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76 条记录 (耗时 0.019 秒)

    Methods of making an antistatic agent
    44.
    发明申请
    Methods of making an antistatic agent 有权
    制造抗静电剂的方法

    公开(公告)号：US20050228194A1

    公开(公告)日：2005-10-13

    申请号：US10966774

    申请日：2004-10-15

    申请人： Theodorus Hoeks ,  Chiel Leenders ,  Robert van de Grampel

    发明人： Theodorus Hoeks ,  Chiel Leenders ,  Robert van de Grampel

    IPC分类号： C07C303/32 ,  C07C309/06 ,  C07F9/54 ,  C07C39/02 ,  C07F9/02

    CPC分类号： C07C303/32 ,  C08K5/50 ,  Y10S524/912 ,  C07C309/06

    摘要： A method for making the phosphonium sulfonate salt of generic formula (1): wherein each X is independently a halogen or hydrogen, provided that the molar ratio of halogen to hydrogen is greater than about 0.90; p is 0 or 1 and q and r are integers of 0 to about 7 provided that q+r is less than 8 and that if p is not zero then r is greater than zero; and each R is the same or different hydrocarbon radical containing 1 to about 18 carbon atoms, the method comprising combining in an aqueous medium a compound of generic formula (2): wherein M is Li or Na, and X, q, p, and r are as defined above, with a stoichiometric excess of a compound of the generic formula (3): (R)4P-Z  (3) wherein Z is a halogen and R is as defined above; and separating the product of formula (1) from the medium.

    摘要翻译： 制备通式（1）的鏻磺酸盐的方法：其中每个X独立地为卤素或氢，条件是卤素与氢的摩尔比大于约0.90; p为0或1，q和r为0至约7的整数，条件是q + r小于8，如果p不为零，则r大于零; 并且每个R是含有1至约18个碳原子的相同或不同的烃基，该方法包括在水性介质中混合通式（2）的化合物：其中M是Li或Na，X，q，p和 r如上所定义，化学计量过量的通式（3）的化合物：<？in-line-formula description =“In-line Formulas”end =“lead”→（R） PZ（3）<？in-line-formula description =“In-line Formulas”end =“tail”？>其中Z是卤素，R如上定义; 和将式（1）的产物与介质分离。

    Hydrogenation reaction catalyst precursor, process for production thereof and process for production of alcohol
    46.
    发明授权
    Hydrogenation reaction catalyst precursor, process for production thereof and process for production of alcohol 失效
    氢化反应催化剂前体，其制备方法和醇的生产方法

    公开(公告)号：US5478789A

    公开(公告)日：1995-12-26

    申请号：US317368

    申请日：1994-10-04

    申请人： Yasuyuki Hattori ,  Kiyoshi Tsukada

    发明人： Yasuyuki Hattori ,  Kiyoshi Tsukada

    IPC分类号： B01J23/76 ,  B01J21/06 ,  B01J23/78 ,  B01J23/80 ,  B01J29/76 ,  B01J37/02 ,  C07B61/00 ,  C07C29/149 ,  C07C31/02 ,  C07C33/02 ,  C07C35/02 ,  C07C37/01 ,  C07C39/02 ,  B01J23/72 ,  C07C27/04

    CPC分类号： B01J37/0209 ,  B01J23/78 ,  B01J23/80 ,  B01J37/024 ,  C07C29/149 ,  B01J21/063 ,  B01J21/066 ,  Y02P20/52

    摘要： A hydrogenation reaction catalyst precursor of the present invention comprises a catalyst carrier (A) and a metal oxide composition (B) carried on or mixed with the catalyst carrier (A) at a weight ratio of (B)/(A)=15/85 to 65/35; the catalyst carrier (A) comprising a carrier base material of silica, etc. and a coating of titanium oxide and/or titanium hydroxide, the metal oxide composition (B) comprising copper oxide, zinc oxide, and at least one oxide of a metal selected from the group consisting of an element of group IIa of the periodic table, an element of group IIIb of the table, a lanthanide element, and an actinide element at a weight ratio of 100/(0 to 25)/(0 to 25). A hydrogenation reaction catalyst with a high catalytic activity and a high reaction selectivity is obtained by reduction of the hydrogenation reaction catalyst precursor. By the use of the hydrogenation reaction catalyst of the present invention, a high quality alcohol can be produced at a high yield and with a high selectivity even at a low reaction temperature and a low hydrogen pressure.

