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公开(公告)号：US09993811B2
公开(公告)日：2018-06-12
申请号：US14438566
申请日：2013-10-25
发明人： Lingping Zhou , Ziyang Liu , Jiexiao Zhang , Mingde Xu , Weilin Zhang , Huiping Tian , Yuxia Zhu
IPC分类号： C01B39/00 , B01J29/08 , B01J29/06 , C01B39/06 , B01J19/24 , C01B39/02 , C01B39/24 , B01J19/00 , B01J19/22 , B01J6/00 , B01J8/00
CPC分类号： B01J29/088 , B01J6/002 , B01J8/002 , B01J8/0055 , B01J19/006 , B01J19/22 , B01J19/2415 , B01J29/06 , B01J2029/081 , B01J2219/0077 , B01J2219/18 , B01J2219/187 , B01J2219/1943 , B01J2219/24 , B01J2229/16 , B01J2229/32 , C01B39/00 , C01B39/026 , C01B39/06 , C01B39/24
摘要： A process for preparing a catalytic cracking catalyst, which process comprises: a molecular sieve is introduced into a gas-phase ultra-stabilization reactor, the molecular sieve is moved without the conveying of carrier gas from a molecular sieve inlet of the gas-phase ultra-stabilization reactor to a molecular sieve outlet of the gas-phase ultra-stabilization reactor, and the molecular sieve is contacted and reacted with a gaseous SiCl4 in the gas-phase ultra-stabilization reactor, the molecular sieve resulting from the contacting and the reacting is optionally washed, then mixed with a matrix and water into slurry, and shaped into particles.
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公开(公告)号：US09896343B2
公开(公告)日：2018-02-20
申请号：US14527657
申请日：2014-10-29
发明人： Changjiu Xia , Bin Zhu , Min Lin , Xinxin Peng , Xingtian Shu , Chunfeng Shi
CPC分类号： C01B39/00 , C01B39/085 , C01P2004/90 , C01P2006/17
摘要： The present invention relates to a titanium silicalite molecular sieve, wherein the crystal grain of the titanium silicalite molecular sieve has a ratio of (surface Si/Ti ratio):(bulk Si/Ti ratio) being larger than 1.1 and less than 5.
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公开(公告)号：US20180022613A1
公开(公告)日：2018-01-25
申请号：US15656079
申请日：2017-07-21
发明人： Yanpeng YANG , Aizeng MA
IPC分类号： C01F7/42
CPC分类号： C01F7/42 , C01F7/36 , C01P2004/61
摘要： A method of producing a highly-pure aluminum hydroxide, comprising the following steps: (1) reacting alcohol with metal aluminum to produce aluminum alkoxide, then hydrolyzing the aluminum alkoxide with water to produce an aluminum hydroxide slurry and an alcohol, filtering the aluminum hydroxide slurry, washing a resulting filter cake with water to remove the alcohol trapped therein, and drying the filter cake after the water washing to produce an aluminum hydroxide powder, (2) sending the alcohol-containing water produced in step (1) to an alcohol extraction unit for separating water and alcohol through extraction, and sending the separated water back to step (1) for recycling, (3) dehydrating the hydrous alcohol produced by hydrolyzing the aluminum alkoxide in step (1) before using it as the raw materials for reacting metal aluminum with alcohol to produce aluminum alkoxide in step (1). The method can improve the recovery of alcohol, reduce the production cost of a highly-pure aluminum hydroxide, improve the purity of aluminum oxide and achieve a zero discharge of sewage by recycling water.
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64.发明申请公开(公告)号：US20180015445A1
公开(公告)日：2018-01-18
申请号：US15546791
申请日：2016-01-27
发明人： Chunfeng SHI , Junfeng RONG , Peng YU , Jingxin XIE , Mingsheng ZONG , Weiguo LIN
CPC分类号： B01J27/24 , B01J35/1014 , B01J35/1019 , B01J37/08 , C01B32/15 , C01B32/168 , C07C5/48 , C07C11/06 , C07C11/08 , C07C11/167 , C07C15/46 , C07C2527/24
摘要： A heteroatom-containing nano-carbon material, based on the total weight of said heteroatom-containing nano-carbon material and calculated as the elements, has an oxygen content of 1-6 wt %, a nitrogen content of 0-2 wt %, a carbon content of 92-99 wt %. In its XPS, the ratio of the oxygen content as determined with the peak(s) in the range of 531.0-532.5 eV to the oxygen content as determined with the peak(s) in the range of 532.6-533.5 eV is 0.2-0.8; the ratio of the carbon content as determined with the peak(s) in the range of 288.6-288.8 eV to the carbon content as determined with the peak(s) in the range of 286.0-286.2 eV is 0.2-1; the ratio of the nitrogen content as determined with the peak(s) in the range of 398.5-400.1 eV to the total nitrogen content is 0.7-1. The heteroatom-containing nano-carbon material shows a good catalytic capability in dehydrogenation of hydrocarbons.
