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1.发明申请公开(公告)号：US20070129472A1
公开(公告)日：2007-06-07
申请号：US11674373
申请日：2007-02-13
CPC分类号： C07C303/32 , C08K5/50 , Y10S524/912 , C07C309/06
摘要： A method for preparing a thermoplastic composition containing an antistatic agent is described. The antistatic agent is a phosphonium sulfonate salt of generic formula (1) wherein each X is independently a halogen or hydrogen, provided that the molar ratio of halogen to hydrogen is greater than about 0.90; p is 0 or 1 and q and r are integers of 0 to about 7 provided that q+r is less than 8 and that if p is not zero then r is greater than zero; and each R is the same or different hydrocarbon radical containing 1 to about 18 carbon atoms. The phosphonium sulfonate salt is prepared by a method that includes combining in an aqueous medium a compound of generic formula (2) wherein M is Li or Na, and X, q, p, and r are as defined above, with a stoichiometric excess of a compound of the generic formula (3) (R)4P-Z (3)wherein Z is a halogen and R is as defined above; and separating the product of formula (1) from the medium. The phosphonium sulfonate salt is then combined with a thermoplastic resin.
摘要翻译： 描述了制备含有抗静电剂的热塑性组合物的方法。 抗静电剂是通式（1）的鏻磺酸盐，其中每个X独立地是卤素或氢，条件是卤素与氢的摩尔比大于约0.90; p为0或1，q和r为0至约7的整数，条件是q + r小于8，如果p不为零，则r大于零; 并且每个R是含有1至约18个碳原子的相同或不同的烃基。 鏻磺酸盐的制备方法包括在水性介质中将通式（2）的化合物（其中M为Li或Na，X，q，p和r如上定义）与化学计量过量的 通式（3）的化合物<？in-line-formula description =“In-line Formulas”end =“lead”？（R）4 PZ（3） line-formula description =“In-line Formulas”end =“tail”？>其中Z是卤素，R如上定义; 和将式（1）的产物与介质分离。 然后将鏻磺酸盐与热塑性树脂组合。
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2.发明申请Thermoplastic composition, method of making, and articles formed therefrom 审中-公开热塑性组合物，制造方法和由其形成的制品公开(公告)号：US20070155913A1
公开(公告)日：2007-07-05
申请号：US11326153
申请日：2006-01-04
CPC分类号： C08L67/02 , C08L69/005 , C08L2666/18
摘要： A thermoplastic composition comprises a polyester-polycarbonate polymer comprising isophthalate-terephthalate-resorcinol ester units and carbonate units, and a poly(alkylene ester) comprising ethylene terephthalate units, 1,4-cyclohexyldimethylene terephthalate units, or a combination of ethylene terephthalate units and 1,4-cyclohexyldimethylene terephthalate units, wherein the sum of the mole percentage values of isophthalate-terephthalate-resorcinol ester units in the polyester-polycarbonate polymer, and of the mole percentage values of 1,4-cyclohexanedimethylene terephthalate units in the poly(alkylene ester) polymer, is a value greater than 40. In other embodiments, polycarbonate may be included. Also disclosed is a method for forming the thermoplastic compositions, and articles prepared therefrom.
