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    Ni-based corrosion resistant alloy and corrosion resistant member for supercritical ammonia reactor made of the alloy
    1.
    发明授权
    Ni-based corrosion resistant alloy and corrosion resistant member for supercritical ammonia reactor made of the alloy 有权
    Ni合金耐腐蚀合金和超临界氨反应器耐腐蚀材料

    公开(公告)号：US08414828B2

    公开(公告)日：2013-04-09

    申请号：US12064297

    申请日：2006-08-22

    申请人： Yoshihiko Yamamura ,  Shinya Sato ,  Shinichi Nishiya

    发明人： Yoshihiko Yamamura ,  Shinya Sato ,  Shinichi Nishiya

    IPC分类号： C22C19/05

    CPC分类号： B01J3/008 ,  B01J19/02 ,  B01J2219/0236 ,  B01J2219/0277 ,  B01J2219/029 ,  C22C19/052 ,  C22C19/053 ,  C22C19/055 ,  C22C19/056 ,  Y02P20/544

    摘要： A material is presented that exhibits excellent corrosion resistance to supercritical ammonia and is suitable for a supercritical ammonia reactor. An Ni-based corrosion resistant alloy includes from 15% or more to 50% or less by mass of Cr and any one or both of Mo and W, wherein a [(content of Mo)+0.5×(content of W)] is from 1.5% or more to 8.5% or less by mass, a value of 1.8×[% content of Cr]/{[% content of Mo]+0.5×[% content of W]} is from 3.0 or more to 70.0 or less and the balance is Ni and an unavoidable impurity. The alloy may be used to configure a supercritical ammonia reactor or the material is coated on a surface that contacts with a supercritical ammonia fluid. The alloy exhibits excellent corrosion resistance to supercritical ammonia and a mineralizer added the supercritical ammonia. The safety and reliability of an apparatus can be improved, the producing cost can be reduced, the apparatus lifetime can be extended and the running cost can be reduced.

    摘要翻译： 对超临界氨表现出优异的耐腐蚀性，适用于超临界氨反应器的材料。 镍基耐腐蚀合金包含15质量％以上至50质量％以下的Cr和Mo和W中的任一种或两种，其中[（Mo含量）+ 0.5×（W含量）]为 从1.5％以上至8.5％以下，1.8×[Cr含量％] [{Mo含量] + 0.5×[W含量％]的值为3.0以上〜70.0以上 较少，平衡是Ni和不可避免的杂质。 该合金可用于构造超临界氨反应器，或者该材料涂覆在与超临界氨流体接触的表面上。 该合金对超临界氨表现出优异的耐腐蚀性，并且矿化剂加入超临界氨。 可以提高设备的安全性和可靠性，可以降低生产成本，延长设备使用寿命，降低运行成本。

    Pressure vessel for growing single crystals
    2.
    发明授权
    Pressure vessel for growing single crystals 有权
    用于生长单晶的压力容器

    公开(公告)号：US09127372B2

    公开(公告)日：2015-09-08

    申请号：US11813805

    申请日：2006-01-11

    申请人： Yuji Sasagawa ,  Osamu Wakao ,  Yoshihiko Yamamura ,  Shigeharu Akatsuka ,  Keiichiro Matsushita

    发明人： Yuji Sasagawa ,  Osamu Wakao ,  Yoshihiko Yamamura ,  Shigeharu Akatsuka ,  Keiichiro Matsushita

    IPC分类号： C30B35/00 ,  C30B7/10

    CPC分类号： C30B7/10 ,  B01J3/04 ,  C23C30/00 ,  C30B35/002 ,  Y10T29/49826 ,  Y10T117/10 ,  Y10T117/1096

    摘要： An object of the present invention is to manufacture single crystals of high quality on an industrial production scale by preventing impurities from being mixed in single crystals when the single crystals are produced by the solvothermal method.A pressure vessel body 1, in which a supercritical state is maintained, is made of heat resistant alloy, a portion of the pressure vessel body is open, a corrosion-resistant mechanical lining 5 is provided on an inner face of the pressure vessel and on an entire outer circumferential edge of the opening, and the opening is sealed by an airtight mating face formed out of a corrosion-resistant mechanical lining, which is formed on the outer circumferential edge of the opening, and by an airtight mating face of the corrosion-resistant mechanical lining cover 6 on an inner face of the cover 3 through a corrosion-resistant gasket member. Since the pressure vessel body and the inner face of the cover are covered with the corrosion-resistant mechanical lining, corrosion can be prevented. The corrosion-resistant mechanical lining ensures the sealing property on the airtight mating face between the pressure vessel body and the cover and further effectively prevents corrosion in the airtight sealing portion and it becomes possible to repeatedly open and close the airtight sealing portion.

