Preparation of alkylcyclohexanol polyoxyethylene ether emulsifier and application thereof

    公开(公告)号:US12116455B2

    公开(公告)日:2024-10-15

    申请号:US17113309

    申请日:2020-12-07

    CPC classification number: C08G65/2648 C08G65/2609 C09K23/00

    Abstract: The disclosure discloses preparation and application of an alkylcyclohexanol polyoxyethylene ether emulsifier, and belongs to the technical field of surfactants. By performing ethylene oxide adducting on alkylcyclohexanol polyoxyethylene ether (1-3) and using a strong alkaline suspension dispersed in the solvent and alkylcyclohexanol polyoxyethylene ether (1-3) as a catalyst, nonionic surfactants alkylcyclohexanol polyoxyethylene ether (5-17) are synthesized. The products all have good characteristics of nonionic surfactants, and contain lower content of polyethylene. The products such as nonylcyclohexanol ethoxylate (7) and nonylcyclohexanol ethoxylate (9) have emulsifying properties similar to the emulsifying property of nonylphenol ethoxylate (10), and therefore can substitute for nonylphenol ethoxylate (10) as an emulsifier.

    Perfluoro surfactant and preparation method therefor

    公开(公告)号:US12018200B2

    公开(公告)日:2024-06-25

    申请号:US17293699

    申请日:2019-10-30

    Inventor: Ai Chen

    CPC classification number: C09K23/007 C08G65/007

    Abstract: A perfluoro surfactant and a preparation method therefor. A carbon fluorine bond is not prone to break when the perfluoro surfactant is used as an emulsifier in a fluorine polymer reaction, such that the average molecular weight of a fluorine polymer generated in the fluorine polymer reaction is significantly increased. The preparation method is implemented in a continuous micro-channel reaction system, where the retention time of a reactant in the reaction system can be greatly shortened to few minutes or even seconds, a back-mixing phenomenon in the reaction system can be basically eliminated, and thus the occurrence of a side reaction, an optical coupling reaction, can be greatly reduced. There are reaction stages comprising an ozonization reaction and a photo-oxidation reaction.

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