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    Apparatus and methods for deoxidizing metal surfaces
    1.
    发明授权
    Apparatus and methods for deoxidizing metal surfaces 失效
    用于使金属表面脱氧的装置和方法

    公开(公告)号：US08142841B2

    公开(公告)日：2012-03-27

    申请号：US11454667

    申请日：2006-06-16

    申请人： Kevin K. Meagher ,  Timm L. Kelly

    发明人： Kevin K. Meagher ,  Timm L. Kelly

    IPC分类号： B05D5/12 ,  B05D1/36

    CPC分类号： H01M8/0228 ,  C23G1/00 ,  C23G1/08 ,  C23G1/081 ,  C23G1/086 ,  C23G1/18 ,  C23G3/02 ,  C23G3/021 ,  C23G3/023 ,  C23G3/024 ,  C23G3/027 ,  C25F1/04 ,  C25F1/06 ,  H01M8/0206 ,  H01M8/0221

    摘要： Methods for deoxidizing metallic surfaces are disclosed. Such a method may include contacting a surface of a metal strip with one or more chemical solutions until a potential drop across a thickness of the metal strip is less than a pre-selected value. To process a metal strip such that it may be suitable for fabrication of a bipolar plate for use in a fuel cell, the metal strip may be processed until the potential drop is less then about 15 mV. A surface of the metal strip may be contacted for a first period of time with a first chemical solution having a pH of between 10 and 14. Thereafter, the surface may be contacted for a second period of time with a second chemical solution having a pH of between 1 and 3. A conductive organic coating may then be applied to the surface. Such methods are particularly suitable for use in connection with a coil coating process.

    摘要翻译： 公开了用于脱氧金属表面的方法。 这种方法可以包括使金属带的表面与一种或多种化学溶液接触，直到穿过金属带的厚度的电位降小于预选值。 为了处理金属条，使得它可能适用于制造用于燃料电池的双极板，可以处理金属条，直到电位降小于约15mV。 金属带的表面可以与pH为10-14之间的第一化学溶液接触第一时间段。此后，可以用第二化学溶液接触表面第二个时间段，其pH值为 可以在1和3之间。然后可以将导电有机涂层施加到表面。 这种方法特别适合于与线圈涂覆过程相结合使用。

    Coating solution for metal surfaces
    3.
    发明授权
    Coating solution for metal surfaces 失效
    金属表面涂层溶液

    公开(公告)号：US4313769A

    公开(公告)日：1982-02-02

    申请号：US165734

    申请日：1980-07-03

    申请人： Frank J. Frelin ,  Timm L. Kelly ,  Anthony J. Malloy

    发明人： Frank J. Frelin ,  Timm L. Kelly ,  Anthony J. Malloy

    IPC分类号： C23C22/34 ,  C23F7/06

    CPC分类号： C23C22/34

    摘要： In an acidic aqueous coating solution which contains zirconium, hafnium or titanium, and fluoride and which is effective in forming on an aluminum surface a non-chromate coating to which overlying coatings adhere tightly and which is corrosion resistant and resists being discolored when subjected to hot water, the improvement comprising including in said coating solution a surfactant in an amount such that a coating formed from the surfactant-containing coating solution has an improved tendency to resist being discolored by hot water.

    摘要翻译： 在含有锆，铪或钛和氟化物的酸性水性涂料溶液中，其有效地在铝表面上形成非铬酸盐涂层，其上覆盖的涂层紧密地粘附，并且当耐热时耐腐蚀和抗变色 水，所述改进包括在所述涂布溶液中包含表面活性剂，其量使得由含表面活性剂的涂布溶液形成的涂层具有抵抗由热水变色的改善的趋势。

    Coating solution for metal surfaces
    4.
    发明授权
    Coating solution for metal surfaces 失效
    金属表面涂层溶液

    公开(公告)号：US4273592A

    公开(公告)日：1981-06-16

    申请号：US107017

    申请日：1979-12-26

    申请人： Timm L. Kelly

    发明人： Timm L. Kelly

    IPC分类号： C09D5/08 ,  C23C22/34 ,  C23C22/37 ,  C23C30/00 ,  C23F7/06

    CPC分类号： C23C22/34 ,  Y10T428/31786

    摘要： An acidic aqueous coating solution for forming a coating on an aluminum surface which is corrosion resistant and to which overlying coatings adhere excellently. The coating solution contains a zirconium and/or hafnium compound, a fluoride compound, and a polyhydroxy compound having no more than 7 carbon atoms. The coating solution is capable of forming on an aluminum surface a uniformly colorless and clear coating so that the coated surface has the appearance of the underlying metal surface, that is, the coating can be formed without changing the appearance of the metal surface. When coating a bright shiny aluminum surface, there can be produced a coated surface having a uniformly bright shiny appearance which is maintained even after the coated surface is subjected to boiling water. Such surface is capable of undergoing the "muffle test" to confirm the presence of the clear and colorless coating.