摘要翻译： 热塑性组合物包括含有间苯二甲酸酯 - 对苯二甲酸酯 - 间苯二酚酯单元和碳酸酯单元的聚酯 - 聚碳酸酯聚合物和包含对苯二甲酸乙二醇酯单元，1,4-环己基二亚甲基对苯二甲酸酯单元或对苯二甲酸乙二醇酯单元的组合的聚（亚烷基酯） ，其中聚酯 - 聚碳酸酯聚合物中间苯二甲酸酯 - 对苯二甲酸酯 - 间苯二酚酯单元的摩尔百分比值之和和聚对苯二甲酸亚烷基酯聚对苯二甲酸丁二醇酯单元的摩尔百分比值的总和， ）聚合物是大于40的值。在其它实施方案中，可以包括聚碳酸酯。 还公开了一种形成热塑性组合物的方法及其制备的制品。
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公开(公告)号：US20060100327A1
公开(公告)日：2006-05-11
申请号：US10983878
申请日：2004-11-08
IPC分类号： C08K5/49
CPC分类号： C07C303/32 , C07F9/5407 , C07C309/06 , C07C309/10
摘要： Disclosed are methods for making the phosphonium sulfonate salt of generic formula (1): wherein each X is independently a halogen or hydrogen, provided that the molar ratio of halogen to hydrogen is greater than about 0.90; p is 0 or 1 and q and r are integers of 0 to about 7 provided that q+r is less than 8 and that if p is 1 then r is greater than zero; and each R is the same or different hydrocarbon radical containing 1 to about 18 carbon atoms, the method comprising the steps of combining in an aqueous medium, a compound of the generic formula (2): wherein M is K, and X, q, p, and r are as defined above, with a compound of the generic formula (3): (R)4P-Z (3) wherein Z is a halogen and R is as defined above; and separating the phosphonium sulfonate of formula (1) from the aqueous medium. Also disclosed is an antistatic composition comprising phosphonium sulfonate (1), and articles prepared therefrom.
摘要翻译： 公开了制备通式（1）的鏻磺酸盐的方法：其中每个X独立地是卤素或氢，条件是卤素与氢的摩尔比大于约0.90; p为0或1，q和r为0至约7的整数，条件是q + r小于8，如果p为1，则r大于零; 并且每个R是含有1至约18个碳原子的相同或不同的烃基，该方法包括以下步骤：在水性介质中混合通式（2）的化合物：其中M是K，X，q， p和r如上所定义，与通式（3）的化合物：<？in-line-formula description =“In-line Formulas”end =“lead”？（R） PZ（3）<？in-line-formula description =“In-line Formulas”end =“tail”？>其中Z是卤素，R如上所定义; 并将式（1）的磺酸鏻与水性介质分离。 还公开了包含磺酸鏻（1）和由其制备的制品的抗静电组合物。
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4.发明授权Thermoplastic composition, method of manufacture thereof, and articles derived therefrom 有权热塑性组合物，其制造方法和由其衍生的制品公开(公告)号：US07691304B2
公开(公告)日：2010-04-06
申请号：US11765027
申请日：2007-06-19
IPC分类号： C08G64/00
CPC分类号： C08L67/02 , C08K5/0008 , C08L69/00 , C08L69/005 , Y10T428/24124 , Y10T428/31786 , C08L2666/18
摘要： Disclosed herein is a thermoplastic composition comprising a combination of 10 to 80 wt. % of a polyester, more than 0 to 50 wt. % of a polycarbonate, and 10 to 90 wt. % of at least one polyester-polycarbonate copolymer comprising, based on the total weight of the copolymer, 15 to 95 wt. % of arylate ester units, and 5 to 85 wt. % of aromatic carbonate units. Also disclosed is a method of forming the compositions, and articles prepared therefrom, for example transparent covers.
摘要翻译： 本文公开了一种热塑性组合物，其包含10至80重量％ ％的聚酯，大于0至50wt。 ％的聚碳酸酯，和10〜90wt。 ％的至少一种聚酯 - 聚碳酸酯共聚物，基于共聚物的总重量为15〜95重量％ ％的芳基酯单元，和5至85wt。 ％的芳族碳酸酯单元。 还公开了形成组合物的方法和由其制备的制品，例如透明盖。
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公开(公告)号：US20050228194A1
公开(公告)日：2005-10-13
申请号：US10966774
申请日：2004-10-15
IPC分类号： C07C303/32 , C07C309/06 , C07F9/54 , C07C39/02 , C07F9/02
CPC分类号： C07C303/32 , C08K5/50 , Y10S524/912 , C07C309/06
摘要： A method for making the phosphonium sulfonate salt of generic formula (1): wherein each X is independently a halogen or hydrogen, provided that the molar ratio of halogen to hydrogen is greater than about 0.90; p is 0 or 1 and q and r are integers of 0 to about 7 provided that q+r is less than 8 and that if p is not zero then r is greater than zero; and each R is the same or different hydrocarbon radical containing 1 to about 18 carbon atoms, the method comprising combining in an aqueous medium a compound of generic formula (2): wherein M is Li or Na, and X, q, p, and r are as defined above, with a stoichiometric excess of a compound of the generic formula (3): (R)4P-Z (3) wherein Z is a halogen and R is as defined above; and separating the product of formula (1) from the medium.
