PROCESS FOR PRODUCTION OF MAGNESIUM FLUORIDE SOL SOLUTIONS FROM ALKOXIDES COMPRISING ADDITION OF MAGNESIUM SALTS
    2.
    发明申请
    PROCESS FOR PRODUCTION OF MAGNESIUM FLUORIDE SOL SOLUTIONS FROM ALKOXIDES COMPRISING ADDITION OF MAGNESIUM SALTS 审中-公开
    从包含镁盐添加物的烷氧化物生产氟化镁溶液的方法

    公开(公告)号:US20150231587A1

    公开(公告)日:2015-08-20

    申请号:US14428989

    申请日:2013-09-18

    申请人: NANOFLUOR GmbH

    发明人: Erhard Kemnitz

    IPC分类号: B01J13/00 C03C17/22 C09D1/00

    摘要: The invention relates to a method for obtaining a magnesium fluoride (MgF2) sol solution, comprising the steps of providing a magnesium alkoxide precursor in a non-aqueous solvent and adding 1.85 to 2.05 molar equivalents of non-aqueous hydrofluoric acid, characterized in that the reaction proceeds in the presence of a second magnesium fluoride precursor selected from the group of salts of strong, volatile acids, such as a chloride, bromide, iodide, nitrate or triflate of magnesium, or of a catalytic amount of a strong, volatile acid; and/or an additive non-magnesium fluoride precursor selected from the group of salts of strong, volatile acids, such as a chloride, bromide, iodide, nitrate or triflate of lithium, antimony, tin calcium, strontium, barium, aluminium, silicium, zirconium, titanium or zinc. The invention further relates to sol solutions, method of applying the sol solutions of the invention to surfaces as a coating, and to antireflective coatings obtained thereby.

    摘要翻译: 本发明涉及一种获得氟化镁(MgF 2)溶胶溶液的方法,包括以下步骤:在非水溶剂中提供醇镁前体,并加入1.85-2.05摩尔当量的非水性氢氟酸,其特征在于: 反应在存在选自强挥发性酸如氯化物,溴化物,碘化物,硝酸盐或氟化三氟甲磺酸盐或催化量的强挥发酸的盐的第二氟化镁前体的存在下进行; 和/或选自锂,锑,锡钙,锶,钡,铝,硅等的强挥发性酸如氯化物,溴化物,碘化物,硝酸盐或三氟甲磺酸盐的盐的添加剂非氟化镁前体, 锆,钛或锌。 本发明还涉及溶胶溶液,将本发明的溶胶溶液涂布到作为涂层的表面上的方法以及由此获得的抗反射涂层。

    SYSTEMS AND METHODS FOR PRODUCING MULTI-COMPONENT COLLOIDAL STRUCTURES
    3.
    发明申请
    SYSTEMS AND METHODS FOR PRODUCING MULTI-COMPONENT COLLOIDAL STRUCTURES 审中-公开
    用于生产多组分胶体结构的系统和方法

    公开(公告)号:US20100204459A1

    公开(公告)日:2010-08-12

    申请号:US12670913

    申请日:2008-08-27

    摘要: A system for producing multi-component colloidal structures has a supply system; an assembly system that is in fluid connection with the supply system to receive a supply of colloidal structural components from the supply system; and an output system in fluid connection with the assembly system. The assembly system has an assembly chamber adapted to contain colloidal structural components during assembly of a multi-component colloidal structure and is structured and arranged to control positions and orientations of first and second c structural components in the assembly chamber to bring the first and second colloidal structural components together in predetermined relative positions and orientations for assembly into at least a portion of the multi-component colloidal structure.

    摘要翻译: 一种用于生产多组分胶体结构的系统具有供应系统; 与所述供应系统流体连接以从所述供应系统接收胶体结构部件的供应的组装系统; 以及与组装系统流体连接的输出系统。 组装系统具有适于在组装多组分胶体结构期间容纳胶体结构组分的组合室,并且其被构造和布置成控制组装室中第一和第二c结构组分的位置和取向,以使第一和第二胶体 结构部件一起在预定的相对位置和取向上,用于组装到多组分胶体结构的至少一部分中。

    Process for the production of emulsions and dispersions
    4.
    发明授权
    Process for the production of emulsions and dispersions 失效
    生产乳液和分散体的方法

    公开(公告)号:US07696252B2

    公开(公告)日:2010-04-13

    申请号:US10703094

    申请日:2003-11-05

    申请人: Richard M Pashley

    发明人: Richard M Pashley

    摘要: Methods for the formation of colloidal suspensions. The method includes combining an aqueous substance with a second substance that is normally immiscible with the aqueous substance, to form a mixture, and before, during or after the combining removing dissolved gases from one or both of the aqueous and second substance, whereby the aqueous and second substances mix and form a colloidal suspension. The methods for the formation of colloidal suspensions include methods for the formation of emulsions as well as particulate dispersions. The methods used to form the colloidal suspensions in accordance with the present invention produce colloidal suspensions that are stable for periods from an hour to several weeks in the absence of surfactants or stabilizing agents.

