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公开(公告)号:US11313042B2
公开(公告)日:2022-04-26
申请号:US16566647
申请日:2019-09-10
Applicant: FEI Company
Inventor: Thomas G. Miller , Jason Arjavac , Michael Moriarty
IPC: H01J37/00 , C23F1/04 , H01J37/302 , G01N1/32 , H01J37/305 , H01J37/304
Abstract: A method, system, and computer-readable medium for forming transmission electron microscopy sample lamellae using a focused ion beam including directing a high energy focused ion beam toward a bulk volume of material; milling away the unwanted volume of material to produce an unfinished sample lamella with one or more exposed faces having a damage layer; characterizing the removal rate of the focused ion beam; subsequent to characterizing the removal rate, directing a low energy focused ion beam toward the unfinished sample lamella for a predetermined milling time to deliver a specified dose of ions per area from the low energy focused ion beam; and milling the unfinished sample lamella with the low energy focused ion beam to remove at least a portion of the damage layer to produce the finished sample lamella including at least a portion of the feature of interest.
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公开(公告)号:US09581526B2
公开(公告)日:2017-02-28
申请号:US15047064
申请日:2016-02-18
Applicant: FEI Company
Inventor: Jason Arjavac , Pei Zou , David James Tasker , Maximus Theodorus Otten , Gerhard Daniel
IPC: G01N1/28 , G01N1/06 , G01N1/08 , G01N23/04 , G01N1/32 , H01J37/305 , H01J37/26 , H01J37/06 , H01J37/18 , H01J37/20 , H01J37/28
CPC classification number: G01N1/28 , G01N1/06 , G01N1/08 , G01N1/32 , G01N23/04 , H01J37/06 , H01J37/18 , H01J37/20 , H01J37/26 , H01J37/28 , H01J37/3056 , H01J2237/063 , H01J2237/182 , H01J2237/204 , H01J2237/208 , H01J2237/2802 , H01J2237/31745 , H01J2237/31749
Abstract: An improved method and apparatus for S/TEM sample preparation and analysis. Preferred embodiments of the present invention provide improved methods for TEM sample creation, especially for small geometry (
Abstract translation: 一种用于S / TEM样品制备和分析的改进方法和装置。 本发明的优选实施例提供用于TEM样品制备的改进方法,特别是对于小几何(<100nm厚)TEM薄片。 本发明的优选实施例还通过提供部分或全部自动化TEM样品制作的方法来提供在诸如集成电路或半导体晶片上制造的其它结构的物体上的基于S / TEM的测量的在线方法,以使得创建过程 并分析TEM样品减少劳动密集度,并提高TEM分析的产量和再现性。
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公开(公告)号:US09275831B2
公开(公告)日:2016-03-01
申请号:US14546244
申请日:2014-11-18
Applicant: FEI Company
Inventor: Jason Arjavac , Pei Zou , David James Tasker , Maximus Theodorus Otten , Gerhard Daniel
IPC: H01J37/28 , H01J37/305 , G01N1/06 , G01N1/08 , G01N1/28 , G01N23/04 , G01N1/32 , H01J37/26 , H01J37/06 , H01J37/18 , H01J37/20
CPC classification number: G01N1/28 , G01N1/06 , G01N1/08 , G01N1/32 , G01N23/04 , H01J37/06 , H01J37/18 , H01J37/20 , H01J37/26 , H01J37/28 , H01J37/3056 , H01J2237/063 , H01J2237/182 , H01J2237/204 , H01J2237/208 , H01J2237/2802 , H01J2237/31745 , H01J2237/31749
Abstract: An improved method and apparatus for S/TEM sample preparation and analysis. Preferred embodiments of the present invention provide improved methods for TEM sample creation, especially for small geometry (
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公开(公告)号:US20150206707A1
公开(公告)日:2015-07-23
申请号:US14546244
申请日:2014-11-18
Applicant: FEI Company
Inventor: Jason Arjavac , Pei Zou , David James Tasker , Maximus Theodorus Otten , Gerhard Daniel
CPC classification number: G01N1/28 , G01N1/06 , G01N1/08 , G01N1/32 , G01N23/04 , H01J37/06 , H01J37/18 , H01J37/20 , H01J37/26 , H01J37/28 , H01J37/3056 , H01J2237/063 , H01J2237/182 , H01J2237/204 , H01J2237/208 , H01J2237/2802 , H01J2237/31745 , H01J2237/31749
