Nanostructured titanic acid salts and preparation process and use thereof

    公开(公告)号:US11554966B2

    公开(公告)日:2023-01-17

    申请号:US16554862

    申请日:2019-08-29

    摘要: The present invention provides a nanostructured titanic acid salt and a preparation process and use thereof. The process comprises preparing a dispersion containing titanium peroxy complex; slowly adding a metal compound to the dispersion containing the titanium peroxy complex to form a solution; adding an alcohol to the solution under normal temperature and normal pressure to produce the nanostructured titanic acid salt precursor precipitate in the solution, and separating the precipitate to obtain the titanic acid salt precursor; drying the precursor, and then heat treating it to obtain the nanostructured titanic acid salt product. The present invention provides a process for preparing a titanic acid salt with simple preparation process, easy control for process parameters and easy large-scale industrial production.

    PROCESS FOR THE PRODUCTION OF TITANIUM DIOXIDE, AND TITANIUM DIOXIDE OBTAINED THEREBY

    公开(公告)号:US20220194812A1

    公开(公告)日:2022-06-23

    申请号:US17688913

    申请日:2022-03-08

    摘要: A process for producing a particulate TiO2 includes supplementing metatitanic acid with an alkali compound in a quantity of 1200 ppm to 2400 ppm of alkali, with a phosphorus compound in a quantity of 0.1 wt.-% to 0.3 wt.-% by weight of P, expressed as phosphorus, and with an aluminum compound in a quantity of 1 ppm to 1000 ppm of Al, expressed as Al, to obtain a mixture. The quantity of the alkali compound, of the phosphorus compound, and of the aluminum compound are with respect to the TiO2 content. The mixture is calcined at a constant temperature of 940° C. to 1020° C. until a numerical fraction X50 of TiO2 has a primary crystallite size of at least 200 nm, to obtain a calcined mixture. The calcined mixture is cooled to obtain a cooled calcined mixture. The cooled calcined mixture is grinded to obtain the particulate TiO2.

    PREPARATION OF TITANIUM DIOXIDE
    8.
    发明申请

    公开(公告)号:US20210403339A1

    公开(公告)日:2021-12-30

    申请号:US17291106

    申请日:2019-11-07

    申请人: TNG LIMITED

    IPC分类号: C01G23/053 C01G23/08

    摘要: A method for the preparation of titanium dioxide, the method comprising the steps of subjecting a titanium containing leach residue to a concentrated sulfuric acid digest step; and in turn subjecting that residue to a leach in dilute sulfuric acid, whereby a black liquor is obtained and from which titanium dioxide is in turn obtained.