-
公开(公告)号:US11229893B2
公开(公告)日:2022-01-25
申请号:US16239845
申请日:2019-01-04
发明人: Yasuyuki Fukushima , Kozue Akazaki , Yasutomo Tanaka , Kazuma Akikubo , Takeshi Nakamura , Yukihiro Shimogaki , Takeshi Momose , Noboru Sato , Kohei Shima , Yuichi Funato
IPC分类号: B01J12/00 , C04B35/565 , C01B33/107 , C01B32/977 , C23C16/42 , C01B32/963 , C23C16/32
摘要: Provided is a method of producing a silicon compound material, including the steps of: storing a silicon carbide preform in a reaction furnace; supplying a raw material gas containing methyltrichlorosilane to the reaction furnace to infiltrate the preform with silicon carbide; and controlling and reducing a temperature of a gas discharged from the reaction furnace at a predetermined rate to subject the gas to continuous thermal history, to thereby decrease generation of a liquid or solid by-product derived from the gas.
-
公开(公告)号:US11142820B2
公开(公告)日:2021-10-12
申请号:US16250488
申请日:2019-01-17
发明人: Xiaoyue Huang , Deming Zhang , Minna Hovinen , Ziyou Zhou
IPC分类号: C23C16/32 , G02B6/02 , C01B32/963 , C23C16/453
摘要: In a method for depositing a layer of amorphous hydrogenated silicon carbide (SiC:H), a gas mixture comprising a reactive gas to inert gas volume ratio of 1:12 to 2:3 is introduced into a reaction chamber of a plasma-enhanced chemical vapor deposition apparatus. The reactive gas has a ratio of Si of 50 to 60, C of 3 to 13, and H of 32 to 42 at %. The inert gas comprises i) a first inert gas selected from helium, neon and mixtures; and ii) a second inert gas selected from argon, krypton, xenon and mixtures. The reaction plasma is at a power frequency of 1-16 MHz at a power level of 100 W to 700 W. The resulting layer exhibits a refractive index of not less than 2.4 and a loss of not more than 180 dB/cm at an indicated wavelength within 800 to 900 nm.
-
公开(公告)号:US11052647B2
公开(公告)日:2021-07-06
申请号:US15976753
申请日:2018-05-10
发明人: David Glen Findley
IPC分类号: B33Y10/00 , H01L21/02 , C30B7/14 , H01L23/15 , B33Y30/00 , C30B29/36 , C30B29/04 , B28B1/00 , B33Y70/00 , C01B32/26 , C09D11/037 , C01B32/963 , C09D11/033 , C01B32/05
摘要: In an embodiment, a system includes a three-dimensional (3D) printer, a neutral feedstock, a p-doped feedstock, an n-doped feedstock, and a laser. The 3D printer includes a platen and an enclosure. The platen includes an inert metal. The enclosure includes an inert atmosphere. The neutral feedstock is configured to be deposited onto the platen. The neutral feedstock includes a halogenated solution and a nanoparticle having a negative electron affinity. The p-doped feedstock is configured to be deposited onto the platen. The p-doped feedstock includes a boronated compound introduced to the neutral feedstock. The n-doped feedstock is configured to be deposited onto the platen. The n-doped feedstock includes a phosphorous compound introduced to the neutral feedstock. The laser is configured to induce the nanoparticle to emit solvated electrons into the halogenated solution to form, by reduction, layers of a ceramic comprising a neutral layer, a p-doped layer, and an n-doped layer.
-
公开(公告)号:US20210139330A1
公开(公告)日:2021-05-13
申请号:US16729065
申请日:2019-12-27
发明人: Ta-Ching HSIAO , Chu-Pi JENG , Mu-Hsi SUNG , Kuo-Lun HUANG
IPC分类号: C01B32/05 , C01B32/963 , C01B32/97
摘要: A method of purifying silicon carbide powder includes: providing a container with a surface coated by a nitrogen-removal metal layer, wherein the nitrogen-removal metal layer is tantalum, niobium, tungsten, or a combination thereof; putting a silicon carbide powder into the container to contact the nitrogen-removal metal layer; and heating the silicon carbide powder under an inert gas at a pressure of 400 torr to 760 torr at 1700° C. to 2300° C. for 2 to 10 hours, thereby reducing the nitrogen content of the silicon carbide powder.
-
公开(公告)号:US10730753B2
公开(公告)日:2020-08-04
申请号:US16171408
申请日:2018-10-26
发明人: Sang Whan Park , Mi Rae Youm , Sung Il Yun
IPC分类号: C01B32/963 , B01J27/224
摘要: The present invention relates to an eco-friendly method for preparing a porous silicon carbide structure, which is capable of preparing a porous silicon carbide structure having meso- or macro-sized pores without using a harmful phenolic resin as a carbon source.
-
6.