    摘要翻译： 用于在铝表面上形成涂层的酸性水性涂料溶液，其具有耐腐蚀性并且其上覆盖的涂层优异地粘附。 涂层溶液含有锆和/或铪化合物，氟化合物和不超过7个碳原子的多羟基化合物。 涂层溶液能够在铝表面上形成均匀无色透明的涂层，使得涂覆表面具有下面的金属表面的外观，即可以在不改变金属表面的外观的情况下形成涂层。 当涂上光亮的铝合金表面时，即使在涂布表面经受沸水后，也可以产生具有均匀亮泽光泽外观的涂层表面。 这种表面能够进行“马弗炉试验”以确认透明无色涂层的存在。

    High performance non-chrome pretreatment for can-end stock aluminum
    6.
    发明授权
    High performance non-chrome pretreatment for can-end stock aluminum 有权
    高性能非铬预处理罐头库存铝

    公开(公告)号：US06881279B2

    公开(公告)日：2005-04-19

    申请号：US10316403

    申请日：2002-12-11

    申请人： Kevin K. Meagher ,  Thomas J. Prescott ,  Timm L. Kelly

    发明人： Kevin K. Meagher ,  Thomas J. Prescott ,  Timm L. Kelly

    IPC分类号： B32B15/04 ,  C04B9/02 ,  C09K3/00 ,  C23C20060101 ,  C23C2/00 ,  C23C22/07 ,  C23C22/36 ,  C23C22/48

    CPC分类号： C23C22/361 ,  C23C22/34 ,  C23C22/83

    摘要： A chemically and thermally stable chromate free aqueous liquid treatment for metals, especially aluminum, that imparts corrosion resistance as good as that from conventional chromate containing treatments, contains water and a fluoroacid selected from the group consisting of H2TiF6, H2 ZrF6, H2HfF6, H2SiF6, H2GeF6, H2SnF6, HBF4, and mixtures thereof; a water soluble organic carboxylic acid that contains at least two hydroxyl groups, exclusive of the hydroxyl groups that are part of any carboxyl groups, per carboxyl group in each acid molecule, the water soluble salts of such acids, and mixtures thereof; a source of phosphate ions; and an organic component selected from the group consisting of tannins and amino-phenolic polymers.

    摘要翻译： 对于具有与常规含铬处理剂相同的耐腐蚀性的金属，特别是铝的化学和热稳定的无铬酸盐水溶液处理，含有水和选自H 2 O 3的氟酸， TiF 6，H 2 ZrF 6，H 2 HfF 6，H 2， H 2 SiF 6，H 2，GeF 6，H 2 SnF 6 HBF 4，及其混合物; 含有至少两个羟基的水溶性有机羧酸，不包含任何羧基的一部分的羟基，每个酸分子中的每个羧基，这些酸的水溶性盐及其混合物; 磷酸根离子源; 和选自单宁和氨基 - 酚聚合物的有机组分。

    Process and composition for conversion coating with improved heat stability
    7.
    发明授权
    Process and composition for conversion coating with improved heat stability 失效
    具有改善热稳定性的转化涂层的工艺和组成

    公开(公告)号：US06558480B1

    公开(公告)日：2003-05-06

    申请号：US09807159

    申请日：2001-07-23

    申请人： Gary L. Rochfort ,  Timm L. Kelly ,  Richard D. Banaszak

    发明人： Gary L. Rochfort ,  Timm L. Kelly ,  Richard D. Banaszak

    IPC分类号： C23C2200

    CPC分类号： C23C22/34

    摘要： A conversion coating that does not substantially diminish the luster of a metal surface on which it is coated nor impair adhesion to the surface of lacquers and printing inks commonly used on beverage containers may be provided by contacting the metal surface with an aqueous liquid composition comprising water and at least the following components: (A) a component of one or more dissolved transition metal compounds that contain zirconium and may also include titanium, provided that zirconium constitutes more than 30% of the moles of the total moles or zirconium and titanium; (B) a component of at least one dissolved compound that contains inorganically bonded fluorine and is not part of component (A); and (C) a component of dissolved organic polymer molecules.

    摘要翻译： 可以通过使金属表面与包含水的水性液体组合物接触来提供不会显着降低其上涂覆的金属表面的光泽或损害对表面和通常用于饮料容器上的印刷油墨的表面的转化涂层 和至少以下组分：（A）含有锆的一种或多种溶解的过渡金属化合物的组分，并且还可以包括钛，条件是锆占总摩尔数的30％以上或锆和钛; （B）至少一种含有无机结合的氟并且不是组分（A）的一部分的溶解化合物的组分; 和（C）溶解的有机聚合物分子的组分。