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公开(公告)号：US20240279560A1
公开(公告)日：2024-08-22
申请号：US18587678
申请日：2024-02-26
Inventor： Jack Lawrence Waldron , Kylen J. Smith
CPC classification number: C10G27/12 , B01J14/00 , B01J19/242 , B01J19/246 , B01J2219/00006 , B01J2219/00033 , B01J2219/00479 , B01J2219/3325
Abstract: A reaction column comprises a plurality of cells each of which has a lower cell portion and an upper cell portion. The cells are arranged sequentially, from an uppermost cell to a lowermost cell. The fuel inlet is configured to direct fluid through the reaction column from a lower cell portion of the lowermost cell to an upper cell portion of the uppermost cell, and out of the fuel outlet. The reagent inlet is configured to direct reagent through the reaction column from the upper cell portion of the uppermost cell to the lower cell portion of the lowermost cell. The plurality of cells may be vertically or horizontally positioned, as well as inclined and the like. Systems and methods are likewise disclosed.
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公开(公告)号：US20240043463A1
公开(公告)日：2024-02-08
申请号：US18380664
申请日：2023-10-17
Applicant: CONTEMPORARY AMPEREX TECHNOLOGY CO., LIMITED
Inventor： Shaojun LIU , Wenwei ZHAN , Xinxin ZHANG , Chuying OUYANG , Qingzheng LI
CPC classification number: C07F19/00 , H01M4/5825 , C01B25/45 , B01J14/00 , B01J19/245 , B01J19/06 , B01J19/10 , B01J19/0013 , H01M2004/028
Abstract: A continuous reaction system for preparing a ferromanganese oxalate precursor may comprise a first dissolution reactor, a second dissolution reactor, a first reactor, a second reactor, a material storage tank, and an ultrasonic reactor; the first dissolution reactor may be configured to accommodate a metal salt solution required for preparing the ferromanganese oxalate precursor, and the second dissolution reactor may be configured to accommodate a precipitant solution required for preparing the ferromanganese oxalate precursor; the first reactor may include a first feed port and a first overflow port, and the first feed port of the first reactor may be interconnected to a first discharge port of the first dissolution reactor and a second discharge port of the second dissolution reactor respectively through two pipelines.
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公开(公告)号：US20190241483A1
公开(公告)日：2019-08-08
申请号：US16386974
申请日：2019-04-17
Applicant: NOVA Chemicals (International) S.A.
Inventor： Stephen Brown , Peter Zoricak , Eric Clavelle
CPC classification number: C07C2/32 , B01J8/10 , B01J14/00 , B01J19/002 , B01J19/0066 , B01J19/18 , B01J2208/00867 , B01J2219/00033 , B01J2219/00247 , B01J2219/00252 , B01J2219/0099 , C07C2/36 , C07C2531/14 , C07C2531/22 , C07C2531/24 , C07C2531/34 , C08F10/02 , C08F2/002 , C08F2/01 , C08F210/16 , C08F210/14 , C08F2500/02 , C07C11/107 , C07C11/02
Abstract: This invention relates to a self cleaning reactor and to a process for the oligomerization of ethylene that employs a self-cleaning reactor. The reactor includes a mass of inert, particulate cleaning bodies that are entrained by the liquid in the reactor and scour the internal surfaces of the reactor during normal operation. This scouring action reduces the level of fouling on the reactor surfaces. Foulant material (polyethylene) is removed from the process on a continuous basis but the cleaning bodies remain within the reactor.
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公开(公告)号：US10081005B2
公开(公告)日：2018-09-25
申请号：US14777973
申请日：2014-03-26
Applicant: THE REGENTS OF THE UNIVERSITY OF CALIFORNIA
Inventor： Melissa Moore , R. Michael Van Dam , Kevin Quinn , Shane Claggett , Henry Herman , Mark Lazari
CPC classification number: B01J19/004 , B01J14/00 , B01J19/0093 , B01J2219/00799 , B01J2219/00801 , B01J2219/00813 , B01J2219/00815 , B01J2219/00817 , B01J2219/00831 , B01J2219/00873 , B01J2219/00889 , B01J2219/00909 , B01J2219/00918 , B01J2219/0097 , B01J2219/00986 , C07H17/02
Abstract: An automated radiosynthesizer device includes a plurality of reactor assemblies, each reactor assembly being operatively connected to a horizontal actuator for moving the reactor assembly in the horizontal direction and a vertical actuator for moving the reactor assembly in the vertical direction. A plurality of disposable cassettes are disposed above each of the plurality of reactor assemblies, each cassette comprising a lower surface comprising a plurality of sealed and un-sealed gaskets, wherein the un-sealed gaskets are connected to internal fluid paths within the cassette. The device includes a three-axis reagent and gas handling robot disposed above the plurality of cassettes and terminates in a vial gripper and a gas manifold having an inert gas port and a vacuum port. The device includes a control system configured to control the horizontal actuator and vertical actuator of each reactor assembly and the three-axis reagent and gas handling robot.
