公开(公告)号：US12084466B1

公开(公告)日：2024-09-10

申请号：US18470776

申请日：2023-09-20

Applicant: Honeywell Federal Manufacturing & Technologies, LLC

Inventor： Dakota Even

IPC: C07F7/08 ,  C07F7/20

CPC classification number: C07F7/0836 ,  C07F7/20

Abstract: Methods, systems, and computer-readable media for purification of trimethylsilanol (TMSOH) from a hexamethyldisiloxane (HMDSO) impurity present within an initial feedstock material. A salt-out assisted liquid-liquid extraction (SALLE) process may be used including adding an extraction solution, extracting the HMDSO impurity, and separating/washing to remove the extraction solution and water from the feedstock such that an increased purity product is provided.

公开(公告)号：US20240199515A1

公开(公告)日：2024-06-20

申请号：US18287807

申请日：2022-04-19

Applicant: TOKUYAMA CORPORATION

Inventor： Daisuke ABIKO ,  Kimihiro MIURA ,  Wataru ICHINOSE ,  Takenori ISOMURA

IPC: C07C29/74 ,  C07F7/20

CPC classification number: C07C29/74 ,  C07F7/20

Abstract: Provided is an ultraviolet ray irradiation device, in which a flow tube through which a substance to be irradiated with ultraviolet ray flows is wound in a spiral manner around a bar-shaped ultraviolet ray source. Also provided is a method for purifying an organic compound that contains an organic lead compound as an impurity, the method comprising: a step for irradiating the organic compound with ultraviolet ray using the ultraviolet ray irradiation device; and a step for removing a lead component that is generated as the result of the irradiation of the organic lead compound with the ultraviolet ray from the organic compound.

公开(公告)号：US10066060B2

公开(公告)日：2018-09-04

申请号：US14655144

申请日：2013-12-26

Applicant: Dow Corning Toray Co., Ltd.

Inventor： Seiki Tamura ,  Tatsuo Souda ,  Sayuri Sawayama ,  Seiji Hori

IPC: C07F7/04 ,  C08G77/46 ,  C07F7/20 ,  C08G77/34 ,  C08L83/12 ,  A61Q19/00 ,  A61K8/894 ,  C08G77/38

CPC classification number: C08G77/46 ,  A61K8/894 ,  A61K2800/10 ,  A61Q19/00 ,  C07F7/20 ,  C08G77/34 ,  C08G77/38 ,  C08L83/12 ,  C08L71/00

Abstract: The present invention relates to a production method for a liquid high-purity organosilicon compound, the method comprising the steps of: adding, to a mixture containing an organosilicon compound selected from a group consisting of organomodified silcones and organomodified silanes and impurities, an organic wax having affinity with the impurities and having a higher melting point than the organosilicon compound, melting and mixing while heating, and introducing the impurities into the melted organic wax; obtaining a solidified product of the organic wax by cooling the organic wax; and performing solid/liquid phase separation on the organosilicon compound and the solidified product of the organic wax. With the present invention, it is possible to provide a useful method for producing a high-purity organosilicon compound stably and on a commercial scale.

公开(公告)号：US20180155371A1

公开(公告)日：2018-06-07

申请号：US15567272

申请日：2016-06-17

Applicant: Dow Corning Corporation

Inventor： Michael A. Depierro ,  Marc Halpern ,  Thomas J Jackson ,  Karen J Kloet ,  Aaron R Sprague

IPC: C07F7/18 ,  C07F7/20

CPC classification number: C07F7/20 ,  C07F7/1804

Abstract: A process for preparing an acryloyloxysilane, comprising: reacting a metal salt of a carboxylic acid having the formula [CR22═CR1CO−]aMa+ (I), with a haloorganoalkoxysilane having the formula XR3Si(OR4)nR53-n (II) at a temperature of from 50 to 160° C. and in the presence of a catalyst, and in the presence of water, an alcohol comprising 1 to 5 carbon atoms, or a combination of water and an alcohol comprising 1 to 5 carbon atoms, to form a mixture comprising an acryloyloxysilane and a metal halide having the formula Ma+X−a (III), wherein R1 is H, R7COO−Ma+, or C1-C6 hydrocarbyl, each R2 is independently R1 or [COO−]Ma+, Ma+ is an alkali metal cation or alkaline earth metal cation, a is 1 or 2, X is halo, R3 is C1-C6 hydrocarbylene, each R4 is independently C1-C10 hydrocarbyl, each R5 is independently R1 and n is an integer from 1 to 3.

