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公开(公告)号：US09266087B2
公开(公告)日：2016-02-23
申请号：US14077426
申请日：2013-11-12
IPC分类号： B01J20/18 , B01J20/22 , B01J31/22 , C01B39/48 , B01D53/02 , B01J29/70 , B01J29/76 , B01J29/78 , B01J35/00 , B01J35/10
CPC分类号： B01J20/226 , B01D53/02 , B01D2253/116 , B01D2256/245 , B01D2257/504 , B01J20/186 , B01J29/70 , B01J29/76 , B01J29/78 , B01J31/22 , B01J35/002 , B01J35/1014 , B01J35/1038 , C01B39/48 , Y02C10/08 , Y02P20/152
摘要： The present invention relates to molecular sieves having the structure of ITQ-32 is synthesized from a reaction mixture substantially free of fluoride ions and comprising 4,4-dimethyl, 1-cyclohexyl-piperazinium cations in its pore structure, as well as methods of making such molecular sieves and methods of using them.
摘要翻译： 本发明涉及具有ITQ-32结构的分子筛，其基本上不含氟离子的反应混合物，其孔结构中包含4,4-二甲基，1-环己基 - 哌嗪鎓阳离子，以及制备方法 这种分子筛和使用它们的方法。
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公开(公告)号：US20150087841A1
公开(公告)日：2015-03-26
申请号：US14541777
申请日：2014-11-14
IPC分类号： C07D453/02 , C07D211/12
CPC分类号： C07D453/02 , B01J29/70 , C01B39/04 , C01B39/48 , C07D211/12 , C07D295/037
摘要： A method of synthesizing a crystalline molecular sieve having an MSE framework type comprises crystallizing a reaction mixture comprising a source of water, a source of an oxide of a tetravalent element, Y, selected from at least one of silicon, tin, titanium, vanadium, and germanium, optionally a source of a trivalent element, X, a source of an alkali or alkaline earth metal, M, and a source of organic dications, Q, such as 3-hydroxy-1-(4-(1-methylpiperidin-1-ium-1-yl)butyl)quinuclidin-1-ium, 3-hydroxy-1-(5-(1-methylpiperidin-1-ium-1-yl)pentyl)quinuclidin-1-ium, 1,1′-(butane-1,4-diyl)bis(1-methylpiperidin-1-ium), 1,1′-(pentane-1,5-diyl)bis(1-methylpiperidin-1-ium), 1,1′-(hexane-1,6-diyl)bis(1-methylpiperidin-1-ium), and 1,1′-((3as,6as)-octahydropentalene-2,5-diyl)bis(1-methylpiperidin-1-ium).
摘要翻译： 合成具有MSE骨架类型的结晶分子筛的方法包括使包含水源，四价元素的氧化物源Y的反应混合物结晶，Y选自硅，锡，钛，钒， 和锗，任选的三价元素的源，X，碱金属或碱土金属的源，M和有机二价元素的Q，例如3-羟基-1-（4-（1-甲基哌啶-4-基） （1-（1-甲基哌啶-1-基）戊基）奎宁环ium，1,1'ium基-1- yl基）丁基）奎宁环ium，3-羟基-1- - （丁烷-1,4-二基）双（1-甲基哌啶-1-基），1,1' - （戊烷-1,5-二基）双（1-甲基哌啶-1-基），1,1' - （己烷-1,6-二基）双（1-甲基哌啶-1-基）和1,1' - （（3as，6as） - 八氢二烯-2,5-二基）双（1-甲基哌啶-1-基） ium）。
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公开(公告)号：US08025863B2
公开(公告)日：2011-09-27
申请号：US12214631
申请日：2008-06-20
CPC分类号： C07D295/023 , C01B37/02 , C01B39/48
摘要： A method of synthesizing a crystalline molecular sieve having an MSE framework type comprises crystallizing a reaction mixture comprising a source of water, a source of an oxide of a tetravalent element, Y, selected from at least one of silicon, tin, titanium, vanadium and germanium, a source of an alkali or alkaline earth metal, M, and a source of organic cations, Q, having the following general structure: in which R1 is hydrogen or an alkyl group, and R2 and R3 are alkyl groups.
摘要翻译： 合成具有MSE骨架类型的结晶分子筛的方法包括将包含水源，四价元素的氧化物源Y的反应混合物结晶，Y选自硅，锡，钛，钒和 锗，碱金属或碱土金属的源，M和有机阳离子源Q，具有以下一般结构：其中R1是氢或烷基，R2和R3是烷基。
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公开(公告)号：US20160031920A1
公开(公告)日：2016-02-04
申请号：US14736730
申请日：2015-06-11
申请人： Partha Nandi , Mobae Afeworki , Quddus Nizami , Simon C. Weston
发明人： Partha Nandi , Mobae Afeworki , Quddus Nizami , Simon C. Weston
CPC分类号： C07F15/025 , B01J20/226 , B01J31/1691 , C07F5/003 , C07F5/069
摘要： An imidazolate framework material comprises a general structure, M1-IM-M2, wherein IM is an imidazolate or a substituted imidazolate linking moiety, such as a 4,5-dicyanoimidazolate or a hydrolyzed or substituted 4,5 dicyanoimidazolate linking moiety, wherein M1 and M2 comprise the same or different metal cations, wherein at least one of M1 and M2 comprises a trivalent metal cation and wherein neither M1 nor M2 comprises a monovalent cation.
