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    METHOD FOR PRODUCING NANOPARTICLES FROM A LIQUID MIXTURE
    42.
    发明申请
    METHOD FOR PRODUCING NANOPARTICLES FROM A LIQUID MIXTURE 审中-公开

    公开(公告)号：US20200231438A1

    公开(公告)日：2020-07-23

    申请号：US16494695

    申请日：2018-03-16

    Applicant: TECHNISCHE UNIVERSITÄT BERLIN

    Inventor： Sebastian SCHIMEK ,  Christian Oliver PASCHEREIT ,  Moritz SIEBER

    IPC: C01B13/34 ,  C01G49/06 ,  C01G45/02 ,  C01G9/03 ,  C01F7/30 ,  C01G23/07 ,  C01B33/18 ,  B01J10/00 ,  B01J19/26

    Abstract: A process for the production of nanoparticles from a liquid mixture comprising at least one precursor and at least one solvent in a reactor with continuous through-flow comprises the steps of feeding at least one oxygen-containing gas inflow stream having a temperature into the at least one reactor, adding at least one fuel having a temperature to the oxygen-containing gas inflow stream, wherein the fuel and the oxygen-containing gas inflow stream form a homogeneous ignitable mixture having a temperature, wherein the temperature of the homogeneous ignitable mixture is above the autoignition temperature of the homogeneous ignitable mixture, introducing at least one precursor-solvent mixture into the homogeneous ignitable mixture; autoignition of the ignitable mixture of oxygen-containing gas and fuel after an ignition delay time to form a stabilized flame and reacting the precursor-solvent mixture in the stabilized flame to form nanoparticles from the metal salt precursor, removing the formed nanoparticles.

    Process for solid-state polycondensation
    43.
    发明授权
    Process for solid-state polycondensation 有权

    公开(公告)号：US10604620B2

    公开(公告)日：2020-03-31

    申请号：US14367390

    申请日：2012-12-18

    Applicant: Bühler Thermal Processes AG

    Inventor： Andreas Christel

    IPC: C08G63/181 ,  C08G63/80 ,  C08G63/78 ,  C08G63/183 ,  B01J10/00

    Abstract: A method and an apparatus for solid-state polycondensation of polyesters, preferably polyethylene terephthalate and/or copolymers thereof. The method and apparatus are both characterized by a solid-state polycondensation being performed with polyester prepolymer particles in a reaction chamber in which an absolute pressure is in the range from 10 mbar to 200 mbar, and a process gas flow in the range of an R-value of 0.005 to 0.05. The polycondensation is carried out over a time of from 2 to 30 hours and at a temperature of from 180° C. to 5° below a crystalline melting point of the polyester prepolymer particles in order to achieve an intrinsic viscosity of from 0.70 to 0.95 dl/g. The R value is defined as a ratio of an hourly amount of process gas (in kg) flowing through the reaction space to an hourly amount of polymer (in kg) flowing through the reaction space: R = m ⁡ ( gas ) ⁢ / ⁢ h m ⁡ ( polymer ) ⁢ / ⁢ h .

    Packing
    44.
    发明授权
    Packing 有权

    公开(公告)号：US10596484B2

    公开(公告)日：2020-03-24

    申请号：US15924654

    申请日：2018-03-19

    Applicant: IHI Corporation

    Inventor： Yoshiyuki Iso ,  Jian Huang ,  Mariko Saga ,  Shinsuke Matsuno ,  Hiroyuki Uchida ,  Naoki Fujiwara ,  Kenji Takano ,  Kenji Tokuda ,  Shiko Nakamura

    IPC: B01J19/32 ,  B01D3/26 ,  B01D53/18 ,  B01J10/00

    Abstract: A packing has a plurality of sheet materials spaced and arranged in parallel, and liquid flows along the flat surface thereof in a standing use state. Each sheet material has at least one member group including a plurality of support members arranged such that the upper end of the uppermost support member corresponds to the upper end of the sheet material and the lower end of the lowermost support member corresponds to the lower end of the sheet material. Each support member has a pair of support walls parallel to the liquid flow direction and perpendicular to the sheet material surface, and a bridging part connecting the support walls. A sandwiching structure is formed that one sheet material is held by at least one support member attached thereto and at least one support member attached to an adjacent sheet material, and it extends linearly through the plurality of sheet materials.

    REACTOR SYSTEM
    47.
    发明申请
    REACTOR SYSTEM 审中-公开

    公开(公告)号：US20190247815A1

    公开(公告)日：2019-08-15

    申请号：US16296761

    申请日：2019-03-08

    Applicant: Rachel Burton ,  Greg Austic ,  Xiaohu Fan

    Inventor： Rachel Burton ,  Greg Austic ,  Xiaohu Fan

    IPC: B01J8/00 ,  B01J19/18 ,  B01J10/00 ,  B01J19/00 ,  B01J4/00

    CPC classification number: B01J8/008 ,  B01J4/004 ,  B01J10/00 ,  B01J19/006 ,  B01J19/1881 ,  B01J2208/00796 ,  B01J2219/00006 ,  B01J2219/00094

    Abstract: A reactor tank is provided having an enzyme inlet, a heating jacket positioned around the exterior center of the tank, a gas outlet for communicating with a vacuum apparatus to create a vacuum within the reactor tank and for communicating with a condensing unit, a first gas inlet for receiving gas from a feed tank and a first liquid outlet for recirculating the liquid from the first liquid outlet back to the feed tank. The reactor tank further includes a sparged unit and a screen positioned within the tank between the sparged unit and the first liquid outlet, where the sparged unit is connected to the first gas inlet for receiving gas from the feed tank. The reactor tank is utilized in a reactor system further including a condensing unit, vacuum pump or venturi valve, a first feed tank connected to the first gas inlet, a coalescer having at least one circulation pipe and a first circulation pump connected to the first liquid outlet for circulating a portion of the liquid dispelled from the liquid outlet to the coalescer, which after being filtered through coalescer is recirculated through circulation pipe back to the first feed tank.

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