    摘要翻译: 形成胶体悬浮液的方法。 该方法包括将水性物质与通常与水性物质不混溶的第二物质混合以形成混合物,并且在组合之前,期间或之后从水溶液和第二物质中的一种或两种除去溶解气体,由此将水性 并且第二物质混合并形成胶态悬浮液。 形成胶体悬浮液的方法包括形成乳液以及颗粒分散体的方法。 用于形成根据本发明的胶体悬浮液的方法产生胶体悬浮液,其在不存在表面活性剂或稳定剂的情况下稳定时间为1小时至数周。

    Method for the preparation of nanoparticles
    5.
    发明申请
    Method for the preparation of nanoparticles 审中-公开
    制备纳米粒子的方法

    公开(公告)号:US20040091542A1

    公开(公告)日:2004-05-13

    申请号:US10466365

    申请日:2003-12-11

    IPC分类号: A61K009/14 B29B009/00

    摘要: The invention relates to free nano-sized particles of active agents e.g. therapeutic, cosmetic or diagnostic agents, and to a method for the preparation of such particles. The method comprises providing a liquid feed stock comprising an active agent or combination of two or more active agents, atomising the liquid feed stock, suspending the droplets in a carrier gas, and passing the carrier gas and droplets through a heated tube flow reactor under predetermined residence time and temperature history, and collecting the particles produced. Nano-sized crystalline spherical uncharged particles with narrow aerodynamic particle size distribution and rough surfaces, are obtained. The particles show improved dissolution rate in-vitro and bioavailability in-vivo, dispersibility and stability.

    摘要翻译: 本发明涉及活性剂的游离纳米尺寸颗粒,例如 治疗剂,化妆品或诊断剂,以及制备这种颗粒的方法。 该方法包括提供液体原料,其包含活性剂或两种或更多种活性剂的组合,使液体原料雾化,将液滴悬浮在载气中,并使载气和液滴通过加热的管流反应器在预定的 停留时间和温度历史,并收集生成的颗粒。 获得具有窄空气动力学粒度分布和粗糙表面的纳米尺寸的结晶球形不带电粒子。 颗粒体外显示改善的溶出速率和体内,分散性和稳定性的生物利用度。

    Process for the production of emulsions and dispersions
    7.
    发明申请
    Process for the production of emulsions and dispersions 失效
    生产乳液和分散体的方法

    公开(公告)号:US20050096398A1

    公开(公告)日:2005-05-05

    申请号:US10703094

    申请日:2003-11-05

    申请人: Richard Pashley

    发明人: Richard Pashley

    摘要: Methods for the formation of colloidal suspensions. The method includes combining an aqueous substance with a second substance that is normally immiscible with the aqueous substance, to form a mixture, and before, during or after the combining removing dissolved gases from one or both of the aqueous and second substance, whereby the aqueous and second substances mix and form a colloidal suspension. The methods for the formation of colloidal suspensions include methods for the formation of emulsions as well as particulate dispersions. The methods used to form the colloidal suspensions in accordance with the present invention produce colloidal suspensions that are stable for periods from an hour to several weeks in the absence of surfactants or stabilizing agents.

    摘要翻译: 形成胶体悬浮液的方法。 该方法包括将水性物质与通常与水性物质不混溶的第二物质混合以形成混合物,并且在组合之前,期间或之后从水溶液和第二物质中的一种或两种除去溶解气体,由此将水性 并且第二物质混合并形成胶态悬浮液。 形成胶体悬浮液的方法包括形成乳液以及颗粒分散体的方法。 用于形成根据本发明的胶体悬浮液的方法产生胶体悬浮液,其在不存在表面活性剂或稳定剂的情况下稳定时间为1小时至数周。

    Organic sol comprising at least one oxygenated rare-earth compound,
synthesis method therefor, and use of said sol for catalysis
    10.
    发明授权
    Organic sol comprising at least one oxygenated rare-earth compound, synthesis method therefor, and use of said sol for catalysis 有权
    包含至少一种含氧稀土化合物的有机溶胶,其合成方法和所述溶胶用于催化

    公开(公告)号:US6136048A

    公开(公告)日:2000-10-24

    申请号:US68925

    申请日:1998-11-19

    摘要: A method for processing soot containing one or more rare earths, wherein said soot is contacted with an oxygen-containing gas, is disclosed. The method comprises (a) preparing an aqueous phase comprising a dispersion of at least one oxygenated metal compound; (b) simultaneously or consecutively contacting a suspension from step (a) with an organic phase including at least one amphiphilic agent and preferably an organic mixture or compound as the solvent; and c recovering the organic phase. Said oxygenated metal compound is produced by means of a method according to which a solution including at least one soluble rare-earth salt, usually an acetate and/or a chloride, is prepared; the solution is contacted with a basic medium and the resulting reaction mixture is maintained at a basic pH; and the precipitate formed by atomization or freeze-drying is recovered. Said method is useful in inorganic synthesis and catalysis.

    摘要翻译: PCT No.PCT / FR96 / 01852 Sec。 371日期:1998年11月19日 102(e)1998年11月19日PCT PCT 1996年11月22日PCT公布。 第WO97 / 19022号公报 日期1997年5月29日公开了一种用于处理含有一种或多种稀土的烟灰的方法,其中所述烟灰与含氧气体接触。 该方法包括(a)制备包含至少一种含氧金属化合物的分散体的水相; (b)同时或连续地将来自步骤(a)的悬浮液与包含至少一种两亲性试剂,优选有机混合物或化合物的有机相作为溶剂接触; 和+ E,crc c + EE回收有机相。 所述氧化金属化合物是通过制备包含至少一种可溶性稀土盐(通常为乙酸盐和/或氯化物)的溶液的方法生产的。 将溶液与碱性介质接触,并将所得反应混合物保持在碱性pH下; 回收通过雾化或冷冻干燥形成的沉淀物。 所述方法可用于无机合成和催化。