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公开(公告)号：US09944753B2
公开(公告)日：2018-04-17
申请号：US15037633
申请日：2014-11-20
Applicant: Ernest Keith Marchildon , Karen A. Surgenor , Bryan D. Kaushiva
Inventor： Ernest Keith Marchildon , Karen A. Surgenor , Bryan D. Kaushiva
CPC classification number: C08G69/28 , B01J4/002 , B01J10/002 , B01J14/00 , B01J19/0006 , B01J19/006 , B01J19/0066 , B01J19/18 , B01J19/245 , B01J2219/00186 , B01J2219/002 , B01J2219/00202 , B01J2219/00231 , C08L77/00
Abstract: A continuous process for the manufacture of a polyamide, the process comprising the steps of: (i) flowing a stream A comprising a molten dicarboxylic acid, or a molten dicarboxylic acid-rich mixture comprising a dicarboxylic acid and a diamine, through a first stage and at least one more reaction stage of a vertical multistage reactor, wherein the first stage is at the top of the reactor; (ii) counter-currently flowing a stream B comprising a diamine as either a vapor or a diamine-rich liquid through at least one of the stages below the first reaction stage of said vertical multistage reactor; (iii) accumulating a liquid phase material P comprising polyamide at and/or below the final stage of said reactor; wherein said reactor is equipped with internal features suitable for effecting contact between counter-currently flowing streams A and B; and wherein said process further comprises the step of agitating said liquid phase material P by injecting a gaseous stream C comprising steam, or at least one inert gas, or a mixture of steam and at least one inert gas into the reactor at or below the final stage of the reactor. The invention further provides a vertical multistage reactor configured to implement said process.
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Patent Agency Ranking
公开(公告)号：US20180098537A1
公开(公告)日：2018-04-12
申请号：US15836368
申请日：2017-12-08
Applicant: Ecolab USA Inc.
Inventor： PAUL R. KRAUS , THOMAS C. RUSTAD
IPC: A01N37/16
CPC classification number: A01N37/16 , A01N37/02 , A01N59/00 , A61L2/18 , A61L2/186 , A61L2/24 , A61L2202/14 , B01J4/001 , B01J4/008 , B01J14/00 , B01J19/0006 , B01J19/0013 , B01J19/24 , B01J2219/00049 , B01J2219/00121 , B01J2219/00159 , B01J2219/24 , C02F1/50 , C02F1/722 , C02F2103/08 , C07C407/00 , C07C409/24 , A01N2300/00
Abstract: Methods and systems for on-site, continuous generation of peracid chemistry, namely peroxycarboxylic acids and peroxycarboxylic acid forming compositions, are disclosed. In particular, an adjustable biocide formulator or generator system is designed for on-site generation of peroxycarboxylic acids and peroxycarboxylic acid forming compositions from sugar esters. Methods of using the in situ generated peroxycarboxylic acids and peroxycarboxylic acid forming compositions are also disclosed.
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公开(公告)号：US20180079713A1
公开(公告)日：2018-03-22
申请号：US15820632
申请日：2017-11-22
Applicant: Arkema France
Inventor： Yves Bernardin , Xavier MARCARIAN , Romain BILLON
IPC: C07C231/12 , C07C305/06 , B01J14/00 , C07C235/06 , C07C233/09 , C07C231/06 , C07C69/54 , C07C67/20 , C07C57/04 , C07C51/08 , C07C303/24 , B01J19/00 , B01J19/02 , B01J19/24
CPC classification number: C07C231/12 , B01J14/00 , B01J19/0013 , B01J19/002 , B01J19/006 , B01J19/02 , B01J19/245 , B01J19/249 , B01J2219/0004 , B01J2219/00058 , B01J2219/00063 , B01J2219/00065 , B01J2219/00162 , B01J2219/00166 , B01J2219/00182 , B01J2219/0027 , B01J2219/00272 , B01J2219/00768 , B01J2219/0286 , B01J2219/029 , B01J2219/182 , B01J2219/1943 , B01J2219/2475 , C07C51/08 , C07C57/04 , C07C67/20 , C07C69/54 , C07C231/06 , C07C233/09 , C07C235/06 , C07C303/24 , C07C305/06
Abstract: The invention relates to a thermal conversion vessel (200) used during amidification step of acetone cyanohydrin (ACH), in the industrial process for production of a methyl methacrylate (MMA) or methacrylic acid (MAA). The thermal conversion vessel (200) is used for converting an hydrolysis mixture of α-hydroxyisobutyramide (HIBAM), α-sulfatoisobutyramide (SIBAM), 2-methacrylamide (MACRYDE) and methacrylique acid (MAA), into a mixture of 2-methacrylamide (MACRYDE). It comprises: at least one compartment (C1, C2, C3, . . . Ci) comprising an inner wall (206a, 206b, 206i) separating said compartment into two communicating parts (C1a, C1b) by a passage provided between the bottom of said vessel and said inner wall, said compartment having a space above said inner wall, for separating gas phase from liquid phase during thermal conversion, said compartment being connected to an outlet valve (204a, 204b, . . . 204i). Such vessel allows obtaining a high yield thermal conversion in very safe conditions.
