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    SPINEL CATALYSTS FOR WATER AND HYDROCARBON OXIDATION
    43.
    发明申请
    SPINEL CATALYSTS FOR WATER AND HYDROCARBON OXIDATION 有权
    用于水和碳氢化合物的螺旋体催化剂

    公开(公告)号：US20130040806A1

    公开(公告)日：2013-02-14

    申请号：US13643439

    申请日：2011-06-24

    Applicant: G. Charles Dismukes ,  Martha Greenblatt

    Inventor： G. Charles Dismukes ,  Martha Greenblatt

    IPC: B01J35/02 ,  B01J23/34 ,  B01J23/78 ,  B01J31/26 ,  H01G9/00 ,  C07B41/02 ,  C25B11/06 ,  C25B9/00 ,  C02F1/461 ,  B01J23/04 ,  B01J23/75

    CPC classification number: C25B1/003 ,  B01J35/004 ,  C25B3/02 ,  Y02E60/366 ,  Y02P20/135 ,  Y10S502/524 ,  Y10T29/417

    Abstract: A catalyst for the electrolysis of water molecules and hydrocarbons, the catalyst including catalytic groups comprising A1-xB2−yB′yO4 spinels having a cubical M4O4 core, wherein A is Li or Na, B and B′ are independently any transition metal or main group metal, M is B, B′, or both, x is a number from 0 to 1, and y is a number from 0 to 2. In photo-electrolytic applications, a plurality of catalytic groups are supported on a conductive support substrate capable of incorporating water molecules. At least some of the catalytic groups, supported by the support substrate, are able to catalytically interact with water molecules incorporated into the support substrate. The catalyst can also be used as part of a photo-electrochemical cell for the generation of electrical energy.

    Abstract translation: 用于水分子和烃的电解的催化剂，包括具有立方M4O4芯的Al-xB2-yB'yO4尖晶石的催化剂的催化剂，其中A为Li或Na，B和B'独立地为任何过渡金属或主族 金属，M是B，B'或两者，x是0至1的数，y是0至2的数。在光电解应用中，多个催化基团负载在能够承载的导电支撑基板上 并入水分子。 由支持底物负载的至少一些催化基团能够与结合到载体基底中的水分子进行催化相互作用。 催化剂也可以用作用于产生电能的光电池的一部分。

    Ionic liquids
    45.
    发明授权
    Ionic liquids 有权
    离子液体

    公开(公告)号：US08088917B2

    公开(公告)日：2012-01-03

    申请号：US12128893

    申请日：2008-05-29

    Applicant: Stewart Forsyth ,  Kenneth R. Seddon ,  Keith Whiston ,  Sudhir Aki

    Inventor： Stewart Forsyth ,  Kenneth R. Seddon ,  Keith Whiston ,  Sudhir Aki

    IPC: C07D223/00 ,  C07D223/14 ,  C07D487/00 ,  C07D491/00 ,  C07D513/00 ,  C07D405/00 ,  C07D409/00 ,  C07D223/04 ,  C07D295/00 ,  C09K3/00

    CPC classification number: C07D211/14 ,  C07D223/04 ,  C25B3/02

    Abstract: The invention relates to an ionic liquid composition and a method for preparing the ionic liquid. The ionic liquid comprises a cation containing the Formula I, as herein disclosed, and wherein: n is 2, R1 is selected from the group consisting of: H, C1-C12 alkyl, aryl or together with R2 may form a heterocyclic ring, and R2 is selected from the group consisting of: H, C1-C12 alkyl, aryl or together with R1 may form a heterocyclic ring, and R3 is selected from the group consisting of hydrogen and C1-C12 alkyl, and wherein R1 and R2 are not simultaneously selected from hydrogen.

    Abstract translation: 本发明涉及一种离子液体组合物和一种制备离子液体的方法。 离子液体包含本文公开的含有式I的阳离子，其中n为2，R 1选自：H，C 1 -C 12烷基，芳基或与R 2一起形成杂环，并且 R 2选自：H，C 1 -C 12烷基，芳基或与R 1一起形成杂环，并且R 3选自氢和C 1 -C 12烷基，并且其中R 1和R 2不是 同时选自氢。

    Method for preparing a polycarboxylic composition comprising an electrochemical oxidation stage of a monosaccharide composition
    47.
    发明授权
    Method for preparing a polycarboxylic composition comprising an electrochemical oxidation stage of a monosaccharide composition 失效
    制备包含单糖组合物的电化学氧化阶段的多元羧酸组合物的方法

