Method and apparatus for making a vapor of precise concentration by sublimation

    公开(公告)号:US12104252B2

    公开(公告)日:2024-10-01

    申请号:US17493278

    申请日:2021-10-04

    Inventor: Egbert G. Woelk

    CPC classification number: C23C16/52 C23C16/4481 C23C16/45506

    Abstract: Techniques for controlling a solid precursor vapor source are provided. An example method of controlling a solid precursor vapor source includes providing a carrier gas to a sublimation vessel containing a solid precursor material, wherein the carrier gas is heated with a carrier gas temperature control device prior to entering the sublimation vessel, measuring a temperature of a vapor exiting the sublimation vessel, and controlling a temperature of the carrier gas with the carrier gas temperature control device based at least in part on the temperature of the vapor exiting the sublimation vessel.

    REMOTE SOLID SOURCE REACTANT DELIVERY SYSTEMS FOR VAPOR DEPOSITION REACTORS

    公开(公告)号:US20230175127A1

    公开(公告)日:2023-06-08

    申请号:US18074629

    申请日:2022-12-05

    Inventor: Todd Dunn Paul Ma

    CPC classification number: C23C16/4481 C23C16/45561 C23C16/52

    Abstract: Herein disclosed are systems and methods related to remote delivery systems using solid source chemical bulk fill vessels. The delivery system can include a vapor deposition reactor, two or more bulk fill vessels remote from the vapor deposition reactor, an interconnect line, a line heater, and a gas panel comprising one or more valves. Each bulk fill vessel is configured to hold solid source chemical reactant therein. The bulk fill vessels can each include fluid outlets. The interconnect line can fluidly connect the vapor deposition reactor with each bulk fill vessel. The line heater can heat at least a portion of the interconnect line to at least a minimum line temperature. The one or more valves of the gas panel can switch a flow of vaporized chemical reactant through the interconnect line from being from one fluid outlet to being from another fluid outlet.

    METHODS FOR METAL-ORGANIC CHEMICAL VAPOUR DEPOSITION USING SOLUTIONS OF INDIUM-ALKYL COMPOUNDS IN HYDROCARBONS

    公开(公告)号:US20180355478A1

    公开(公告)日:2018-12-13

    申请号:US15778274

    申请日:2016-11-24

    Abstract: The invention relates to methods for producing an indium-containing layer by metal-organic vapor phase deposition, wherein the indium-containing layer is generated on a substrate in a reaction chamber, wherein the indium is delivered to the process in the form of an indium-containing precursor compound with the formula InR3, wherein the radicals R, independently of one another, are selected from alkyl radicals with 1 to 6 C atoms, characterized in that the delivery of the indium-containing precursor compound takes place in a solution that contains a solvent and the indium-containing precursor compound dissolved therein, wherein the solvent has at least one hydrocarbon with 1 to 8 carbon atoms.The invention also relates to a solution consisting of a compound of formula InR3, wherein R are selected independently of one another from alkyl radicals with 1 to 6 C atoms, and at least one hydrocarbon having 1 to 8 carbon atoms, uses of the solution for producing an indium-containing layer by metal-organic vapor deposition, and devices for executing the method.

    Perovskite Thin Film Low-pressure Chemical Deposition Equipment and Uses Thereof

    公开(公告)号:US20180233296A1

    公开(公告)日:2018-08-16

    申请号:US15944694

    申请日:2018-04-03

    Abstract: The present disclosure relates to perovskite thin film low-pressure chemical deposition equipment and a usage method thereof, and application of the usage method. The equipment comprises a main chamber, wherein two precursor heating plates and a substrate holddown groove are respectively arranged in the main chamber, the precursor heating plates are respectively provided with precursor containers, a plurality of groups of substrates on which a thin film is to be deposited are arranged on the substrate holddown groove, each group is provided with two substrates which are tightly attached back to back, and the surface of each of the two substrates on which a thin film is to be deposited faces towards one end of the main chamber; the left and right ends of the main chamber respectively communicate with carrier gas pipelines provided with carrier gas inlet mass flow control valves, the main chamber also communicates with a vacuum providing unit, and the main chamber is also provided with a main chamber heater for heating the substrates; and the carrier gas pipelines on the two ends respectively communicate with solvent evaporators. By adopting simultaneous introduction of the gas from the two ends of the main chamber and the substrate back-to-back configuration mode, the rate of preparing the perovskite thin film by the method is doubled as compared with the existing methods.

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