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    Low-fluoride, reactive polyisobutylene
    14.
    发明授权
    Low-fluoride, reactive polyisobutylene 有权

    公开(公告)号：US09617363B1

    公开(公告)日：2017-04-11

    申请号：US15059589

    申请日：2016-03-03

    申请人： TPC Group LLC

    发明人： Rajeev Kumar ,  André M Gobin ,  Wayne Ouellette ,  Michael O. Nutt ,  Leonard M. Czupski ,  Peggy J. Macatangay

    IPC分类号： C08F2/00 ,  C08F4/00 ,  C08F210/00 ,  C08F110/10 ,  B01J19/18

    CPC分类号： C08F110/10 ,  B01J4/001 ,  B01J19/18 ,  B01J2219/00094 ,  B01J2219/00768 ,  C08F2500/02 ,  C08F4/14

    摘要： A method of making a low-fluoride reactive PIB composition includes (a) providing a modified C4 feedstock by way of blending a mixed C4 feedstock with a second feedstock having a lower LB/IsoB ratio; or providing a C4 feedstock with an LB/IsoB index of less than 10%; (b) feeding the modified C4 feedstock or the C4 feedstock with an LB/IsoB index of less than 10% to a CSTR with a homogeneous catalyst comprising BF3 and a modifier selected from alcohols, ethers and mixtures thereof; (c) polymerizing the modified C4 feedstock or the C4 feedstock with an LB/IsoB index of less than 10% in the reactor while maintaining the reactor at a temperature above −15° C. and utilizing a residence time less than 45 minutes to produce a crude PIB composition in a polymerization mixture; and (d) recovering a purified PIB composition from the polymerization mixture having a molecular weight, Mn, from 250 to 5000 Daltons and an alpha vinylidene content of at least 50 mol %. The crude PIB composition suitably has a fluoride content of less than 100 ppm and the purified PIB composition has a fluoride content of less than 20 ppm in preferred embodiments. In the most preferred embodiments, ammonium salts are used to neutralize the catalyst and fluoride salts are sublimed from the product at elevated temperatures.

    Injection Device, in Particular For Injecting a Hydrocarbon Feedstock into a Refining Unit
    15.
    发明申请
    Injection Device, in Particular For Injecting a Hydrocarbon Feedstock into a Refining Unit 审中-公开
    注射装置，特别是用于将烃原料注入精炼装置

    公开(公告)号：US20170043311A1

    公开(公告)日：2017-02-16

    申请号：US15306877

    申请日：2015-04-27

    申请人： Total Raffinage Chimie

    发明人： Romain Lesage

    IPC分类号： B01J8/24 ,  C10G11/00 ,  B01J4/00

    CPC分类号： B01J8/24 ,  B01J4/001 ,  B01J2208/00902 ,  C10G11/00

    摘要： Embodiments of an injection device shaped in order to atomize a liquid into droplets by means of a gas are disclosed herein. The injection device may comprise a body having a gas inlet orifice intended to be connected to a gas supply duct. The injection device may further comprise an outlet orifice for discharging the atomized liquid. The injection device may also comprise a straight internal duct connecting the inlet orifice to the outlet orifice along an axial direction of said body. At least two liquid inlet ducts may be intended to be connected to at least one liquid supply duct pass through said body radially or substantially radially and open into said internal duct. These liquid inlet ducts may each have an axis and are arranged so that their axes intersect at one and the same point on an axial line extending inside the internal duct.

    摘要翻译： 本文公开了通过气体将液体雾化成液滴而成形的注射装置的实施方案。 注射装置可以包括具有旨在连接到气体供应管道的气体入口孔的主体。 注射装置还可以包括用于排出雾化液体的出口孔。 注射装置还可以包括沿着所述主体的轴向方向将入口孔连接到出口孔的直的内部管道。 至少两个液体入口管道可以被连接到至少一个液体供应管道，径向地或基本上径向地穿过所述主体并且打开到所述内部管道中。 这些液体入口管道可以各自具有轴线并且被布置成使得它们的轴线在在内部管道内部延伸的轴线上的同一点相交。

    Process and device for unloading particulate material from a vessel
    17.
    发明授权
    Process and device for unloading particulate material from a vessel 有权
    从容器中卸载颗粒材料的工艺和装置

    公开(公告)号：US09446362B2

    公开(公告)日：2016-09-20

    申请号：US14021191

    申请日：2013-09-09

    申请人： PETROVAL

    发明人： Adriaan Stander

    IPC分类号： B65G53/00 ,  B01J4/00 ,  B01J8/00 ,  B65G53/42

    CPC分类号： B01J4/001 ,  B01J8/004 ,  B01J2208/00761 ,  B65G53/42 ,  Y10T137/0318 ,  Y10T137/8593

    摘要： The present invention concerns a process for unloading a bed (2) of particulate material from a vessel (1), which comprises inserting a removable and portable extraction pipe (4) into the lower part of said bed, injecting a fluidization gas upwardly into the extraction pipe (4) from the bottom part thereof, along the entire length of the extraction pipe (4), and applying a positive pressure differential between the inlet and the outlet of said extraction pipe.The present invention further concerns a device suitable for implementing such a process.