    摘要翻译： 本发明的目的是通过在通过溶剂热法制造单晶时，通过防止杂质混合在单晶中，在工业生产规模上制造高质量的单晶。 保持超临界状态的压力容器主体1由耐热合金制成，压力容器主体的一部分打开，在压力容器的内表面上设置耐腐蚀的机械衬里5， 开口的整个外圆周边缘，并且开口由形成在开口的外周边缘上的耐腐蚀机械衬里形成的气密配合面和由腐蚀的气密配合面密封 通过耐腐蚀的垫圈构件在盖3的内表面上具有耐力的机械衬里盖6。 由于压力容器主体和盖的内表面被耐腐蚀的机械衬里覆盖，所以可以防止腐蚀。 耐腐蚀机械衬里确保了压力容器主体和盖之间的气密配合面上的密封性能，并且进一步有效地防止了气密密封部分中的腐蚀，并且可以重复地打开和关闭气密密封部分。

    Production method, production vessel and member for nitride crystal
    5.
    发明授权
    Production method, production vessel and member for nitride crystal 有权
    生产方法，生产容器和氮化物晶体元件

    公开(公告)号：US08609059B2

    公开(公告)日：2013-12-17

    申请号：US13481989

    申请日：2012-05-29

    申请人： Yutaka Mikawa ,  Makiko Kiyomi ,  Yuji Kagamitani ,  Toru Ishiguro ,  Yoshihiko Yamamura

    发明人： Yutaka Mikawa ,  Makiko Kiyomi ,  Yuji Kagamitani ,  Toru Ishiguro ,  Yoshihiko Yamamura

    IPC分类号： C30B11/00 ,  C30B35/00 ,  C30B28/06 ,  C30B19/00 ,  B01J3/04 ,  B01D9/00 ,  C01B21/06

    CPC分类号： C30B29/406 ,  C30B7/105 ,  C30B29/403

    摘要： To provide a production method for a nitride crystal, where a nitride crystal can be prevented from precipitating in a portion other than on a seed crystal and the production efficiency of a gallium nitride single crystal grown on the seed crystal can be enhanced. In a method for producing a nitride crystal by an ammonothermal method in a vessel containing a mineralizer-containing solution, out of the surfaces of said vessel and a member provided in said vessel, at least a part of the portion coming into contact with said solution is constituted by a metal or alloy containing one or more atoms selected from the group consisting of tantalum (Ta), tungsten (W) and titanium (Ti), and has a surface roughness (Ra) of less than 1.80 μm.

    摘要翻译： 为了提供氮化物晶体的制造方法，其中可以防止氮化物晶体在晶种以外的部分析出，并且可以提高在晶种上生长的氮化镓单晶的生产效率。 在包含含矿化剂的溶液的容器中通过氨热法制造氮化物晶体的方法中，在所述容器的表面和设置在所述容器中的部件之外，与所述溶液接触的部分的至少一部分 由含有一种或多种选自钽（Ta），钨（W）和钛（Ti）的原子的金属或合金构成，并且具有小于1.80μm的表面粗糙度（Ra）。

    NI-BASED CORROSION RESISTANT ALLOY AND CORROSION RESISTANT MEMBER FOR SUPERCRITICAL AMMONIA REACTOR MADE OF THE ALLOY
    9.
    发明申请
    NI-BASED CORROSION RESISTANT ALLOY AND CORROSION RESISTANT MEMBER FOR SUPERCRITICAL AMMONIA REACTOR MADE OF THE ALLOY 有权
    耐碱耐腐蚀合金及耐腐蚀材料的合金超临界反应器

    公开(公告)号：US20090280024A1

    公开(公告)日：2009-11-12

    申请号：US12064297

    申请日：2006-08-22

    申请人： Yoshihiko Yamamura ,  Shinya Sato ,  Shinichi Nishiya

    发明人： Yoshihiko Yamamura ,  Shinya Sato ,  Shinichi Nishiya

    IPC分类号： C22C19/05

    CPC分类号： B01J3/008 ,  B01J19/02 ,  B01J2219/0236 ,  B01J2219/0277 ,  B01J2219/029 ,  C22C19/052 ,  C22C19/053 ,  C22C19/055 ,  C22C19/056 ,  Y02P20/544

