公开(公告)号：US20240313285A1

公开(公告)日：2024-09-19

申请号：US18268445

申请日：2021-12-17

申请人： Queen's University at Kingston

发明人： Ahmad Ghahreman ,  Harshit Mahandra ,  Yeonuk Choi

IPC分类号： H01M10/54 ,  C01B25/30 ,  C01D15/08 ,  C01G49/02 ,  C22B3/22 ,  C22B3/44 ,  C22B7/00 ,  C22B26/12

CPC分类号： H01M10/54 ,  C01B25/30 ,  C01D15/08 ,  C01G49/02 ,  C22B3/22 ,  C22B3/44 ,  C22B7/007 ,  C22B26/12

摘要： Methods for recycling lithium and iron containing material, such as batteries, include selectively leaching lithium from the material by disposing the material in a powder form in a solution comprising formic acid and hydrogen peroxide, filtering the solution to obtain a first leach liquor comprising lithium and a residue comprising iron phosphate and carbon, subjecting the first leach liquor to a first precipitation to remove residual iron from the leach liquor and obtain a second leach liquor, and subjecting the second leach liquor to a second precipitation, wherein lithium is precipitated and a third leach liquor is obtained. The third leach liquor may be subjected to a third precipitation using trisodium phosphate or sodium carbonate. The material may be a battery cathode, such as a lithium iron phosphate battery cathode.

公开(公告)号：US12055541B2

公开(公告)日：2024-08-06

申请号：US18460221

申请日：2023-09-01

申请人： THE BRIGHAM AND WOMEN'S HOSPITAL, INC.

发明人： Omid Farokhzad ,  Morteza Mahmoudi ,  Claudia Corbo

IPC分类号： G01N31/00 ,  C01G49/02 ,  G01N33/53 ,  G01N33/543 ,  G01N33/574 ,  G01N33/68 ,  G06F18/24 ,  G06N20/20 ,  G16B40/20 ,  B82Y35/00

CPC分类号： G01N33/5432 ,  C01G49/02 ,  G01N33/54326 ,  G01N33/57488 ,  G01N33/6842 ,  G01N33/6848 ,  G06F18/24 ,  G06N20/20 ,  G16B40/20 ,  B82Y35/00 ,  C01P2004/64 ,  G06F2218/20

摘要： The present disclosure provides a system comprising a communication interface and computer for assigning a label to the biomolecule fingerprint, wherein the label corresponds to a biological state. The present disclosure also provides a sensor arrays for detecting biomolecules and methods of use. In some embodiments, the sensor arrays are capable of determining a disease state in a subject.

公开(公告)号：US12054805B2

公开(公告)日：2024-08-06

申请号：US17243032

申请日：2021-04-28

申请人： University of Kansas

发明人： Mark Brandon Shiflett ,  David Richard Corbin ,  Ankit Verma

IPC分类号： C22B21/00 ,  C01F7/20 ,  C01G49/02 ,  C22B3/12

CPC分类号： C22B21/0015 ,  C01F7/20 ,  C01G49/02 ,  C22B3/12

摘要： Methods for recovering a metal from a metal-containing material are provided. In embodiments, such a method comprises exposing a metal-containing material to a leaching solution comprising a solvent and a binoxalate, a tetraoxalate, or a combination thereof, under conditions to provide a leachate comprising a soluble metal oxalate; inducing precipitation of a metal-containing precipitate comprising the metal of the soluble metal oxalate from the leachate; and recovering the metal-containing precipitate.

