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    Ultrafine particle enclosing fullerene and production method thereof
    1.
    发明授权
    Ultrafine particle enclosing fullerene and production method thereof 有权
    包围富勒烯的超细颗粒及其制造方法

    公开(公告)号：US5951832A

    公开(公告)日：1999-09-14

    申请号：US166799

    申请日：1998-10-06

    申请人： Shun-ichiro Tanaka ,  Bing She Xu

    发明人： Shun-ichiro Tanaka ,  Bing She Xu

    IPC分类号： B01J19/08 ,  B01J19/12 ,  C01B31/02 ,  C01B31/00

    CPC分类号： B82Y30/00 ,  B82Y40/00 ,  C01B31/0206 ,  C01B31/0213 ,  Y10S423/39 ,  Y10S423/40 ,  Y10S977/736

    摘要： After an ultrafine particle is disposed on a giant fullerene by driving the ultrafine particle using an electron beam, the ultrafine particle is enclosed in a core hollow portion of the giant fullerene, by contracting the giant fullerene with the electron beam irradiation. Or a metal ultrafine particle composed of an active metal is enclosed in the core hollow portion of the giant fullerene, by irradiating a high energy beam such as the electron beam to an amorphous carbon including the active metal to form the giant fullerene in an irradiated portion, and by contracting the giant fullerene with the irradiation of the high energy beam.

    摘要翻译： 在通过使用电子束驱动超细颗粒将超细颗粒设置在巨型富勒烯上之后，通过用电子束照射收缩巨型富勒烯，将超细颗粒封闭在巨富勒烯的芯空心部分中。 或者由活性金属构成的金属超微粒子通过将诸如电子束的高能束照射到包含活性金属的无定形碳上而被包围在巨型富勒烯的芯空心部分中，以在照射部分中形成巨富勒烯 ，并通过高能束照射来承担巨型富勒烯。

    Ultrafine particle enclosing fullerene and production method thereof
    2.
    发明授权
    Ultrafine particle enclosing fullerene and production method thereof 失效
    包围富勒烯的超细颗粒及其制造方法

    公开(公告)号：US5919429A

    公开(公告)日：1999-07-06

    申请号：US942488

    申请日：1997-10-02

    申请人： Shun-ichiro Tanaka ,  Bing She Xu

    发明人： Shun-ichiro Tanaka ,  Bing She Xu

    IPC分类号： B01J19/08 ,  B01J19/12 ,  C01B31/02 ,  C01B31/00

    CPC分类号： B82Y30/00 ,  B82Y40/00 ,  C01B31/0206 ,  C01B31/0213 ,  Y10S423/39 ,  Y10S423/40 ,  Y10S977/736

    摘要： After an ultrafine particle is disposed on a giant fullerene by driving the ultrafine particle 1 using an electron beam, the ultrafine particle is enclosed in a core hollow portion of the giant fullerene, by contracting the giant fullerene with the electron beam irradiation. Or a metal ultrafine particle composed of an active metal is enclosed in the core hollow portion of the giant fullerene, by irradiating a high energy beam such as the electron beam to an amorphous carbon under existing of the active metal to form the giant fullerene in an irradiated portion, and by contracting the giant fullerene with the irradiation of the high energy beam such as the electron beam.

    摘要翻译： 在通过使用电子束驱动超细颗粒1将超细颗粒设置在巨型富勒烯上之后，通过用电子束照射收缩巨型富勒烯，将超细颗粒封闭在巨富勒烯的芯空心部分中。 或者由活性金属构成的金属超微粒子通过将诸如电子束的高能束照射到活性金属存在下的无定形碳中而封闭在巨富勒烯的芯空心部分中，以形成巨富勒烯 照射部分，以及通过诸如电子束的高能束的照射来收缩巨型富勒烯。

    Ultrafine particles and production method thereof
    3.
    发明授权
    Ultrafine particles and production method thereof 失效
    超细颗粒及其制备方法

    公开(公告)号：US5772754A

    公开(公告)日：1998-06-30

    申请号：US598053

    申请日：1996-02-07

    申请人： Shun-ichiro Tanaka ,  Bing She Xu

    发明人： Shun-ichiro Tanaka ,  Bing She Xu

    IPC分类号： B01J19/08 ,  B22F1/00 ,  B22F9/20 ,  B22F9/30 ,  C01B13/14 ,  C01F7/02 ,  C30B28/12 ,  C30B29/16 ,  C30B1/06

    CPC分类号： B82Y30/00 ,  B22F1/0018 ,  B22F9/30 ,  C01B13/145 ,  C01F7/027 ,  B22F2202/11 ,  C01P2004/32 ,  C01P2004/62 ,  C01P2004/64

