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    PIMARIC TYPE RESIN ACID PRODUCT, AND METHOD OF PREPARING THE SAME
    7.
    发明申请
    PIMARIC TYPE RESIN ACID PRODUCT, AND METHOD OF PREPARING THE SAME 审中-公开
    PIMARIC型树脂酸产品及其制备方法

    公开(公告)号：US20140148572A1

    公开(公告)日：2014-05-29

    申请号：US14170038

    申请日：2014-01-31

    申请人： INSTITUTE OF CHEMICAL INDUSTRY OF FOREST PRODUCTS, CAF

    发明人： Zhendong Zhao ,  Yuxiang Chen ,  Liangwu Bi ,  Yan Gu ,  Dongmei Li ,  Jing Wang ,  Yanju Lu

    IPC分类号： C08H99/00

    CPC分类号： C08H99/00 ,  C07B41/08 ,  C07C2603/26 ,  C08H8/00

    摘要： A method for preparing pimaric acid type resin acids includes: step (1) adding refined resin acid, turpentine, or rosin along with maleic anhydride at a mass ratio of 1:0.3-1.5 into a reaction bottle, dissolving the ingredients into a C1-C10 lower fatty acid solvent, the mass ratio of the C1-C10 low fatty acid to refined resin acid is 0.05-30:1, then carrying out additional reaction by heating directly or with assistance of a microwave, subsequently cooling, crystallizing, filtering, and washing; and step (2) combining the filtrates collected in step (1), stripping the solvent by vacuum distillation to obtain pimaric acid type resin acid coarse product, dissolving the resulting coarse product in NaOH aqueous solution to prepare aqueous solution of pimaric acid type resin acid salt, adjusting the pH to 6-14 with a mineral acid or an organic acid, and either directly purifying or acidifying followed by purifying to obtain the final product.

    摘要翻译： 制备海松酸型树脂酸的方法包括：步骤（1）将质量比为1:0.3-1.5的精制树脂酸，松节油或松香与马来酸酐加入到反应瓶中，将成分溶解在C1- C10低级脂肪酸溶剂，C1-C10低级脂肪酸与精制树脂酸的质量比为0.05-30:1，然后直接加热或在微波辅助下进行附加反应，随后冷却，结晶，过滤， 洗涤; 和步骤（2）将步骤（1）中收集的滤液合并，通过真空蒸馏除去溶剂，得到海松酸型树脂酸粗产物，将所得粗产物溶解在NaOH水溶液中，制备海松酸型树脂酸水溶液 盐，用无机酸或有机酸将pH调节至6-14，直接纯化或酸化，然后纯化，得到最终产物。

    PROCESS AND INTERMEDIATE COMPOUNDS USEFUL IN THE PREPARATION OF STATINS
    8.
    发明申请
    PROCESS AND INTERMEDIATE COMPOUNDS USEFUL IN THE PREPARATION OF STATINS 失效
    过程和中间化合物在制备统计数据中有用

    公开(公告)号：US20120323011A1

    公开(公告)日：2012-12-20

    申请号：US13599606

    申请日：2012-08-30

    申请人： David John Moody ,  Jonathan William Wiffen

    发明人： David John Moody ,  Jonathan William Wiffen

    IPC分类号： C07C51/31 ,  C07D405/06 ,  C07D309/30 ,  C07D309/10 ,  C07C51/36 ,  C07C51/347

    CPC分类号： C07B41/08 ,  C07C51/09 ,  C07D209/24 ,  C07D215/14 ,  C07D257/04 ,  C07D309/10 ,  C07D309/30 ,  C07D405/06 ,  Y02P20/55 ,  C07C59/58

    摘要： There is provides a process for the preparation of a compound of formula (7): wherein R is an optionally substituted hydrocarbyl group or an optionally substituted heterocyclic group; provides that R is not a compound of Formula (a): wherein Ra represents an alkyl group, such as a C1-16 alkyl group, and preferably an isopropyl group; Rb represents an aryl group, preferably a 4-fluorophenyl group; Rc represents hydrogen, a protecting group or an alkyl group, such as a C1-16 alkyl group, and preferably a methyl group; and Rd represents hydrogen, a protecting group or a SO2Re group where Re is an alkyl group, such as a C1-16 alkyl group, and preferably a methyl group.

    摘要翻译： 提供制备式（7）化合物的方法：其中R是任选取代的烃基或任选取代的杂环基; 提供R不是式（a）的化合物：其中R a表示烷基，例如C 1-16烷基，优选异丙基; Rb表示芳基，优选4-氟苯基; Rc表示氢，保护基或烷基，例如C1-16烷基，优选甲基; Rd表示氢，保护基或SO 2 Re基，其中Re为烷基，例如C 1-16烷基，优选甲基。

    Process for producing carboxylated compound
    9.
    发明授权
    Process for producing carboxylated compound 失效
    羧化化合物的制备方法

    公开(公告)号：US5310944A

    公开(公告)日：1994-05-10

    申请号：US975444

    申请日：1992-01-17

    申请人： Takao Kawaki ,  Yuh Miyauchi ,  Toshio Watanabe ,  Katsushige Hayashi ,  Satoshi Ueno ,  Hiroshi Ogawa ,  Fumiya Zaima

    发明人： Takao Kawaki ,  Yuh Miyauchi ,  Toshio Watanabe ,  Katsushige Hayashi ,  Satoshi Ueno ,  Hiroshi Ogawa ,  Fumiya Zaima

    IPC分类号： C07B41/08 ,  C07B41/12 ,  C07C51/285 ,  C07D315/00 ,  C07D313/04 ,  C07D307/33 ,  C07D309/30

    CPC分类号： C07D315/00 ,  C07B41/08 ,  C07B41/12 ,  C07C51/285

    摘要： A process for producing a carboxylated compound, which comprises reacting a carbonyl compound with hydrogen peroxide in the presence of an organo-arsenic acid of the formula (1), ##STR1## wherein: R.sup.1 is a C.sub.1 -C.sub.12 alkyl group which may be substituted or an aryl group which may be substituted,R.sup.2 is a hydroxyl group or the same group as that which defines R.sup.1,or alternatively, R.sup.1 and R.sup.2 may bond to each other to form a five-membered or six-membered ring together with As atoms to which these groups are bonded, andthe substituent(s) substituted on the above groups is/are selected from hydroxyl, carboxyl, carbonyl, sulfonyl, sulfonium, an amino group, an ammonium group, an alkyl group, an alkoxyl group and a halogen atom,while a water concentration in a reaction system is maintained at not more than 2% by weight, thereby to form a corresponding carboxylated compound.

    摘要翻译： 一种羧化化合物的制备方法，其包括在式（1）的有机砷酸存在下使羰基化合物与过氧化氢反应，其中：R1是C1-C12烷基， 可以被取代，或者可以被取代的芳基，R 2是与定义R 1的羟基或者相同的基团，或者，R 1和R 2可以彼此键合以形成五元或六元环在一起 与这些基团键合的As原子，并且上述取代基的取代基选自羟基，羧基，羰基，磺酰基，锍，氨基，铵基，烷基，烷氧基 基团和卤素原子，而反应体系中的水浓度保持在不超过2重量％，从而形成相应的羧化化合物。