Abstract: An improved method and apparatus for S/TEM sample preparation and analysis. Preferred embodiments of the present invention provide improved methods for TEM sample creation, especially for small geometry (
Abstract translation: 一种用于S / TEM样品制备和分析的改进方法和装置。 本发明的优选实施例提供用于TEM样品制备的改进方法,特别是对于小几何(<100nm厚)TEM薄片。 本发明的优选实施例还通过提供部分或全部自动化TEM样品制作的方法来提供在诸如集成电路或半导体晶片上制造的其它结构的物体上的基于S / TEM的测量的在线方法,以使得创建过程 并分析TEM样品减少劳动密集度,并提高TEM分析的产量和再现性。
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公开(公告)号:US08890064B2
公开(公告)日:2014-11-18
申请号:US13777018
申请日:2013-02-26
Applicant: FEI Company
Inventor: Jason Arjavac , Pei Zou , David James Tasker , Maximus Theodorus Otten , Gerhard Daniel
IPC: H01J37/26 , H01J37/305 , G01N1/32 , G01N1/28
CPC classification number: G01N1/28 , G01N1/06 , G01N1/08 , G01N1/32 , G01N23/04 , H01J37/06 , H01J37/18 , H01J37/20 , H01J37/26 , H01J37/28 , H01J37/3056 , H01J2237/063 , H01J2237/182 , H01J2237/204 , H01J2237/208 , H01J2237/2802 , H01J2237/31745 , H01J2237/31749
Abstract: An improved method and apparatus for S/TEM sample preparation and analysis. Preferred embodiments of the present invention provide improved methods for TEM sample creation, especially for small geometry (
Abstract translation: 一种用于S / TEM样品制备和分析的改进方法和装置。 本发明的优选实施例提供用于TEM样品制备的改进方法,特别是对于小几何(<100nm厚)TEM薄片。 本发明的优选实施例还通过提供部分或全部自动化TEM样品制作的方法来提供在诸如集成电路或半导体晶片上制造的其它结构的物体上的基于S / TEM的测量的在线方法,以使得创建过程 并分析TEM样品减少劳动密集度,并提高TEM分析的产量和再现性。
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公开(公告)号:US20230197403A1
公开(公告)日:2023-06-22
申请号:US17873532
申请日:2022-07-26
Applicant: FEI Company
Inventor: Thomas Gary Miller , Jason Arjavac , Brian Routh, JR. , Mark Biedrzycki
IPC: H01J37/30 , H01J37/305 , H01J37/28 , H01J37/147
CPC classification number: H01J37/3005 , H01J37/3053 , H01J37/28 , H01J37/1478 , H01J2237/30405
Abstract: Methods and apparatus are disclosed for integration of image-based metrology into a milling workflow. A first ion beam milling operation is performed to an edge at a distance from a final target position on a sample. An SEM image of the sample is used to determine a distance between the milled edge and a reference structure on the sample. Based on the determined distance, the ion beam is adjusted to perform a second milling operation to shift the milled edge to the final target position. Extensions to iterative procedures are disclosed. Various geometric configurations and corrections are disclosed. Manufacturing and analytic applications are disclosed in a variety of fields, including read-write head manufacture and TEM sample preparation. Other combinations of imaging and milling tools can be used.
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公开(公告)号:US20200095688A1
公开(公告)日:2020-03-26
申请号:US16566647
申请日:2019-09-10
Applicant: FEI Company
Inventor: Thomas G. Miller , Jason Arjavac , Michael Moriarty
IPC: C23F1/04 , H01J37/302 , G01N1/32 , H01J37/305
Abstract: A method, system, and computer-readable medium for forming transmission electron microscopy sample lamellae using a focused ion beam including directing a high energy focused ion beam toward a bulk volume of material; milling away the unwanted volume of material to produce an unfinished sample lamella with one or more exposed faces having a damage layer; characterizing the removal rate of the focused ion beam; subsequent to characterizing the removal rate, directing a low energy focused ion beam toward the unfinished sample lamella for a predetermined milling time to deliver a specified dose of ions per area from the low energy focused ion beam; and milling the unfinished sample lamella with the low energy focused ion beam to remove at least a portion of the damage layer to produce the finished sample lamella including at least a portion of the feature of interest.