    摘要： An electron beam of more than 1.times.10.sup.19 e/cm.sup.2 .multidot.sec is irradiated to metastable metal oxide particles such as .theta.-Al.sub.2 O.sub.3 particles or the like disposed on an amorphous carbon film. A phase transformation or the like of the metastable metal oxide particles is occurred by the electron beam irradiation. Thus, stable metal oxide ultrafine particles such as an .alpha.-Al.sub.2 O.sub.3 ultrafine particle 2 whose diameter is more tiny than the metastable metal oxide particles used, and a metal ultrafine particle composed of an oxide such as Al ultrafine particles are produced.

    摘要翻译： 将大于1×10 19 e / cm 2·sec的电子束照射到设置在无定形碳膜上的亚稳态金属氧化物颗粒如θ-Al 2 O 3颗粒等。 通过电子束照射发生亚稳态金属氧化物颗粒的相变等。 因此，制造稳定的金属氧化物超细颗粒，例如其直径比所用的亚稳态金属氧化物颗粒更微小的α-Al 2 O 3超细颗粒2，以及由诸如Al超细颗粒的氧化物组成的金属超细颗粒。

    Ultrafine particle and production method thereof, production method of ultrafine particle bonded body, and fullerene and production method thereof
    5.
    发明授权
    Ultrafine particle and production method thereof, production method of ultrafine particle bonded body, and fullerene and production method thereof 失效
    超细颗粒及其制造方法，超细颗粒粘结体的制造方法，富勒烯及其制造方法

    公开(公告)号：US06017630A

    公开(公告)日：2000-01-25

    申请号：US861019

    申请日：1997-05-21

    申请人： Shun-ichiro Tanaka ,  BingShe Xu

    发明人： Shun-ichiro Tanaka ,  BingShe Xu

    IPC分类号： B01J19/08 ,  B01J19/12 ,  B22F1/00 ,  B22F9/02 ,  B22F9/06 ,  C01B31/02 ,  B32B5/16

    CPC分类号： B82Y30/00 ,  B01J19/081 ,  B01J19/121 ,  B01J19/122 ,  B22F1/0018 ,  B22F9/02 ,  B22F9/06 ,  B82Y40/00 ,  C01B31/0206 ,  C01B31/0213 ,  B22F2999/00 ,  Y10T428/12493 ,  Y10T428/2982 ,  Y10T428/30

    摘要： A target material having pores is disposed on a substrate. A high energy beam is irradiated to the inner walls of the pores of the target material in a slanting direction. Constituent atoms or molecules of the target material are detached from it to obtain a single or plurality of ultrafine particles separated as a unit substance. The superfine particles are formed at desired positions corresponding to the pores of the target material. Besides, by using an amorphous carbon substrate as the substrate, fullerenes such as an onion-like graphite are formed with the ultrafine particles as nucleation points. When the high energy beam is irradiated to at least two neighboring metal ultrafine particles, these metal ultrafine particles are bonded mutually. When the obtained metal ultrafine particle bonded body has a corresponding grain boundary, the high energy beam is further irradiated to lower value .SIGMA. of the corresponding grain boundary of the bonded interface. Besides, the metal ultrafine particle bonded body can also be made into a monocrystal grain or a polycrystal grain. Such a metal ultrafine particle bonded body is stable.

    摘要翻译： 具有孔的目标材料设置在基板上。 高能量束以倾斜方向照射到目标材料的孔的内壁。 将目标材料的成分原子或分子与其分离以获得作为单位物质分离的单个或多个超微粒子。 超细颗粒形成在对应于目标材料的孔的所需位置。 此外，通过使用无定形碳基板作为基板，以超细粒子为核心点形成诸如洋葱状石墨的富勒烯。 当高能束照射到至少两个相邻的金属超细颗粒时，这些金属超细颗粒相互粘合。 当所得到的金属超微粒子接合体具有相应的晶界时，将高能束进一步照射到键合界面的相应晶界的较低值SIGMA。 此外，金属超微粒子接合体也可以制成单晶粒或多晶粒。 这种金属超微粒粘结体是稳定的。