公开(公告)号：US09321793B2

公开(公告)日：2016-04-26

申请号：US14400575

申请日：2013-05-01

Applicant: Dow Corning Corporation

Inventor： Robert Thomas Larsen ,  Michael W. Toepke

IPC: C07F7/12 ,  C07F7/20 ,  B01D15/18 ,  B01D15/32

CPC classification number: C07F7/20 ,  B01D15/185 ,  B01D15/322 ,  B01D15/325

Abstract: The present invention relates to a method for separating organohalosilanes. The method includes introducing a mixture including at least a first organohalosilane and a second organohalosilane onto a chromatographic bed including a stationary phase. The method also includes passing a liquid mobile phase through the chromatographic bed to produce an eluate including at least one fraction enriched in the first organohalosilane and at least one fraction enriched in the second organohalosilane.

Abstract translation: 本发明涉及一种分离有机卤代硅烷的方法。 该方法包括将包含至少第一有机卤硅烷和第二有机卤代硅烷的混合物引入到包含固定相的色谱床上。 该方法还包括使液体流动相通过色谱床以产生包含富含第一有机卤代硅烷的至少一个级分和富含第二有机卤代硅烷的至少一个级分的洗脱液。

公开(公告)号：US09073953B2

公开(公告)日：2015-07-07

申请号：US14380079

申请日：2013-01-16

Applicant: Central Glass Company, Limited

Inventor： Takuya Teshima ,  Takaaki Shibayama ,  Yosuke Nakamura ,  Tomoyuki Hiraoka

IPC: C07F7/08 ,  C07F7/20

CPC classification number: C07F7/20 ,  C07F7/0896

Abstract: Disclosed is a method for refining trimethylsilane, including the steps of (1) preparing an activated carbon loaded with at least copper (II) oxide and zinc oxide; (2) adsorbing a trimethylsilane onto the activated carbon; and (3) bringing a trimethylsilane containing silane, methylsilane or dimethylsilane as an impurity into contact with the activated carbon finished with the step (2) to remove the impurity from the trimethylsilane by adsorbing the impurity. According to this method, heat generation of the activated carbon is suppressed and impurities such as dimethylsilane, etc. can be removed efficiently.

Abstract translation: 公开了一种精制三甲基硅烷的方法，包括以下步骤：（1）制备负载至少氧化铜（II）和氧化锌的活性炭; （2）将三甲基硅烷吸附在活性炭上; 和（3）使含有硅烷，甲基硅烷或二甲基硅烷的三甲基硅烷作为杂质与步骤（2）完成的活性炭接触，通过吸附杂质从三甲基硅烷中除去杂质。 根据该方法，能够抑制活性炭的发热，有效地除去二甲基硅烷等杂质。

公开(公告)号：US08937196B2

公开(公告)日：2015-01-20

申请号：US13877468

申请日：2011-11-14

Applicant: Robert Fosdick ,  Stephen Kamin ,  Hanh Vo ,  Tylyn Weickert

Inventor： Robert Fosdick ,  Stephen Kamin ,  Hanh Vo ,  Tylyn Weickert

IPC: C07F7/20 ,  B01D11/04 ,  C08G77/34 ,  B01J20/28

CPC classification number: C07F7/20 ,  B01D11/04 ,  B01J20/28004 ,  B01J20/28023 ,  C08G77/34

Abstract: A process for removing an impurity from a siloxane comprising i) flowing a first liquid through a fiber bundle comprising a plurality of fibers extending lengthwise in a conduit, wherein the bundle has an upstream end and a downstream end, and the first liquid flows in a direction from the upstream end of the bundle to the downstream end; and ii) while continuing (i), flowing a second liquid comprising a siloxane and an impurity through the fiber bundle in a direction from the upstream end of the bundle to the downstream end of the bundle to effect transfer of at least a portion of the impurity from the second liquid to the first liquid, wherein the first liquid and the second liquid are substantially immiscible.