    摘要翻译： 本发明的氢化反应催化剂前体包含负载或与催化剂载体（A）以（B）/（A）= 15 /（重量比）的比例负载的催化剂载体（A）和金属氧化物组合物（B） 85至65/35; 包含二氧化硅载体基材等的催化剂载体（A）和氧化钛和/或氢氧化钛的涂层，所述金属氧化物组合物（B）包含氧化铜，氧化锌和至少一种金属氧化物 选自元素周期表IIa族元素，表IIIb族元素，镧系元素和锕系元素，重量比为100 /（0-25）/（0-25） ）。 通过还原氢化反应催化剂前体获得具有高催化活性和高反应选择性的氢化反应催化剂。 通过使用本发明的氢化反应催化剂，即使在低的反应温度和低的氢气压力下，也可以高产率和高选择性地制备高品质的醇。

    Process for manufacturing creosote with non-settling out salts
    48.
    发明授权
    Process for manufacturing creosote with non-settling out salts 失效
    制造具有非沉淀盐的杂酚油的方法

    公开(公告)号：US4603226A

    公开(公告)日：1986-07-29

    申请号：US801455

    申请日：1985-11-25

    申请人： George H. Collingwood ,  Gail L. Erickson ,  Howard L. Simon ,  Roger L. Haley ,  Bill E. Sparling

    发明人： George H. Collingwood ,  Gail L. Erickson ,  Howard L. Simon ,  Roger L. Haley ,  Bill E. Sparling

    IPC分类号： C07C39/02

    CPC分类号： C07C39/02

    摘要： A stable creosote product is prepared from which little or no sludge heel settles and which does not require heat to be applied to prevent settling out of solids. The stable product is obtained by a method that mechanically reduces the particle size or the salts that form upon cooling below the limpid point. The layer of salt which settles on the bottom of the beaker is then mechanically broken and homogenized. The fine salts which had previously settled and were homogenized, did not resettle but remained relatively evenly dispersed throughout the mixture and remained dispersed even after prolonged periods of uninterrupted standing. The salts are not allowed to settle before homogenizing. Little or no heel formation was detected in the creosote in which the settled and material was homogenized as described.

    摘要翻译： 制备稳定的杂酚油产品，由此很少或没有污泥后跟沉降，并且不需要施加热量以防止沉淀出固体。 稳定的产物是通过机械地降低颗粒大小的方法获得的，或者是在冷却下方形成的盐。 然后将沉淀在烧杯底部的盐层机械破碎并均化。 先前沉降并均质化的细盐没有重新定位，但仍然相对均匀地分散在整个混合物中，并且即使在长时间不间断的静置后也保持分散。 在均化之前不允许盐沉降。 在所述杂酚油中检测到很少或没有脚跟形成，其中沉淀的和材料如所述均化。

    Hydroxy aromatic compounds from alkali metal hydroxide and mononuclear aromatic compound
    49.
    发明授权
    Hydroxy aromatic compounds from alkali metal hydroxide and mononuclear aromatic compound 失效
    来自碱金属氢氧化物和单核芳香族化合物的羟基芳族化合物

    公开(公告)号：US4533763A

    公开(公告)日：1985-08-06

    申请号：US561615

    申请日：1983-12-14

    申请人： Barton Milligan ,  George B. DeLaMater

    发明人： Barton Milligan ,  George B. DeLaMater

    IPC分类号： C07C37/00 ,  C07C39/02

    CPC分类号： C07C37/64 ,  C07C37/055

    摘要： This invention pertains to a process for preparing hydroxy mononuclear aromatic compounds by reacting an alkali metal hydroxide with a mononuclear aromatic compound, e.g., benzene, xylene or toluene. The reaction is carried out in the presence of a metallic hydrogenation catalyst, suitably copper, nickel, rhodium or cobalt, the metal being present in an amount sufficient for catalyzing the reaction. The hydroxy mononuclear aromatic compound is then formed by adding a protonating agent to the resulting reaction product, with the protonating agent liberating the hydroxy compound from the salt.

    摘要翻译： 本发明涉及通过使碱金属氢氧化物与单核芳族化合物如苯，二甲苯或甲苯反应来制备羟基单核芳族化合物的方法。 该反应在金属氢化催化剂，适当的铜，镍，铑或钴的存在下进行，金属的存在量足以催化反应。 然后通过向所得反应产物中加入质子化试剂形成羟基单核芳族化合物，质子化剂从盐中释放出羟基化合物。

    Process for the hydroxylation of aromatic compounds
    50.
    发明授权
    Process for the hydroxylation of aromatic compounds 失效
    芳香族化合物羟基化方法

    公开(公告)号：US4301307A

    公开(公告)日：1981-11-17

    申请号：US105776

    申请日：1979-12-20

    申请人： Michel Jouffret

    发明人： Michel Jouffret

    IPC分类号： C07C43/23 ,  C07C27/00 ,  C07C37/60 ,  C07C39/02 ,  C07C39/04 ,  C07C39/06 ,  C07C39/08 ,  C07C39/10 ,  C07C41/00 ,  C07C67/00 ,  C07C41/26

    CPC分类号： C07C37/60 ,  C07C41/26

    摘要： Aromatic hydrocarbons and particularly phenols and phenol ethers can be hydroxylated by reacting the aromatic compound with hydrogen peroxide in a reaction medium comprising trifluoromethanesulfonic acid. High yields of hydroxylated aromatic compounds are obtained by this process which avoids the use of extremely corrosive and difficult to handle agents. Phenol is hydroxylated predominantly to hydroquinone by this process.

    摘要翻译： 通过在包含三氟甲磺酸的反应介质中使芳族化合物与过氧化氢反应，芳族烃，特别是酚和酚醚可被羟基化。 羟基化芳族化合物的高产率通过该方法获得，其避免使用极其腐蚀性和难处理剂。 苯酚主要通过该方法羟化为氢醌。