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公开(公告)号：US09861101B2
公开(公告)日：2018-01-09
申请号：US15154283
申请日：2016-05-13
Applicant: ECOLAB USA INC.
Inventor： Paul R. Kraus , Thomas C. Rustad
IPC: A61L9/00 , A61L2/00 , A61L9/01 , B08B3/00 , A01N37/16 , C02F1/50 , C07C407/00 , A01N59/00 , B01J19/00 , B01J4/00 , A61L2/24 , C07C409/24 , A61L2/18 , B01J19/24 , B01J14/00 , C02F1/72 , C02F103/08
CPC classification number: A01N37/16 , A01N37/02 , A01N59/00 , A61L2/18 , A61L2/186 , A61L2/24 , A61L2202/14 , B01J4/001 , B01J4/008 , B01J14/00 , B01J19/0006 , B01J19/0013 , B01J19/24 , B01J2219/00049 , B01J2219/00121 , B01J2219/00159 , B01J2219/24 , C02F1/50 , C02F1/722 , C02F2103/08 , C07C407/00 , C07C409/24 , A01N2300/00
Abstract: Methods and systems for on-site, continuous generation of peracid chemistry, namely peroxycarboxylic acids and peroxycarboxylic acid forming compositions, are disclosed. In particular, an adjustable biocide formulator or generator system is designed for on-site generation of peroxycarboxylic acids and peroxycarboxylic acid forming compositions from sugar esters. Methods of using the in situ generated peroxycarboxylic acids and peroxycarboxylic acid forming compositions are also disclosed.
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公开(公告)号：US09731967B1
公开(公告)日：2017-08-15
申请号：US15382418
申请日：2016-12-16
Applicant: Jerry M Woodall , Thomas E. Rowley
Inventor： Jerry M Woodall , Thomas E. Rowley
CPC classification number: C01B3/08 , B01J7/02 , B01J14/00 , B01J19/002 , B01J2219/00272 , C01F7/42 , C01F7/428
Abstract: A system for producing hydrogen gas, heat and an oxide component using a water splitting process is disclosed. The system involves a dry first chamber containing a passivating-oxide preventing reagent that receives a solid material feedstock and dissolves the solid material feedstock in the passivating-oxide preventing reagent. The passivating-oxide preventing reagent becomes saturated with the solid material in the first chamber and is then transferred to a second chamber without contact with water. In the second chamber, the solid material saturated in the passivating-oxide preventing reagent reacts with the water so as to generate hydrogen gas, an oxide component and heat. Following the reaction, the solid material depleted passivating-oxide preventing reagent and water is recycled to be re-used in the water splitting process.
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10.发明申请公开(公告)号：US20170044021A1
公开(公告)日：2017-02-16
申请号：US15306491
申请日：2014-09-12
Applicant: Nanjing University of Technology
Inventor： Weihong XING , Zhilong XU , Nanping XU , Zhaoxiang ZHONG , Feng ZHANG
CPC classification number: C01G9/02 , B01J14/00 , B01J19/2415 , B01J19/2475 , B01J2219/00033 , B82Y30/00 , C01P2002/72 , C01P2004/03
Abstract: The present invention relaters to a method for continuously preparing a nano zinc oxide with a membrane reactor. A zinc salt solution and a precipitator solution required for the preparation of a zinc oxide are respectively used as dispersion phases, and under the action of a certain pressure, the two reaction solutions respectively penetrate through a membrane tube at a certain rate and disperse quickly under the action of a shear force and react, producing a precursor precipitate. A precursor suspension penetrates through the membrane tube continuously and circularly after being pressurized by a pump, and at the same time, deionized water as a washing fluid is added to a suspension storage tank, wherein impurity ions penetrate through membrane pores and are discharged along with the liquid medium; after the concentration of the impurity ions meets requirements, the concentrated solution is discharged continuously and then spray-dried to obtain a basic zinc carbonate precursor powder. The basic zinc carbonate powder is calcined under certain conditions to obtain the nanostructured zinc oxide powder. The continuous preparation and washing of a powder can be achieved by coupling a membrane washing technique with a membrane dispersion technique. The procedure is simple, the structure of zinc oxide is easy to control and the yield is high.
Abstract translation: 本发明涉及一种用膜反应器连续制备纳米氧化锌的方法。 分别使用锌盐溶液和制备氧化锌所需的沉淀剂溶液作为分散相，并且在一定压力的作用下，两种反应溶液分别以一定速率穿过膜管并快速分散在 剪切力的作用并反应，产生前体沉淀。 前驱体悬浮液在被泵加压之后，连续循环地穿过膜管，同时将去离子水作为洗涤液加入到悬浮储罐中，其中杂质离子穿过膜孔并与 液体介质; 杂质离子浓度满足要求后，浓缩溶液连续排出，然后喷雾干燥，得到碱式碳酸锌前体粉末。 碱性碳酸锌粉末在一定条件下煅烧得到纳米结构氧化锌粉末。 通过将膜洗涤技术与膜分散技术结合可以实现粉末的连续制备和洗涤。 操作简单，氧化锌结构易于控制，产量高。
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