Process for preparing an acryloyloxysilane

    公开(公告)号:US10273254B2

    公开(公告)日:2019-04-30

    申请号:US15567272

    申请日:2016-06-17

    IPC分类号: C07F7/20 C07F7/18

    摘要: A process for preparing an acryloyloxysilane, comprising: reacting a metal salt of a carboxylic acid having the formula [CR22═CR1CO−]aMa+  (I), with a haloorganoalkoxysilane having the formula XR3Si(OR4)nR53-n  (II) at a temperature of from 50 to 160° C. and in the presence of a catalyst, and in the presence of water, an alcohol comprising 1 to 5 carbon atoms, or a combination of water and an alcohol comprising 1 to 5 carbon atoms, to form a mixture comprising an acryloyloxysilane and a metal halide having the formula Ma+X−a  (III), wherein R1 is H, R7COO−Ma+, or C1-C6 hydrocarbyl, each R2 is independently R1 or [COO−]Ma+, Ma+ is an alkali metal cation or alkaline earth metal cation, a is 1 or 2, X is halo, R3 is C1-C6 hydrocarbylene, each R4 is independently C1-C10 hydrocarbyl, each R5 is independently R1 and n is an integer from 1 to 3.

    Process for preparing an acryloyloxysilane

    公开(公告)号:US10246473B2

    公开(公告)日:2019-04-02

    申请号:US15567391

    申请日:2016-06-17

    IPC分类号: C07F7/20 C07F7/18

    摘要: A process for purifying an acryloyloxysilane comprising subjecting a mixture comprising an acryloyloxysilane, a haloorganoalkoxysilane, and an alkane-based non-polar solvent to a temperature and pressure sufficient to vaporize a portion of the non-polar solvent, the haloorganoalkoxysilane, or the non-polar solvent and the haloorganoalkoxysilane from the mixture to produce a purified mixture comprising the acryloyloxysilane. The examples disclose a three-step short-path distillation process, where in the first two passes, the residue-fraction is the one containing the product, whereas in the third path, the distillate is containing the purified product.

    THERMALLY BROKEN ANCHOR AND ASSEMBLY INCLUDING THE SAME

    公开(公告)号:US20170362816A1

    公开(公告)日:2017-12-21

    申请号:US15533782

    申请日:2015-12-16

    IPC分类号: E04B1/41 E04F13/08 E04B1/76

    摘要: An anchor for securing together interior and exterior building components includes a first end having an outer side for engaging the interior building component and an inner side opposite the outer side. The anchor further includes a second end having an outer side and an inner side opposite the outer side of the second end for engaging the exterior building component. A thermal break for reducing thermal bridging between the exterior and interior building components is disposed in a space between the inner sides of the ends and has a first coupling surface bonded to the inner side of the first end and a second coupling surface bonded to the inner side of the second end. An assembly includes the anchor for securing together the interior and exterior building components.