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公开(公告)号：US20170305815A1
公开(公告)日：2017-10-26
申请号：US15520729
申请日：2015-10-20
发明人： Shouye CUI , Youhao XU , Jingchuan YU , Minggang LI , Baoning ZONG , Jinlian TANG , Xin WANG
摘要： Disclosed is a process for producing light olefins, the process comprising: continuously contacting an oxygen-containing compound raw material with catalyst to have a dehydration reaction so as to prepare low-carbon alkene, the reaction pressure P of the dehydration reaction being 1-2 MPa, and the weight hourly space velocity H of the dehydration reaction being 15-50 h−1. The process of preparing light olefins has a simple and continuous operation process, reduces investment, greatly increases production of light olefins and has a high safety.
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公开(公告)号：US09694356B2
公开(公告)日：2017-07-04
申请号：US15081234
申请日：2016-03-25
发明人： Daqing Zhang , Gaoshan Zang , Yuhong Zhang , Jiaxin Wang , Tao Wang
IPC分类号： B01J20/34 , B01J38/44 , B01J27/32 , B01J38/10 , B01J38/60 , B01J38/04 , B01J38/14 , B01J38/18 , B01J38/62 , B01J27/13 , C10G35/09 , C10G35/06 , B01J37/20
CPC分类号： B01J38/44 , B01J27/13 , B01J27/32 , B01J37/20 , B01J38/04 , B01J38/10 , B01J38/14 , B01J38/18 , B01J38/60 , B01J38/62 , C10G35/06 , C10G35/09
摘要： This disclosure describes a method for regenerating a semi-regenerated reforming catalyst. The method comprises adjusting the reaction temperature to 250-480° C., introducing a sulfur-containing naphtha into the reforming reactor, or stopping introducing a feedstock into the reforming reactor, and introducing a sulfur-containing hydrogen into a recycle gas, until the sulfur content in the catalyst is 0.32-0.8 mass %, then the catalyst is subject to coke-burning, oxychlorination and reduction. Alternatively, the method first subjects the spent catalyst to coke-burning followed by introducing sulfate ions thereinto; and then performing oxychlorination and reduction. Disclosed is still another method for regenerating a platinum-rhenium reforming catalyst, which comprises coke-burning the spent catalyst; introducing sulfur and chlorine in the catalyst by impregnation; and then drying, calcinating and reducing.
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公开(公告)号：US20160279626A1
公开(公告)日：2016-09-29
申请号：US15081234
申请日：2016-03-25
发明人： Daqing ZHANG , Gaoshan ZANG , Yuhong ZHANG , Jiaxin WANG , Tao WANG
CPC分类号： B01J38/44 , B01J27/13 , B01J27/32 , B01J37/20 , B01J38/04 , B01J38/10 , B01J38/14 , B01J38/18 , B01J38/60 , B01J38/62 , C10G35/06 , C10G35/09
摘要： A method for regenerating semi-regenerated reforming catalyst comprises adjusting the reaction temperature to 250-480° C.; introducing sulfur-containing naphtha into the reforming reactor, so that the sulfur content in the catalyst is 0.32-0.8 mass %; then stopping introducing the raw materials into the reforming reactor; subjecting the catalyst to coke-burning, oxychlorination and reduction. Another method for regenerating semi-regenerated reforming catalyst comprises coke-burning the spent catalyst; introducing sulfate ions thereinto; then performing oxychlorination and reduction. There is still another method for regenerating a platinum-rhenium reforming catalyst, comprising coke-burning the spent catalyst; introducing sulfur and chlorine by impregnation; then drying, calcinating and reducing. The catalysts regenerated by said methods can be used without presulfurization and have excellent regeneration performance.