摘要翻译： 咪唑烷骨架材料包含一般结构M1-IM-M2，其中IM是咪唑酸酯或取代的咪唑酸酯连接部分，例如4,5-二氰基咪唑化物或水解或取代的4,5二氰基咪唑化物连接部分，其中M1和 M2包含相同或不同的金属阳离子，其中M1和M2中的至少一个包含三价金属阳离子，并且其中M1和M2都不包含一价阳离子。
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5.发明申请Molecular Sieve Composition (EMM-10-P), Its Method of Making, and Use for Hydrocarbon Conversions 有权分子筛组成（EMM-10-P），其制备和用于烃转化的方法公开(公告)号：US20120269718A1
公开(公告)日：2012-10-25
申请号：US13536159
申请日：2012-06-28
IPC分类号： C01B39/48
CPC分类号： C01B39/46 , B01J29/70 , B01J29/7038 , B01J29/7276 , B01J37/0009 , B01J2229/42 , C01B37/02 , C01B39/48 , C07C2/66 , C07C2/864 , C07C4/06 , C07C5/02 , C07C5/10 , C07C5/412 , C07C5/52 , C07C7/13 , C07C2529/70 , C07C2529/72 , C07C2529/74 , Y02P20/52 , Y10S208/02 , C07C15/085
摘要： This invention relates to a crystalline molecular sieve having, in its as-synthesized form, an X-ray diffraction pattern including d-spacing maxima at 13.18±0.25 and 12.33±0.23 Angstroms, wherein the peak intensity of the d-spacing maximum at 13.18±0.25 Angstroms is at least as great as 90% of the peak intensity of the d-spacing maximum at 12.33±0.23 Angstroms. This invention also relates to a method of making thereof.
摘要翻译： 本发明涉及一种结晶分子筛，其以其合成形式具有包括在13.18±0.25和12.33±0.23埃处的d间距最大值的X射线衍射图，其中d间距最大值的峰值强度为13.18 ±0.25埃至少高达12.33±0.23埃处d间距最大峰值强度的90％。 本发明还涉及其制备方法。
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公开(公告)号：US6049018A
公开(公告)日：2000-04-11
申请号：US234544
申请日：1999-01-21
申请人： David C. Calabro , Jane C. Cheng , Robert A. Crane, Jr. , Charles T. Kresge , Sandeep S. Dhingra , Michael A. Steckel , David L. Stern , Simon C. Weston
发明人： David C. Calabro , Jane C. Cheng , Robert A. Crane, Jr. , Charles T. Kresge , Sandeep S. Dhingra , Michael A. Steckel , David L. Stern , Simon C. Weston
IPC分类号： C07D487/04 , B01J29/04 , B01J29/70 , C01B39/08 , C01B39/46 , C01B39/48 , C07B61/00 , C07C2/54 , C07C2/66 , C07C4/18 , C07C5/22 , C07C5/27 , C07C6/12 , C07C15/073 , C07C15/085 , C07D209/56 , C07D487/00 , C01B39/50
CPC分类号： C07C6/126 , B01J29/04 , B01J29/70 , C01B39/085 , C01B39/48 , C07C2/66 , C07C4/18 , C07C5/2708 , C07C6/123 , C07C2529/70
摘要： This invention relates to a new synthetic porous crystalline material, designated MCM-68, a method and novel polycyclic organic cation for its preparation and its use in catalytic conversion of organic compounds. The new crystalline material exhibits a distinctive X-ray diffraction pattern and has a unique crystal structure which contains at least one channel system, in which each channel is defined by a 12-membered ring of tetrahedrally coordinated atoms, and at least two further, independent channel systems, in each of which each channel is defined by a 10-membered ring of tetrahedrally coordinated atoms, wherein the number of unique 10-membered ring channels is twice the number of 12-membered ring channels.