公开(公告)号:US20190135640A1
公开(公告)日:2019-05-09
申请号:US16239845
申请日:2019-01-04
发明人: Yasuyuki FUKUSHIMA , Kozue AKAZAKI , Yasutomo TANAKA , Kazuma AKIKUBO , Takeshi NAKAMURA , Yukihiro SHIMOGAKI , Takeshi MOMOSE , Noboru SATO , Kohei SHIMA , Yuichi FUNATO
IPC分类号: C01B32/963 , C04B35/565 , C23C16/32 , C04B35/80
摘要: Provided is a method of producing a silicon compound material, including the steps of: storing a silicon carbide preform in a reaction furnace; supplying a raw material gas containing methyltrichlorosilane to the reaction furnace to infiltrate the preform with silicon carbide; and controlling and reducing a temperature of a gas discharged from the reaction furnace at a predetermined rate to subject the gas to continuous thermal history, to thereby decrease generation of a liquid or solid by-product derived from the gas.
-
7.
公开(公告)号:US20240183073A1
公开(公告)日:2024-06-06
申请号:US18482216
申请日:2023-10-06
发明人: Soma SAKAKIBARA , Takahiro KANDA
IPC分类号: C30B29/36 , C01B32/963 , C30B25/16
CPC分类号: C30B29/36 , C01B32/963 , C30B25/165
摘要: A method of producing a silicon carbide single crystal includes: arranging a seed crystal in a heating container that defines a reaction chamber; and growing a silicon carbide single crystal on a surface of the seed crystal by supplying a supply gas containing a silicon carbide raw material gas while heating the reaction chamber. In the growing of the silicon carbide single crystal, the silicon carbide single crystal is grown by controlling a total pressure of the supply gas, which is an internal pressure of the heating container, to 40 kPa or more while controlling a flow rate of the silicon carbide raw material gas to a target value.
-
公开(公告)号:US20240021790A1
公开(公告)日:2024-01-18
申请号:US18257999
申请日:2021-12-10
发明人: Jong Chan Lim , Hyun Hee Lim
IPC分类号: H01M4/36 , H01M4/38 , H01M4/587 , H01M10/0525 , C01B32/963 , C01B33/029
CPC分类号: H01M4/364 , H01M4/386 , H01M4/587 , H01M4/366 , H01M10/0525 , C01B32/963 , C01B33/029 , H01M2004/027
摘要: An embodiment of the present invention relates to: an anode material for a lithium ion secondary battery, comprising a silicon-silicon carbide composite; a preparation method therefor; and a lithium ion secondary battery comprising same, and, more specifically, the anode material for a lithium ion secondary battery, according to the embodiment, is an anode material, which comprises a silicon-silicon carbide composite containing silicon particles and silicon carbide particles, wherein the silicon particles and the silicon carbide particles in the silicon-silicon carbide composite are dispersed from each other and the amount of the silicon carbide particles satisfies a specific range, and thus high capacity and excellent cycle characteristics can be implemented while a low volume expansivity is maintained.
-
公开(公告)号:US11670507B2
公开(公告)日:2023-06-06
申请号:US17189702
申请日:2021-03-02
发明人: David Glen Findley
IPC分类号: B28B1/00 , B33Y30/00 , C30B29/04 , H01L21/02 , B33Y10/00 , B33Y70/00 , C01B32/05 , C01B32/26 , C09D11/033 , C09D11/037 , C01B32/963 , C30B7/14 , H01L23/15 , C30B29/36
CPC分类号: H01L21/02628 , B28B1/001 , B33Y10/00 , B33Y30/00 , B33Y70/00 , C01B32/05 , C01B32/26 , C01B32/963 , C09D11/033 , C09D11/037 , C30B7/14 , H01L21/02104 , H01L23/15 , C04B2235/6026 , C30B29/04 , C30B29/36
摘要: In an embodiment, a system includes a three-dimensional (3D) printer, a feedstock, and a laser. The three-dimensional printer includes a platen including an inert metal, and an enclosure including an inert atmosphere. The feedstock is configured to be deposited onto the platen. The feedstock includes a halogenated solution and a nanoparticle having negative electron affinity. The laser is configured to induce the nanoparticle to emit solvated electrons into the halogenated solution to form, by reduction, a ceramic and a diatomic halogen.
-
公开(公告)号:US11557475B2
公开(公告)日:2023-01-17
申请号:US17316824
申请日:2021-05-11
发明人: David Glen Findley
IPC分类号: B33Y30/00 , C30B29/04 , H01L21/02 , B33Y10/00 , C30B7/14 , H01L23/15 , C30B29/36 , B28B1/00 , B33Y70/00 , C01B32/26 , C09D11/037 , C01B32/963 , C09D11/033 , C01B32/05
摘要: In an embodiment, a system includes a three-dimensional (3D) printer, a neutral feedstock, a p-doped feedstock, an n-doped feedstock, and a laser. The 3D printer includes a platen and an enclosure. The platen includes an inert metal. The enclosure includes an inert atmosphere. The neutral feedstock is configured to be deposited onto the platen. The neutral feedstock includes a halogenated solution and a nanoparticle having a negative electron affinity. The p-doped feedstock is configured to be deposited onto the platen. The p-doped feedstock includes a boronated compound introduced to the neutral feedstock. The n-doped feedstock is configured to be deposited onto the platen. The n-doped feedstock includes a phosphorous compound introduced to the neutral feedstock. The laser is configured to induce the nanoparticle to emit solvated electrons into the halogenated solution to form, by reduction, layers of a ceramic comprising a neutral layer, a p-doped layer, and an n-doped layer.
-
-
-
-
-
-
-
-
-