摘要翻译： 制备通式（1）的鏻磺酸盐的方法：其中每个X独立地为卤素或氢，条件是卤素与氢的摩尔比大于约0.90; p为0或1，q和r为0至约7的整数，条件是q + r小于8，如果p不为零，则r大于零; 并且每个R是含有1至约18个碳原子的相同或不同的烃基，该方法包括在水性介质中混合通式（2）的化合物：其中M是Li或Na，X，q，p和 r如上所定义，化学计量过量的通式（3）的化合物：<？in-line-formula description =“In-line Formulas”end =“lead”→（R） PZ（3）<？in-line-formula description =“In-line Formulas”end =“tail”？>其中Z是卤素，R如上定义; 和将式（1）的产物与介质分离。
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6.发明申请公开(公告)号：US20080119597A1
公开(公告)日：2008-05-22
申请号：US11765052
申请日：2007-06-19
CPC分类号： C08L67/02 , C08K5/0008 , C08L69/005 , C08L2205/02 , Y10T428/24124 , Y10T428/31786 , C08L2666/18
摘要： Disclosed herein is a thermoplastic composition comprising a combination of 10 to 80 wt. % of a polyester and 10 to 90 wt. % of at least one two polyester-polycarbonate copolymers comprising, based on the total weight of the copolymer, 10 to 95 wt. % of arylate ester units, and 5 to 85 wt. % of aromatic carbonate units. Also disclosed is a method of forming the compositions, and articles prepared therefrom, for example transparent covers.
摘要翻译： 本文公开了一种热塑性组合物，其包含10至80重量％ ％的聚酯和10至90wt。 至少一种两种聚酯 - 聚碳酸酯共聚物的％，基于共聚物的总重量，包含10至95wt。 ％的芳基酯单元，和5至85wt。 ％的芳族碳酸酯单元。 还公开了形成组合物的方法和由其制备的制品，例如透明盖。
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7.发明申请公开(公告)号：US20080119596A1
公开(公告)日：2008-05-22
申请号：US11765027
申请日：2007-06-19
CPC分类号： C08L67/02 , C08K5/0008 , C08L69/00 , C08L69/005 , Y10T428/24124 , Y10T428/31786 , C08L2666/18
摘要： Disclosed herein is a thermoplastic composition comprising a combination of 10 to 80 wt. % of a polyester, more than 0 to 50 wt. % of a polycarbonate, and 10 to 90 wt. % of at least one polyester-polycarbonate copolymer comprising, based on the total weight of the copolymer, 15 to 95 wt. % of arylate ester units, and 5 to 85 wt. % of aromatic carbonate units. Also disclosed is a method of forming the compositions, and articles prepared therefrom, for example transparent covers.
摘要翻译： 本文公开了一种热塑性组合物，其包含10至80重量％ ％的聚酯，大于0至50wt。 ％的聚碳酸酯，和10〜90wt。 ％的至少一种聚酯 - 聚碳酸酯共聚物，基于共聚物的总重量为15〜95重量％ ％的芳基酯单元，和5至85wt。 ％的芳族碳酸酯单元。 还公开了形成组合物的方法和由其制备的制品，例如透明盖。
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公开(公告)号：US20080015377A1
公开(公告)日：2008-01-17
申请号：US11772309
申请日：2007-07-02
IPC分类号： C07C309/64
CPC分类号： C07C303/32 , C07F9/5407 , C07C309/06 , C07C309/10
摘要： Disclosed are methods for making a phosphonium sulfonate salt of generic formula (1): wherein each X is independently a halogen or hydrogen, provided that the molar ratio of halogen to hydrogen is greater than- about 0.90; p is 0 or 1 and q and r are integers of 0 to about 7 provided that q+r is less than 8 and that if p is 1 then r is greater than zero; and each R is the same or different hydrocarbon radical containing 1 to about 18 carbon atoms.
