-27

    申请号：US657304

    申请日：1984-10-03

    Applicant: Horst Jager

    Inventor： Horst Jager

    IPC: C09B62/002 ,  C09B62/004 ,  C09B62/523 ,  C09B62/62 ,  D06P1/38 ,  C09B19/00 ,  C09B19/02

    CPC classification number: C09B62/0025

    Abstract: The present invention provides new triphendioxazine dyestuffs of the formula ##STR1## wherein W represents an optionally substituted sulphonamide groupZ represents a reactive group or hydrogen and the other substituents are defined as in the text of the application.The new reactive dyes are highly suitable for dyeing and/or printing hydroxyl-containing and/or amide-containing fibre materials. The dyestuffs where Z is H are intermediates in the preparation of the reactive dyestuffs.

    Abstract translation: 本发明提供了新的式（1）的三苯并二恶嗪染料，其中W表示任选取代的磺酰胺基团Z表示反应性基团或氢，其它取代基如本申请案文中所定义。 新的活性染料非常适合用于含羟基和/或酰胺的纤维材料的染色和/或印刷。 Z为H的染料是制备活性染料的中间体。

    Dyestuffs
    10.
    发明授权
    Dyestuffs 失效
    染料

    公开(公告)号：US3996221A

    公开(公告)日：1976-12-07

    申请号：US539744

    申请日：1975-01-09

    Applicant: John Lindley Leng ,  Brian Parton ,  Denis Robert Annesley Ridyard ,  John Robert Lawson

    Inventor： John Lindley Leng ,  Brian Parton ,  Denis Robert Annesley Ridyard ,  John Robert Lawson

    IPC: C09B19/02 ,  C09B62/002 ,  C09B62/04 ,  C07D265/00 ,  C07D273/00 ,  C07D295/00

    CPC classification number: C09B62/0025 ,  C09B19/02

    Abstract: Dyestuffs of the formula ##STR1## WHEREIN (R).sub.n represents n substituents R each of which may be independently halogen, lower alkyl, lower alkoxy or COOHR.sup.1 is H, optionally substituted lower alkyl, optionally substituted aryl or optionally substituted aralkyl,n is 0-3,(a+b) is 0-4,X is O, S or NR.sup.2, where R.sup.2 is H or optionally substituted lower alkyl,Y is an optionally substituted aliphatic or optionally substituted araliphatic linking group, andEach Z is independently a H or a cellulose-reactive group, and when (a+b) is O there is at least one SO.sub.3 H group as substituent on the groups R.sup.1, X or Y.The dyestuffs when both Z are H are valuable acid dyes, e.g. for wool, and when one or both Z are reactive groups the dyestuffs are valuable reactive dyestuff especially for cellulose fibers.

    Abstract translation: 下式的染料n表示n个取代基R，其各自独立地为卤素，低级烷基，低级烷氧基或COOH R 1为H，任选取代的低级烷基，任选取代的芳基或任选取代的芳烷基，N IS 0-3，（A + B）IS 0-4，X为O，S或NR2，其中R2为H或任选取代的低级烷基，Y为任选取代的脂族或任选取代的芳脂族连接基团，EACH Z独立地为 H或纤维素反应性基团，当（a + b）为O时，在基团R 1，X或Y上存在至少一个SO 3 H基团作为取代基。

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