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公开(公告)号:US08993962B2
公开(公告)日:2015-03-31
申请号:US13746124
申请日:2013-01-21
Applicant: FEI Company
Inventor: Enrique Agorio , James Edgar Hudson , Gerhard Daniel , Michael Tanguay , Jason Arjavac
CPC classification number: H01J37/20 , G01N1/286 , G01N1/32 , G01N2001/2873 , G01N2001/2886 , G01R31/2893 , H01J37/26 , H01J37/28 , H01J37/285 , H01J37/31 , H01J2237/202 , H01J2237/2802 , H01J2237/2812 , H01J2237/3109 , H01J2237/3114 , H01J2237/31745
Abstract: An improved method and apparatus for extracting and handling samples for S/TEM analysis. Preferred embodiments of the present invention make use of a micromanipulator and a hollow microprobe probe using vacuum pressure to adhere the microprobe tip to the sample. By applying a small vacuum pressure to the lamella through the microprobe tip, the lamella can be held more securely and its placement controlled more accurately than by using electrostatic force alone. By using a probe having a beveled tip and which can also be rotated around its long axis, the extracted sample can be placed down flat on a sample holder. This allows sample placement and orientation to be precisely controlled, thus greatly increasing predictability of analysis and throughput.
Abstract translation: 一种用于提取和处理样品用于S / TEM分析的改进方法和装置。 本发明的优选实施例利用显微操纵器和使用真空压力的中空微探针探针将微针尖附着到样品上。 通过通过微针尖向薄片施加小的真空压力,可以比通过单独使用静电力更牢固地保持薄片并且其布置更准确。 通过使用具有倾斜尖端并且也可围绕其长轴旋转的探针,所提取的样品可以平放放置在样品架上。 这样可以精确控制样品放置和取向,从而大大提高分析和产量的可预测性。
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公开(公告)号:US08884247B2
公开(公告)日:2014-11-11
申请号:US13626193
申请日:2012-09-25
Applicant: FEI Company
Inventor: Thomas G. Miller , Jason Arjavac , Damon Heer , Michael Strauss , Gerardus Nicolaas Anne van Veen
IPC: G01N1/28 , H01J37/02 , H01J37/305 , H01J37/20 , G01N1/32
CPC classification number: G01N1/28 , G01N1/32 , H01J37/02 , H01J37/20 , H01J37/3023 , H01J37/3056 , H01J2237/31745
Abstract: A method and system for creating an asymmetrical lamella for use in an ex situ TEM, SEM, or STEM procedure is disclosed. The shape of the lamella provides for easy orientation such that a region of interest in the lamella can be placed over a hole in a carbon film providing minimal optical and spectral interference from the carbon film during TEM, SEM, or STEM procedure of chemical analysis.
Abstract translation: 公开了一种用于创建用于非原位TEM,SEM或STEM程序的不对称薄片的方法和系统。 薄片的形状提供容易的取向,使得薄片中的感兴趣区域可以放置在碳膜上的孔上,从而在化学分析的TEM,SEM或STEM过程期间从碳膜提供最小的光学和光谱干扰。
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公开(公告)号:US20130341505A1
公开(公告)日:2013-12-26
申请号:US13777018
申请日:2013-02-26
Applicant: FEI Company
Inventor: Jason Arjavac , Pei Zou , David James Tasker , Maximus Theodorus Otten , Gerhard Daniel
IPC: H01J37/26
CPC classification number: G01N1/28 , G01N1/06 , G01N1/08 , G01N1/32 , G01N23/04 , H01J37/06 , H01J37/18 , H01J37/20 , H01J37/26 , H01J37/28 , H01J37/3056 , H01J2237/063 , H01J2237/182 , H01J2237/204 , H01J2237/208 , H01J2237/2802 , H01J2237/31745 , H01J2237/31749
Abstract: An improved method and apparatus for S/TEM sample preparation and analysis. Preferred embodiments of the present invention provide improved methods for TEM sample creation, especially for small geometry (
Abstract translation: 一种用于S / TEM样品制备和分析的改进方法和装置。 本发明的优选实施例提供用于TEM样品制备的改进方法,特别是对于小几何(<100nm厚)TEM薄片。 本发明的优选实施例还通过提供部分或全部自动化TEM样品制作的方法来提供在诸如集成电路或半导体晶片上制造的其它结构的物体上的基于S / TEM的测量的在线方法,以使得创建过程 并分析TEM样品减少劳动密集度,并提高TEM分析的产量和再现性。
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