Abstract translation: 一种从硅氧烷中除去杂质的方法，包括：i）使第一液体流过纤维束，所述纤维束包括在管道中纵向延伸的多根纤维，其中所述束具有上游端和下游端，并且所述第一液体流入 方向从束的上游端到下游端; 和ii）同时继续（i）使包含硅氧烷和杂质的第二液体沿着从束的上游端到束的下游端的方向流过纤维束，以实现至少一部分 从第二液体到第一液体的杂质，其中第一液体和第二液体基本上是不混溶的。

公开(公告)号：US20140024849A1

公开(公告)日：2014-01-23

申请号：US14007137

申请日：2012-02-27

Applicant: Burkhard Standke ,  Mustafa Guezelsahin ,  Manuel Friedel ,  Joerg Arndt ,  Klaus Koellisch

Inventor： Burkhard Standke ,  Mustafa Guezelsahin ,  Manuel Friedel ,  Joerg Arndt ,  Klaus Koellisch

IPC: C07F7/18

CPC classification number: C07F7/18 ,  B01D15/363 ,  B01J41/07 ,  B01J41/13 ,  B01J47/016 ,  C07F7/1804 ,  C07F7/188 ,  C07F7/20

Abstract: The invention relates to a process for dechlorinating alkylsilanes and siloxanes, and also to the use of basic anion exchanger resins for dechlorinating alkyl silanes and alkylsiloxanes.

Abstract translation: 本发明涉及一种使烷基硅烷和硅氧烷脱氯的方法，还涉及使用碱性阴离子交换树脂来脱氯烷基硅烷和烷基硅氧烷。

公开(公告)号：US20140005408A1

公开(公告)日：2014-01-02

申请号：US13920230

申请日：2013-06-18

Applicant: Krzysztof Skowerski ,  Michal Bieniek

Inventor： Krzysztof Skowerski ,  Michal Bieniek

IPC: B01J31/22

CPC classification number: C07F15/0046 ,  B01J31/2295 ,  C07C6/06 ,  C07C7/10 ,  C07C7/12 ,  C07C67/475 ,  C07C2531/22 ,  C07C2601/08 ,  C07D207/46 ,  C07D307/28 ,  C07F7/1892 ,  C07F7/20

Abstract: This disclosure relates to new metal complexes, such as compounds of Formula 1, and their application in olefin or alkyne metathesis and to methods of carrying out olefin metathesis reactions.

Abstract translation: 本公开涉及新的金属络合物，例如式1的化合物及其在烯烃或炔烃复分解中的应用以及进行烯烃复分解反应的方法。

公开(公告)号：US08476468B2

公开(公告)日：2013-07-02

申请号：US13121702

申请日：2009-10-13

Applicant: Hartwig Rauleder ,  Ekkehard Mueh

Inventor： Hartwig Rauleder ,  Ekkehard Mueh

IPC: C07F7/08

CPC classification number: C07F7/20

Abstract: The invention relates to a process for treating a composition containing silicon compounds, especially organosilanes and/or inorganic silanes, and at least one extraneous metal and/or a compound containing extraneous metal, wherein the composition is contacted with at least one adsorbent and/or a first filter and then a composition in which the content of the extraneous metal and/or of the compound containing extraneous metal has been reduced is obtained. The invention further relates to the use of organic resins, activated carbon, silicates and/or zeolites and/or else of at least one filter with small pore sizes to reduce the level of the compounds mentioned.

Abstract translation: 本发明涉及一种处理包含硅化合物，特别是有机硅烷和/或无机硅烷的组合物和至少一种外来金属和/或含有外来金属的化合物的方法，其中所述组合物与至少一种吸附剂和/或 然后获得第一过滤器，然后获得其中外来金属和/或含有外来金属的化合物的含量已经被还原的组合物。 本发明还涉及使用有机树脂，活性炭，硅酸盐和/或沸石和/或至少一种具有小孔径的过滤器以降低所述化合物的含量。