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    PRO-FRAGRANCE COMPOUNDS
    3.
    发明申请
    PRO-FRAGRANCE COMPOUNDS 有权
    PRO-FRAGRANCE化合物

    公开(公告)号：US20160122271A1

    公开(公告)日：2016-05-05

    申请号：US14889858

    申请日：2014-05-05

    申请人： FIRMENICH SA

    发明人： Brinda INDRADAS ,  Gilbert VIRTUCIO ,  Gary WOMACK

    IPC分类号： C07C43/166 ,  C07C43/215 ,  C11B9/00 ,  C11D3/50

    CPC分类号： C11B9/0061 ,  C07C29/50 ,  C07C43/166 ,  C07C43/215 ,  C07C43/23 ,  C07C45/36 ,  C07C45/37 ,  C07C2601/08 ,  C07C2601/16 ,  C11B9/0003 ,  C11B9/0015 ,  C11B9/0019 ,  C11D3/001 ,  C11D3/507 ,  C07C67/39 ,  C07C69/06 ,  C07C69/07 ,  C07C33/025 ,  C07C47/54 ,  C07C47/232 ,  C07C47/575 ,  C07C31/125 ,  C07C33/02 ,  C07C33/03 ,  C07C35/06 ,  C07C47/542 ,  C07C33/20

    摘要： A compound is provided of Formula (I), wherein R1 represents a C3 to C20 hydrocarbon group derived from an alcohol of formula R1OH, from a formate of formula R1OCH═O, or a cinnamyl aldehyde of Formula (II) wherein a compound of Formula I is capable of releasing a compound, when oxidized, selected from the group consisting of a fragrant alcohol of formula R1OH, a fragrant formate ester of formula R1OCH=0 and aryl aldehyde of Formula (III), wherein R2 is, independently, hydrogen atom, hydroxyl group, optionally substituted C1-C6 alkyl group, C1-C6 alkoxy group, or -0(C=0)CH(CH3)2 wherein any two of R2 may form an optionally substituted 5 or 6 membered ring. The compounds are useful for example as a precursor for the prolonged delivery or release of fragrant compounds such as fragrant alcohols, fragrant aldehydes or fragrant formates.

    摘要翻译： 由式（I）表示的化合物，其中R1表示衍生自式R1OH的醇，式R1OCH = O的甲酸酯或式（Ⅱ）的肉桂醛的C3至C20烃基，其中式 当氧化时，我能够释放化合物，其选自式为R1OH的芳香醇，式R1OCH = 0的芳香甲酸酯和式（III）的芳基醛，其中R2独立地为氢原子 ，羟基，任选取代的C 1 -C 6烷基，C 1 -C 6烷氧基或-O（C = O）CH（CH 3）2，其中任何两个R 2可以形成任选取代的5或6元环。 该化合物可用作例如芳香化合物如芳香醇，芳香醛或芳香甲酸酯延长递送或释放的前体。

    Process for preparing isopropanol and 2-butanol from the corresponding alkanes
    9.
    发明授权
    Process for preparing isopropanol and 2-butanol from the corresponding alkanes 失效
    从相应的烷烃制备异丙醇和2-丁醇的方法

    公开(公告)号：US07750194B2

    公开(公告)日：2010-07-06

    申请号：US12374351

    申请日：2007-07-16

    申请人： Georg Degen ,  Sven Crone ,  Ralf Boehling ,  Ansgar Gereon Altenhoff ,  Wolfgang Rohde ,  Jochen Buerkle ,  Goetz-Peter Schindler ,  Thomas Holtmann ,  Markus Schmitt

    发明人： Georg Degen ,  Sven Crone ,  Ralf Boehling ,  Ansgar Gereon Altenhoff ,  Wolfgang Rohde ,  Jochen Buerkle ,  Goetz-Peter Schindler ,  Thomas Holtmann ,  Markus Schmitt

    IPC分类号： C07C29/09

    CPC分类号： C07C67/04 ,  C07C29/095 ,  Y02P20/127 ,  C07C31/10 ,  C07C31/12 ,  C07C69/06 ,  C07C69/14

    摘要： A process for preparing alkanols (I) selected from the group consisting of isopropanol and 2-butanol from the corresponding alkanes (II) selected from the group consisting of propane and n-butane, comprising the steps of: A) providing a starting gas stream a comprising the alkane (II); B) feeding the starting gas stream a comprising the alkane (II) into a dehydrogenation zone and subjecting the alkane (II) to a dehydrogenation to the alkene (III) to obtain a product gas stream b comprising the alkene (III) and unconverted alkane (II), with or without high boilers, steam, hydrogen and low boilers; C) at least compressing product gas stream b, optionally separating product gas stream b into an aqueous phase c1, a phase c2 comprising the alkene (III) and the alkane (II), with or without high boilers, and a gas phase c3 comprising hydrogen and low boilers; D) reacting product gas stream b or the phase c2 comprising alkene (III) and alkane (II) with an organic acid (IV) in an esterification zone to obtain a product mixture d comprising the corresponding alkyl ester (V) of the organic acid and the unconverted alkane (II); E) removing from product mixture d a gas stream e1 which comprises an alkane (II) and is recycled into the dehydrogenation zone if appropriate, and a product mixture e2 comprising the alkyl ester; F) reacting the product mixture e2 comprising the alkyl ester with water in an ester hydrolysis zone to give a product mixture f comprising the alkanol (I) and the organic acid (IV); G) removing the alkanol (I) and the organic acid (IV) from product mixture f and, if appropriate, recycling the organic acid into the esterification zone.

    摘要翻译： 从选自丙烷和正丁烷的相应的烷烃（II）制备选自异丙醇和2-丁醇的链烷醇（I）的方法，包括以下步骤：A）提供起始气流 a包含烷烃（II）; B）将包含烷烃（II）的起始气体流（a）进料到脱氢区中并使烷烃（II）脱氢至烯烃（III），得到包含烯烃（III）和未转化烷烃的产物气流b （II），有或没有高锅炉，蒸汽，氢气和低锅炉; C）至少压缩产物气流b，任选地将产物气流b分离成水相c1，包含烯烃（III）和烷烃（II）的阶段c2，具有或不具有高锅炉，以及气相c3，其包含 氢和低锅炉; D）使产物气流b或包含烯烃（III）和烷烃（II）的相c与酯化区中的有机酸（IV）反应，得到包含相应的有机酸烷基酯（V）的产物混合物d 和未转化的烷烃（II）; E）从产物混合物d除去包含烷烃（II）的气流e1，并且如果合适的话再循环到脱氢区中，以及包含烷基酯的产物混合物e2; F）在酯水解区中使包含烷基酯的产物混合物e2与水反应，得到包含链烷醇（I）和有机酸（IV）的产物混合物f; G）从产物混合物f中除去链烷醇（I）和有机酸（IV），如果合适，将有机酸再循环到酯化区。