    摘要翻译： 本发明还涉及适于实现这种过程的设备。

    Continuous polymerization device, method for producing polymer composition, and injection valve
    19.
    发明授权
    Continuous polymerization device, method for producing polymer composition, and injection valve 有权
    连续聚合装置，聚合物组合物的制造方法和喷射阀

    公开(公告)号：US09403922B2

    公开(公告)日：2016-08-02

    申请号：US14764890

    申请日：2014-01-15

    申请人： SUMITOMO CHEMICAL COMPANY, LIMITED

    发明人： Masakazu Sumida ,  Kazuhiro Yamazaki ,  Akira Nishitani

    IPC分类号： C08F2/01 ,  B01J19/18 ,  B01J19/24 ,  F16K1/36 ,  F16K21/02 ,  C08F20/10

    CPC分类号： C08F20/10 ,  B01J4/001 ,  B01J19/1862 ,  B01J19/245 ,  B01J2204/002 ,  B01J2219/00058 ,  B01J2219/00103 ,  B01J2219/24 ,  C08F2/01 ,  F16K1/36

    摘要： A continuous polymerization apparatus uses at least a first reactor and a second reactor (10, 20). Each of the reactors (10, 20) comprises a supply port (11a, 21a) and an effluent port (11b, 21b). The supply port (11a) of the first reactor (10) is connected to supply sources (1, 3) of a raw material monomer and a polymerization initiator, and the effluent port (11b) thereof is connected to the supply port (21a) of the second reactor (20) by a connection line (15a). The connection line (15a) is combined with a replenishing line (15b) through an injection valve (50) at a combining part. The injection valve (50) comprises, in a full closure state thereof, a clearance that may cause a fluid comprising at least the raw material monomer to flow from the replenishing line (15b) to the connection line (15a).

    摘要翻译： 连续聚合装置使用至少第一反应器和第二反应器（10,20）。 每个反应器（10,20）包括供给口（11a，21a）和排出口（11b，21b）。 第一反应器（10）的供给口（11a）与原料单体和聚合引发剂的供给源（1,3）连接，其排出口（11b）与供给口（21a）连接， 的第二反应器（20）通过连接管线（15a）。 连接线（15a）通过组合部分处的喷射阀（50）与补充线（15b）组合。 注射阀（50）在其完全关闭状态下包括可能导致至少包含原料单体的流体从补充管线（15b）流向连接管线（15a）的间隙。

    DEVICE FOR SYNTHESIZING A POLYMER WITH REDUCED FORMATION OF DEPOSITS IN THE REACTION CHAMBER
    20.
    发明申请
    DEVICE FOR SYNTHESIZING A POLYMER WITH REDUCED FORMATION OF DEPOSITS IN THE REACTION CHAMBER 有权

    公开(公告)号：US20160130398A1

    公开(公告)日：2016-05-12

    申请号：US14897020

    申请日：2014-06-11

    申请人： BASF SE

    发明人： Ning Zhu ,  Achim Stammer ,  Joachim Clauss ,  Uwe Witt ,  Gad Kory ,  Silke Biedasek

    IPC分类号： C08G69/46 ,  C08G69/28 ,  C08G69/04 ,  C08G69/26

    CPC分类号： C08G69/46 ,  B01J4/001 ,  B01J19/0026 ,  B01J19/0066 ,  B01J19/20 ,  B01J2219/00168 ,  B01J2219/00247 ,  C08F2/002 ,  C08F2/005 ,  C08G69/04 ,  C08G69/265 ,  C08G69/28 ,  C08L77/06

    摘要： The invention relates to a device for synthesizing a polymer accompanied by separating a gaseous substance. Said device comprises: a reactor chamber (1) having a substantially circular cylinder-shaped upper section (11), which is delimited by two circular surfaces (111, 112) and a circumferential surface (113) and has a longitudinal cylinder axis, and a lower section (12), the upper section (11) and the lower section (12) being connected to one another via the first circular surface (111); an inlet opening (2); a first outlet opening (3), which is arranged in a wall of the lower section (12); a second outlet opening (4), which is arranged in the second circular surface (112) or in the circumferential surface (113) between the inlet opening (2) and the second circular surface (112); and a removal device (51), which is arranged so as to be movable along the longitudinal cylinder axis at least between the second circular surface (112) and the inlet opening (2), and contacts the circumferential surface (113). The invention further relates to a method comprising: feeding an oligomer melt (7) into a circular cylinder-shaped first section (11) of a reaction chamber (1) through an inlet opening (2) tangentially to a circumferential surface (113) of the first section (11); polymerizing the oligomer melt (7) to form a polymer melt (8); removing the polymer melt (8) from the reaction chamber (1) through a first outlet opening (3) of the reaction chamber (1); and removing a gaseous substance (9) from the reaction chamber (1) through a second outlet opening (4) of the reaction chamber (1) above the inlet opening (2). Deposits on at least one inner wall of the first section (11) of the reaction chamber (1) above the inlet opening (2) are removed by a removal device (51).