摘要翻译： 再生再生重整催化剂的方法包括将反应温度调节至250-480℃; 将含硫的石脑油引入重整反应器中，使得催化剂中的硫含量为0.32-0.8质量％; 然后停止将原料引入重整反应器; 对催化剂进行焦烧，氧氯化和还原。 再生再生重整催化剂的另一种方法包括焦炭燃烧废催化剂; 向其中引入硫酸根离子; 然后进行氧氯化和还原。 还有另一种再生铂 - 铼重整催化剂的方法，包括焦炭燃烧废催化剂; 通过浸渍引入硫和氯; 然后干燥，煅烧和还原。 通过所述方法再生的催化剂可以在没有预硫化的情况下使用并且具有优异的再生性能。
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68.发明申请HINDERED PHENOL COMPOUND, PREPARATION THEREOF AND USE THEREOF AS AN ANTIOXIDANT 有权苯酚化合物，其制备方法及其作为抗氧化剂的用途公开(公告)号：US20150353858A1
公开(公告)日：2015-12-10
申请号：US14296763
申请日：2014-06-05
发明人： Shuo SU , Jun LONG , Qinghua DUAN , Han ZHOU , Zhiqiang WU , Xinhua LI , Yi ZHAO , Xiaoguang ZHAO
IPC分类号： C10M135/36 , C07D513/04 , C07D279/20 , C07C319/14 , C07D219/08
CPC分类号： C10M135/36 , C07C313/04 , C07C319/14 , C07C323/20 , C07C323/25 , C07C323/32 , C07C323/52 , C07C323/60 , C07D219/08 , C07D279/20 , C07D513/04 , C10M129/10 , C10M135/12 , C10M135/28 , C10M2203/1025 , C10M2207/026 , C10M2207/289 , C10M2215/064 , C10M2215/065 , C10M2219/06 , C10M2219/086 , C10M2219/087 , C10M2219/104 , C10M2219/108 , C10N2230/02 , C10N2230/04 , C10N2230/10 , C10N2230/12
摘要： This invention relates to a novel hindered phenol compound of Formula (I) (wherein the groups R and R′ are as defined in the specification), preparation thereof and use thereof as an antioxidant. By using the hindered phenol compound of this invention as an antioxidant, it is possible to produce a lubricant oil composition exhibiting excellent oxidation resistance at elevated temperatures.
摘要翻译： 本发明涉及式（I）的新型受阻酚化合物（其中基团R和R'如说明书中所定义），其制备及其作为抗氧化剂的用途。 通过使用本发明的受阻酚化合物作为抗氧化剂，可以制备在高温下表现出优异的耐氧化性的润滑油组合物。
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公开(公告)号：US20150284322A1
公开(公告)日：2015-10-08
申请号：US14439562
申请日：2013-10-29
发明人： Chunfeng Shi , Min Lin , Xingtian Shu , Xuhong Mu , Bin Zhu
IPC分类号： C07C315/02 , C07C319/14
CPC分类号： C07C315/02 , C07C319/14 , Y02P20/127 , C07C317/04
摘要： A process for producing dimethyl sulfoxide, wherein said process comprises the following steps: (1) contacting hydrogen sulfide with methanol to produce a mixture containing dimethyl sulfide, and separating dimethyl sulfide from the mixture; and (2) in the presence or absence of a solvent, contacting dimethyl sulfide obtained in step (1) with at least one oxidant and a catalyst to produce a mixture containing dimethyl sulfoxide, said catalyst comprises at least one Ti—Si molecular sieve.
摘要翻译： 一种生产二甲基亚砜的方法，其中所述方法包括以下步骤：（1）使硫化氢与甲醇接触以产生含有二甲基硫醚的混合物，并从混合物中分离出二甲基硫醚; 和（2）在存在或不存在溶剂的情况下，将步骤（1）中获得的二甲基硫醚与至少一种氧化剂和催化剂接触以产生含有二甲基亚砜的混合物，所述催化剂包含至少一种Ti-Si分子筛。
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公开(公告)号：US20150274620A1
公开(公告)日：2015-10-01
申请号：US14429189
申请日：2013-09-17
发明人： Baoning Zong , Dongqiang Ma , Langyou Wen , Bin Sun , Keyong Yang
IPC分类号： C07C29/149 , C07D223/10 , B01J23/80 , B01J23/835 , B01J23/83 , C07C45/00 , C07C67/04
CPC分类号： C07C29/149 , B01J23/76 , B01J23/80 , B01J23/83 , B01J23/835 , B01J23/868 , B01J37/0201 , B01J37/031 , B01J37/06 , C07C45/002 , C07C67/04 , C07C2601/14 , C07D223/10 , Y02P20/127 , Y02P20/52 , C07C31/08 , C07C35/08 , C07C69/14
摘要： This invention relates to a process for co-producing cyclohexanol and alkanol, including a cyclohexene esterification step and a cyclohexyl ester hydrogenation step. This invention further relates to a process for further producing cyclohexanone or caprolactam, starting from the co-producing process, and an apparatus for co-producing cyclohexanol and alkanol. The process for co-producing cyclohexanol and alkanol of this invention is environment-friendly, with low production cost and highly improved atom economy.
摘要翻译： 本发明涉及环己醇和链烷醇的共制造方法，包括环己烯酯化步骤和环己基酯氢化步骤。 本发明还涉及从共同制备方法开始进一步制备环己酮或己内酰胺的方法，以及共同制备环己醇和链烷醇的装置。 本发明的环己醇和链烷醇的共制造方法环保，生产成本低，原子经济性高。
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