摘要翻译： 公开了制备通式（1）的磺酸鏻盐的方法：其中每个X独立地为卤素或氢，条件是卤素与氢的摩尔比大于约0.90; p为0或1，q和r为0至约7的整数，条件是q + r小于8，如果p为1，则r大于零; 并且每个R是含有1至约18个碳原子的相同或不同的烃基。
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9.发明授权Thermoplastic composition, method of manufacture thereof, and articles derived therefrom 有权热塑性组合物，其制造方法和由其衍生的制品公开(公告)号：US07686998B2
公开(公告)日：2010-03-30
申请号：US11765052
申请日：2007-06-19
IPC分类号： C08G63/02
CPC分类号： C08L67/02 , C08K5/0008 , C08L69/005 , C08L2205/02 , Y10T428/24124 , Y10T428/31786 , C08L2666/18
摘要： Disclosed herein is a thermoplastic composition comprising a combination of 10 to 80 wt. % of a polyester and 10 to 90 wt. % of at least one two polyester-polycarbonate copolymers comprising, based on the total weight of the copolymer, 10 to 95 wt. % of arylate ester units, and 5 to 85 wt. % of aromatic carbonate units. Also disclosed is a method of forming the compositions, and articles prepared therefrom, for example transparent covers.
摘要翻译： 本文公开了一种热塑性组合物，其包含10至80重量％ ％的聚酯和10至90wt。 至少一种两种聚酯 - 聚碳酸酯共聚物的％，基于共聚物的总重量，包含10至95wt。 ％的芳基酯单元，和5至85wt。 ％的芳族碳酸酯单元。 还公开了形成组合物的方法和由其制备的制品，例如透明盖。
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10.发明申请公开(公告)号：US20080081857A1
公开(公告)日：2008-04-03
申请号：US11869338
申请日：2007-10-09
CPC分类号： C07C303/32 , C08K5/50 , Y10S524/912 , C07C309/06
摘要： A method for preparing a thermoplastic composition containing an antistatic agent is described. The antistatic agent is a phosphonium sulfonate salt of generic formula (1) wherein each X is independently a halogen or hydrogen, provided that the molar ratio of halogen to hydrogen is greater than about 0.90; p is 0 or 1 and q and r are integers of 0 to about 7 provided that q+r is less than 8 and that if p is not zero then r is greater than zero; and each R is the same or different hydrocarbon radical containing 1 to about 18 carbon atoms. The phosphonium sulfonate salt is prepared by a method that includes combining in an aqueous medium sodium hydroxide and/or lithium hydroxide, a compound of the generic formula (4) wherein X, q, p, and r are as defined above, and a compound of the generic formula (3) (R)4P-Z (3) wherein Z is a halogen and R is as defined above; and separating the phosphonium sulfonate of formula (1) from the aqueous medium. The phosphonium sulfonate salt is then combined with a thermoplastic resin.
摘要翻译： 描述了制备含有抗静电剂的热塑性组合物的方法。 抗静电剂是通式（1）的鏻磺酸盐，其中每个X独立地是卤素或氢，条件是卤素与氢的摩尔比大于约0.90; p为0或1，q和r为0至约7的整数，条件是q + r小于8，如果p不为零，则r大于零; 并且每个R是含有1至约18个碳原子的相同或不同的烃基。 鏻磺酸盐通过包括在水性介质氢氧化钠和/或氢氧化锂中组合其中X，q，p和r如上定义的通式（4）的化合物和化合物 通用公式（3）<？in-line-formula description =“In-line Formulas”end =“lead”？>（R）（3） formula description =“In-line Formulas”end =“tail”？>其中Z是卤素，R如上定义; 并将式（1）的磺酸鏻与水性介质分离。 然后将鏻磺酸盐与热塑性树脂组合。
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