    Graphite intercalation compound
    6.
    发明授权
    Graphite intercalation compound 失效
    石墨插层化合物

    公开(公告)号：US5762898A

    公开(公告)日：1998-06-09

    申请号：US626457

    申请日：1996-04-02

    申请人： BingShe Xu ,  Shun-ichiro Tanaka

    发明人： BingShe Xu ,  Shun-ichiro Tanaka

    IPC分类号： C01B31/00 ,  C01B31/02 ,  C01B31/04 ,  B01D31/02 ,  B01D31/04 ,  B01D31/30

    CPC分类号： B82Y30/00 ,  B82Y40/00 ,  C01B31/0206 ,  C01B31/0415

    摘要： An onion-like graphite 2 is produced by irradiating an electron beam to an amorphous carbon 3 under an active aluminum nanoparticle 1. By further irradiating the electron beam to the onion-like graphite 2 to intercalate aluminum atoms constituting the aluminum nanoparticle 1 in a space between (001) plane and (002) plane of the onion-like graphite 2 having a layer structure, an intercalation compound 4 is produced. Or, after the aluminum nanoparticles were driven and disposed on the onion-like graphite by electron beam, or the like, by irradiating the electron beam to intercalate aluminum atoms in the space between the (001) plane and the (002) plane of the onion-like graphite having a layer structure, the intercalation compound is produced.

    摘要翻译： 通过向活性铝纳米颗粒1下方的无定形碳3照射电子束来制造洋葱状石墨2.通过进一步向洋葱状石墨2照射电子束，将构成铝纳米粒子1的铝原子插入空间 在具有层结构的洋葱状石墨2的（001）面和（002）面之间，形成插层化合物4。 或者，在通过电子束等将铝纳米粒子驱动并配置在洋葱状石墨上之后，通过照射电子束将铝原子插入到（001）面和（002）面之间的空间中 具有层结构的洋葱状石墨，生成插层化合物。

    Fullerene-containing structure and process for producing the same
    8.
    发明授权
    Fullerene-containing structure and process for producing the same 失效
    含富勒烯的结构及其制备方法

    公开(公告)号：US06251522B1

    公开(公告)日：2001-06-26

    申请号：US09381736

    申请日：1999-12-23

    申请人： Shun-ichiro Tanaka ,  Bingshe Xu

    发明人： Shun-ichiro Tanaka ,  Bingshe Xu

    IPC分类号： C01B3102

    CPC分类号： B82Y30/00 ,  B82Y40/00 ,  C01B32/15 ,  C01B32/152 ,  Y10S427/102 ,  Y10S977/734 ,  Y10S977/742 ,  Y10S977/843 ,  Y10T428/30

    摘要： A fullerene containing structure comprises an amorphous carbon base having a first amorphous carbon layer and a second amorphous carbon layer laminated together, and a giant fullerene formed in the neighborhood of layer interface of the amorphous carbon base straddling on both the amorphous carbon layers. A plurality of giant fullerenes generated in the neighborhood of the layer interface are connected together to form a continuum body such as a film structure (a film of giant fullerene) or the like. According to such the fullerene containing structure, a shape and a position to be formed of the giant fullerene, further a state of formation such as a connecting structure or the like can be controlled. In addition, the stable carbon base can protect the generated giant fullerene itself.

    摘要翻译： 含富勒烯的结构包括具有层叠在一起的第一无定形碳层和第二无定形碳层的无定形碳基，以及跨越无定形碳层的无定形碳基的层界面附近形成的巨富勒烯。 在层界面附近产生的多个巨富勒烯连接在一起形成连续体，例如膜结构（巨富勒烯膜）等。 根据这样的含有富勒烯的结构，可以控制由巨富勒烯形成的形状和位置，还可以控制诸如连接结构等的形成状态。 此外，稳定的碳碱可以保护产生的巨型富勒烯本身。

    Ultrafine Al particle and production method thereof
    9.
    发明授权
    Ultrafine Al particle and production method thereof 失效
    超细Al颗粒及其制备方法