摘要翻译： 本发明涉及一种新的合成多孔结晶材料，称为MCM-68，其制备方法和新型多环有机阳离子及其在有机化合物催化转化中的应用。 新的结晶材料表现出独特的X射线衍射图案，并且具有独特的晶体结构，其包含至少一个通道系统，其中每个通道由四面体配位的原子的12元环定义，并且至少两个独立的 通道系统，其中每个通道由四面体配位原子的10元环定义，其中唯一的10-元环通道的数目是12元环通道数目的两倍。
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7.发明授权Integration of pressure swing adsorption with a power plant for CO2 capture/utilization and N2 production 有权将变压吸附与发电厂整合，用于CO2捕集/利用和N2生产公开(公告)号：US09476356B2
公开(公告)日：2016-10-25
申请号：US13917101
申请日：2013-06-13
申请人： Narasimhan Sundaram , Ramesh Gupta , Hans Thomann , Hugo S. Caram , Loren K. Starcher , Franklin F. Mittricker , Simon C. Weston , Scott J. Weigel
发明人： Narasimhan Sundaram , Ramesh Gupta , Hans Thomann , Hugo S. Caram , Loren K. Starcher , Franklin F. Mittricker , Simon C. Weston , Scott J. Weigel
IPC分类号： F02C6/04 , F02C3/34 , B01D53/047
CPC分类号： F02C3/34 , B01D53/047 , B01D2253/1124 , B01D2256/10 , B01D2257/504 , B01D2258/0283 , B01D2259/40056 , F01K17/04 , F02C6/04 , F02C9/16 , F05D2220/31 , F05D2220/32 , F05D2260/61 , F23J2215/50 , Y02C10/04 , Y02C10/08 , Y02E20/14 , Y02E20/16
摘要： Systems and methods are provided for combined cycle power generation while reducing or mitigating emissions during power generation. Recycled exhaust gas from a power generation combustion reaction can be separated using a swing adsorption process so as to generate a high purity CO2 stream while reducing/minimizing the energy required for the separation and without having to reduce the temperature of the exhaust gas. This can allow for improved energy recovery while also generating high purity streams of carbon dioxide and nitrogen.
摘要翻译： 提供系统和方法用于联合循环发电，同时减少或减少发电过程中的排放。 来自发电燃烧反应的回收废气可以使用回转吸附法分离，以产生高纯度CO 2流，同时减少/最小化分离所需的能量，而不必降低废气的温度。 这可以改善能量回收同时产生高纯度的二氧化碳和氮气流。
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公开(公告)号：US08562941B2
公开(公告)日：2013-10-22
申请号：US11637347
申请日：2006-12-12
CPC分类号： C01B39/02 , C01B37/00 , C01B39/026 , C01B39/04 , C01B39/265 , C01B39/42 , C01B39/44 , C01B39/48 , C01B39/54
摘要： The present invention is a method that perturbs the initial crystallization of a material from a less desired phase into a more desired phase. More specifically, the present invention is a method to form a different crystallization of a zeolite, mesoporous material, SAPO4, AlPO4 or porous inorganic oxide after the hydrothermal synthesis has started and a precursor crystalline phase has formed.
摘要翻译： 本发明是一种将材料从不太期望的阶段初始结晶化到更期望的阶段的方法。 更具体地，本发明是在水热合成开始并形成前体结晶相之后形成沸石，介孔材料，SAPO 4，AlPO 4或多孔无机氧化物的不同结晶的方法。
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9.发明申请Molecular Sieve Composition (EMM-10-P), Its Method of Making, and Use for Hydrocarbon Conversions 审中-公开分子筛组成（EMM-10-P），其制备和用于烃转化的方法公开(公告)号：US20110190114A1
公开(公告)日：2011-08-04
申请号：US13004991
申请日：2011-01-12
CPC分类号： C01B39/46 , B01J29/70 , B01J29/7038 , B01J29/7276 , B01J37/0009 , B01J2229/42 , C01B37/02 , C01B39/48 , C07C2/66 , C07C2/864 , C07C4/06 , C07C5/02 , C07C5/10 , C07C5/412 , C07C5/52 , C07C7/13 , C07C2529/70 , C07C2529/72 , C07C2529/74 , Y02P20/52 , Y10S208/02 , C07C15/085
摘要： This invention relates to a crystalline molecular sieve having, in its as-synthesized form, an X-ray diffraction pattern including d-spacing maxima at 13.18±0.25 and 12.33±0.23 Angstroms, wherein the peak intensity of the d-spacing maximum at 13.18±0.25 Angstroms is at least as great as 90% of the peak intensity of the d-spacing maximum at 12.33±0.23 Angstroms. This invention also relates to a method of making thereof.
摘要翻译： 本发明涉及一种结晶分子筛，其以其合成形式具有包括在13.18±0.25和12.33±0.23埃处的d间距最大值的X射线衍射图，其中d间距最大值的峰值强度为13.18 ±0.25埃至少高达12.33±0.23埃处d间距最大峰值强度的90％。 本发明还涉及其制备方法。
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公开(公告)号：US20090318696A1
公开(公告)日：2009-12-24
申请号：US12214631
申请日：2008-06-20
IPC分类号： C07D241/04 , B01J29/06
CPC分类号： C07D295/023 , C01B37/02 , C01B39/48
摘要： A method of synthesizing a crystalline molecular sieve having an MSE framework type comprises crystallizing a reaction mixture comprising a source of water, a source of an oxide of a tetravalent element, Y, selected from at least one of silicon, tin, titanium, vanadium and germanium, a source of an alkali or alkaline earth metal, M, and a source of organic cations, Q, having the following general structure: in which R1 is hydrogen or an alkyl group, and R2 and R3 are alkyl groups.
摘要翻译： 合成具有MSE骨架类型的结晶分子筛的方法包括将包含水源，四价元素的氧化物源Y的反应混合物结晶，Y选自硅，锡，钛，钒和 锗，碱金属或碱土金属的源，M和有机阳离子源Q，具有以下一般结构：其中R1是氢或烷基，R2和R3是烷基。
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