    摘要： The invention intends to provide a material that exhibits excellent corrosion resistance to supercritical ammonia and is suitable for a supercritical ammonia reactor.An Ni-based corrosion resistant alloy includes from 15% or more to 50% or less by mass of Cr and any one or both of Mo and W, wherein a [(content of Mo)+0.5×(content of W)] is from 1.5% or more to 8.5% or less by mass, a value of 1.8×[% content of Cr]/{[% content of Mo]+0.5×[% content of W]} is from 3.0 or more to 70.0 or less and the balance is Ni and an unavoidable impurity. Preferably, content of Fe is less than 3% by mass, and content of C is less than 0.05% by mass. The alloy is used to configure a supercritical ammonia reactor or the material is coated on a surface that contacts with a supercritical ammonia fluid. The alloy exhibits excellent corrosion resistance to supercritical ammonia and a mineralizer added the supercritical ammonia. The safety and reliability of an apparatus can be improved, the producing cost can be reduced, the apparatus lifetime can be extended and the running cost can be reduced.

    摘要翻译： 本发明旨在提供一种对超临界氨具有优异耐腐蚀性并适用于超临界氨反应器的材料。 Ni系耐腐蚀合金含有15质量％以上且50质量％以下的Cr和Mo和W中的任一种或两者，其中[（Mo）+ 0.5×（W含量）]为 从1.5％以上至8.5％以下，Crx / {[Mo含量] + 0.5×[W]的含量为1.8×[％]的值为3.0以上至70.0以上， 较少，平衡是Ni和不可避免的杂质。 Fe的含量优选小于3质量％，C的含量优选为0.05质量％以下。 该合金用于构造超临界氨反应器，或者该材料涂覆在与超临界氨流体接触的表面上。 该合金对超临界氨表现出优异的耐腐蚀性，并且矿化剂加入超临界氨。 可以提高设备的安全性和可靠性，可以降低生产成本，延长设备使用寿命，降低运行成本。

    PRODUCTION METHOD, PRODUCTION VESSEL AND MEMBER FOR NITRIDE CRYSTAL
    10.
    发明申请
    PRODUCTION METHOD, PRODUCTION VESSEL AND MEMBER FOR NITRIDE CRYSTAL 有权
    生产方法，生产船只和硝酸盐晶体的成员

    公开(公告)号：US20120237431A1

    公开(公告)日：2012-09-20

    申请号：US13481989

    申请日：2012-05-29

    申请人： YUTAKA MIKAWA ,  MAKIKO KIYOMI ,  YUJI KAGAMITANI ,  TORU ISHIGURO ,  YOSHIHIKO YAMAMURA

    发明人： YUTAKA MIKAWA ,  MAKIKO KIYOMI ,  YUJI KAGAMITANI ,  TORU ISHIGURO ,  YOSHIHIKO YAMAMURA

    IPC分类号： C30B7/10 ,  C01B21/06 ,  C01B21/00

    CPC分类号： C30B29/406 ,  C30B7/105 ,  C30B29/403

    摘要： To provide a production method for a nitride crystal, where a nitride crystal can be prevented from precipitating in a portion other than on a seed crystal and the production efficiency of a gallium nitride single crystal grown on the seed crystal can be enhanced. In a method for producing a nitride crystal by an ammonothermal method in a vessel containing a mineralizer-containing solution, out of the surfaces of said vessel and a member provided in said vessel, at least a part of the portion coming into contact with said solution is constituted by a metal or alloy containing one or more atoms selected from the group consisting of tantalum (Ta), tungsten (W) and titanium (Ti), and has a surface roughness (Ra) of less than 1.80 μm.

    摘要翻译： 为了提供氮化物晶体的制造方法，其中可以防止氮化物晶体在晶种以外的部分析出，并且可以提高在晶种上生长的氮化镓单晶的生产效率。 在包含含矿化剂的溶液的容器中通过氨热法制造氮化物晶体的方法中，在所述容器的表面和设置在所述容器中的部件之外，与所述溶液接触的部分的至少一部分 由含有一种或多种选自钽（Ta），钨（W）和钛（Ti）的原子的金属或合金构成，表面粗糙度（Ra）小于1.80μm。