公开(公告)号：US11961980B2

公开(公告)日：2024-04-16

申请号：US16499122

申请日：2018-03-29

申请人： JX METALS CORPORATION

发明人： Junichi Arakawa ,  Yasufumi Haga ,  Junichi Ito

IPC分类号： H01M10/54 ,  B09B3/00 ,  B09B5/00 ,  C01G45/02 ,  C01G49/02 ,  C22B1/02 ,  C22B3/00 ,  C22B3/06 ,  C22B3/44 ,  C22B7/00 ,  C22B15/00 ,  C22B21/00 ,  C22B23/00 ,  C22B26/12 ,  H01M10/0525

CPC分类号： H01M10/54 ,  B09B3/00 ,  B09B5/00 ,  C01G45/02 ,  C01G49/02 ,  C22B1/02 ,  C22B3/06 ,  C22B3/44 ,  C22B7/00 ,  C22B7/007 ,  C22B15/00 ,  C22B15/0086 ,  C22B21/00 ,  C22B23/00 ,  C22B23/0415 ,  C22B26/12 ,  H01M10/0525 ,  Y02P10/20 ,  Y02W30/84

摘要： The present invention relates to a method for treating lithium ion battery scrap containing Li, Ni, Co, Mn, Al, Cu and Fe, the method comprising carrying out a calcination step, a crushing step and a sieving step in this order, and after the steps, the method comprising: a leaching step of leaching the lithium ion battery scrap by adding it to an acidic solution to leave at least a part of Cu as a solid; a Fe/Al removal step comprising allowing a leached solution obtained in the leaching step to pass through a Fe removal process for separating and removing Fe by addition of an oxidizing agent and an Al removal process for separating and removing a part of Al by neutralization in any order; an Al/Mn extraction step of extracting and removing a residue of Al and Mn from a separated solution obtained in the Fe/Al removal step by solvent extraction; a Co recovery step of extracting and back-extracting Co from a first extracted solution obtained in the Al/Mn extraction step by solvent extraction and recovering the Co by electrolytic winning; a Ni recovery step of extracting and back-extracting, by solvent extraction, a part of Ni from a second extracted solution obtained by the solvent extraction in the Co recovery step and recovering the Ni by electrolytic winning; a Li concentration step of extracting and back-extracting, by solvent extraction, a residue of Ni and Li from a third extracted solution obtained by the solvent extraction in the Ni recovery step and repeating the operations of the extracting and the back-extracting to concentrate Li; and a Li recovery step of carbonating Li in a Li concentrated solution obtained in the Li concentration step to recover the Li as lithium carbonate.

公开(公告)号：US11641014B2

公开(公告)日：2023-05-02

申请号：US15982776

申请日：2018-05-17

申请人： HHeLi, LLC

发明人： Paige L. Johnson

IPC分类号： H01M10/052 ,  H01M4/131 ,  H01M4/36 ,  H01M4/38 ,  H01M4/48 ,  H01M4/505 ,  H01M4/52 ,  H01M4/525 ,  H01M4/58 ,  H01M4/62 ,  C01G15/00 ,  C01G19/02 ,  C01G23/04 ,  C01G25/02 ,  C01G29/00 ,  C01G30/00 ,  C01G49/00 ,  C01G49/02 ,  H01M10/0525 ,  H01M4/02

摘要： A battery comprising an acidified metal oxide (“AMO”) material, preferably in monodispersed nanoparticulate form 20 nm or less in size, having a pH −12, at least on its surface.

公开(公告)号：US20230093787A9

公开(公告)日：2023-03-23

申请号：US17220637

申请日：2021-04-01

申请人： HHELI, LLC

发明人： Paige L. Johnson ,  Jonathan G. Neff

IPC分类号： H01M4/48 ,  C01G23/047 ,  C01G25/02 ,  C01G49/02

摘要： An acidified metal oxide (“AMO”) material, preferably in monodisperse nanoparticulate form 20 nm or less in size, having a pH −12, at least on its surface. The AMO material is useful in applications such as a battery electrode, catalyst, or photovoltaic component.