    公开(公告)号：US6033783A

    公开(公告)日：2000-03-07

    申请号：US861821

    申请日：1997-05-23

    申请人： Shun-ichiro Tanaka ,  BingShe Xu

    发明人： Shun-ichiro Tanaka ,  BingShe Xu

    IPC分类号： B22F9/04 ,  B22F9/30 ,  C22C21/00 ,  C23C14/14 ,  C23C14/30 ,  C30B23/02 ,  B32B5/16

    CPC分类号： C23C14/30 ,  B22F9/30 ,  C23C14/14 ,  C30B23/002 ,  C30B29/02 ,  B22F2999/00 ,  Y10T428/30

    摘要： An ultrafine Al particle consists of an Al multiply twinned particle. The Al multiply twinned particle has a decahedron structure surrounded by {111} planes. The Al multiply twinned decahedral particle has a diameter of 10 to 30 nm. Such an ultrafine Al particle consisting of the Al multiply twinned decahedral particle is obtained as follows. A metastable Al oxide particle is placed on an amorphous carbon substrate having the reduction effect. Then the electron beam is irradiated to the metastable Al oxide particle placed on the amorphous carbon substrate in the vacuum atmosphere. From the metastable Al oxide particle, Al atoms or Al clusters are emitted and adsorbed to the substrate. By adjusting the electron beam intensity so that the ultrafine Al particle in the above procedure has a diameter from 10 to 30 nm, the Al multiply twinned particle having a decahedron is obtained.

    摘要翻译： 超细Al颗粒由Al多重孪晶颗粒组成。 Al多重孪晶颗粒具有被{111}平面包围的十面体结构。 Al多重双晶十面体粒子的直径为10〜30nm。 由Al多重双晶十面体粒子组成的这种超细Al粒子如下获得。 将亚稳态Al氧化物颗粒放置在具有还原效果的非晶碳衬底上。 然后在真空气氛中将电子束照射到放置在非晶碳基板上的亚稳态Al氧化物颗粒。 从亚稳态Al氧化物颗粒中，Al原子或Al簇被发射并吸附到衬底上。 通过调整电子束强度，使上述方法中的超细Al粒子的直径为10〜30nm，得到具有十面体的Al倍增孪晶粒子。

    Fine projection structure and fabricating method thereof
    10.
    发明授权
    Fine projection structure and fabricating method thereof 失效
    精细投影结构及其制造方法

    公开(公告)号：US6025604A

    公开(公告)日：2000-02-15

    申请号：US94031

    申请日：1998-06-09

    申请人： Yutaka Wakayama ,  Shun-ichiro Tanaka

    发明人： Yutaka Wakayama ,  Shun-ichiro Tanaka

    IPC分类号： H01L29/06 ,  H01L21/20 ,  H01L31/0328 ,  H01L31/0336 ,  H01L31/072

    CPC分类号： H01L21/02378 ,  H01L21/02381 ,  H01L21/02425 ,  H01L21/02433 ,  H01L21/02532 ,  H01L21/02645 ,  H01L21/02653

    摘要： Dispose a fine metal particle on a semiconductor substrate. By heat-treating this in a vacuum, a constituent element of the semiconductor substrate is dissolved into the fine metal particle to form a solid solution, resulting in further formation of a homogeneous liquid phase (liquid droplet) composed of semiconductor-metal. By annealing this, the constituent element of the semiconductor substrate is precipitated from the semiconductor-metal liquid droplet. Thus, a fine projection composite structure comprising a semiconductor substrate, a semiconductor fine projection epitaxially grown selectively at an arbitrary position on the semiconductor substrate, and a metal layer disposed selectively on the semiconductor fine projection, can be obtained. The metal layer can be removed as demands arise. Such a fine projection composite structure possesses applicability in, for instance, an ultra-high integration semiconductor device or a quantum size device.

    摘要翻译： 在半导体衬底上处理细金属颗粒。 通过在真空中进行热处理，将半导体衬底的构成元素溶解在金属微粒中形成固溶体，从而进一步形成由半导体金属构成的均匀的液相（液滴）。 通过退火，半导体衬底的构成元素从半导体 - 金属液滴中析出。 因此，可以获得包括半导体衬底，在半导体衬底上的任意位置选择性地外延生长的半导体精细投影和选择性地设置在半导体精细投影上的金属层的精细投影复合结构。 金属层可根据需要进行移除。 这种精细投影复合结构在例如超高集成度半导体器件或量子尺寸器件中具有适用性。