公开(公告)号：US20230043211A1

公开(公告)日：2023-02-09

申请号：US17834855

申请日：2022-06-07

申请人： Agency for Science, Technology and Research

发明人： Jackie Y. YING ,  Ayman Amin ABDELHAMID

IPC分类号： H01M4/48 ,  C01G19/02 ,  C01G23/08 ,  C01G25/02 ,  C01G33/00 ,  C01G45/02 ,  C01G49/02 ,  C01G51/04 ,  C01G51/00 ,  C01G53/04 ,  C01G53/00 ,  H01M4/485 ,  H01M4/52 ,  H01M4/525 ,  H01M10/0525 ,  H01M4/50

摘要： The present invention generally relates to a method for preparing metal oxide nanosheets. In a preferred embodiment, graphene oxide (GO) or graphite oxide is employed as a template or structure directing agent for the formation of the metal oxide nanosheets, wherein the template is mixed with metal oxide precursor to form a metal oxide precursor-bonded template. Subsequently, the metal oxide precursor-bonded template is calcined to form the metal oxide nanosheets. The present invention also relates to a lithium-ion battery anode comprising the metal oxide nanosheets. In a further preferred embodiment, the battery anode may comprise a reduced template, which is reduced graphene oxide (rGO) or reduced graphite oxide.

公开(公告)号：US11498836B1

公开(公告)日：2022-11-15

申请号：US16899244

申请日：2020-06-11

申请人： L3 Développement de procédés Inc.

发明人： Tommee Metivier-Larochelle ,  Eric F. Larochelle

IPC分类号： C01G49/02 ,  C01G49/06 ,  C01B7/05

摘要： A method for producing an iron pigment and hydrochloric acid with reduced or substantially eliminated waste streams includes: providing an iron chloride solution, wherein the iron chloride solution includes one or both of iron (II) chloride and iron (III) chloride; neutralizing the iron chloride solution with one or both of ammonia and ammonium hydroxide to form a slurry of an iron oxide solid component and an ammonium chloride solution; separating the iron oxide solid component from the ammonium chloride solution; drying the iron oxide solid component to form an iron pigment or pigment intermediate; reacting the ammonium chloride solution with an alkaline-earth metal solid to form an alkaline-earth metal chloride solution and to evolve ammonia as a vapor, wherein at least a portion of the evolved ammonia reacts with water to form ammonium hydroxide; recycling one or both of the evolved ammonia and the formed ammonium chloride for use in connection with the neutralization step; and pyrohydrolyzing the alkaline-earth metal chloride solution to form hydrochloric acid and to regenerate the alkaline-earth metal solid. Iron pigment or pigment intermediate produced in accordance with the method may have a yellow, red, or black color.

公开(公告)号：US11476019B2

公开(公告)日：2022-10-18

申请号：US17113717

申请日：2020-12-07

申请人： LG Chem, Ltd.

发明人： Jin Kyu Lee ,  Sang Bum Ahn

IPC分类号： H01F1/00 ,  B33Y50/02 ,  C08L101/00 ,  B22F3/105 ,  C08K5/00 ,  B29C67/00 ,  H01F41/02 ,  H01F1/37 ,  B22F1/16 ,  C01G49/02 ,  C08J5/00 ,  B33Y10/00 ,  B33Y70/00

摘要： The present application relates to a composition, a 3D printing method using the same, and a three-dimensional shape comprising the same, and provides a composition capable of embodying a precise formation of a three-dimensional shape using a ceramic material and a uniform curing property of the three-dimensional shape.

公开(公告)号：US11435360B2

公开(公告)日：2022-09-06

申请号：US17215923

申请日：2021-03-29

申请人： THE BRIGHAM AND WOMEN'S HOSPITAL, INC.

发明人： Omid Farokhzad ,  Morteza Mahmoudi ,  Claudia Corbo

IPC分类号： G01N31/00 ,  G01N33/53 ,  G01N33/68 ,  C01G49/02 ,  G06K9/00 ,  G06N20/20 ,  G06K9/62 ,  G01N33/543 ,  G16B40/20 ,  G01N33/574 ,  B82Y35/00

摘要： The present disclosure provides a system comprising a communication interface and computer for assigning a label to the biomolecule fingerprint, wherein the label corresponds to a biological state. The present disclosure also provides a sensor arrays for detecting biomolecules and methods of use. In some embodiments, the sensor arrays are capable of determining a disease state in a subject.