    公开(公告)号：US07728170B2

    公开(公告)日：2010-06-01

    申请号：US10528356

    申请日：2003-09-12

    Applicant: Francis Marsais ,  Christian Feasson ,  Guy Queguiner ,  Mathias Ibert ,  Serge Comini ,  Jean-Marc Grossel

    Inventor： Francis Marsais ,  Christian Feasson ,  Guy Queguiner ,  Mathias Ibert ,  Serge Comini ,  Jean-Marc Grossel

    IPC: C25B3/02

    CPC classification number: C07C59/285 ,  C25B3/02

    Abstract: A method for preparing a polycarboxylic composition, includes a stage in which a monosaccharide composition undergoes an electrochemical oxidation treatment carried out in the absence of sodium hypochlorite and in the presence of a) an amine oxide and b) a carbon-based anode. Preferably, the anode is selected from the group comprising carbon felt and granular active carbon. The electrochemical oxidation treatment can be carried out advantageously at a pH, preferably of between 11.5 and 14. The method makes it possible to obtain novel products, especially 2-carboxy-2, 3, 4-trihydroxypentane-dioicious acid, the salts and derivatives thereof.

    Abstract translation: 一种制备多元羧酸组合物的方法，包括其中单糖组合物在不存在次氯酸钠的情况下进行电化学氧化处理并在a）氧化胺和b）碳基阳极存在下进行的阶段。 优选地，阳极选自碳毡和颗粒状活性炭。 电化学氧化处理可以有利地在pH值下进行，优选在11.5和14之间。该方法可以获得新产物，特别是2-羧基-2,3,4-三羟基戊烷二恶酸，其盐和衍生物 其中。

    IONIC LIQUIDS
    48.
    发明申请
    IONIC LIQUIDS 有权
    离子液体

    公开(公告)号：US20080296531A1

    公开(公告)日：2008-12-04

    申请号：US12128893

    申请日：2008-05-29

    Applicant: Keith Whiston ,  STEWART FORSYTH ,  Kenneth R. Seddon

    Inventor： Keith Whiston ,  STEWART FORSYTH ,  Kenneth R. Seddon

    IPC: C09K3/00

    CPC classification number: C07D211/14 ,  C07D223/04 ,  C25B3/02

    Abstract: The invention relates to an ionic liquid composition and a method for preparing the ionic liquid. The ionic liquid comprises a cation containing the Formula I, as herein disclosed, and wherein: n is 1 or 2, R1 is selected from the group consisting of: H, C1-C12 alkyl, aryl or together with R2 may form a heterocyclic ring, and R2 is selected from the group consisting of: H, C1-C12 alkyl, aryl or together with R1 may form a heterocyclic ring, and R3 is selected from the group consisting of hydrogen and C1-C12 alkyl, wherein if n is 1, then R3 is C1-C12 alkyl; and wherein R1 and R2 are not simultaneously selected from hydrogen. The method for the preparation of the ionic liquid composition provided herein starts with at least one N-substitution of the compound of Formula II, as herein disclosed, and wherein: n is 1 or 2, R3 is selected from the group consisting of hydrogen and C1-C12 alkyl, wherein if n is 1, then R3 is C1-C12 alkyl. Further provided is a use of the ionic liquid in a chemical method including at least a method for electrochemical oxidation.

    Abstract translation: 本发明涉及一种离子液体组合物和一种制备离子液体的方法。 离子液体包含如本文公开的含有式I的阳离子，其中n为1或2，R1选自：H，C1-C12烷基，芳基或与R2一起形成杂环 并且R 2选自：H，C 1 -C 12烷基，芳基或与R 1一起可以形成杂环，并且R 3选自氢和C 1 -C 12烷基，其中如果n是1 那么R 3是C 1 -C 12烷基; 并且其中R1和R2不同时选自氢。 制备本文提供的离子液体组合物的方法开始于本文公开的式II化合物的至少一个N-取代，并且其中：n为1或2，R 3选自氢和 C 1 -C 12烷基，其中如果n是1，那么R 3是C 1 -C 12烷基。 还提供了一种使用离子液体的化学方法，至少包括一种电化学氧化方法。

    Electrochemical deblocking solution for electrochemical oligomer synthesis on an electrode array
    49.
    发明申请
    Electrochemical deblocking solution for electrochemical oligomer synthesis on an electrode array 审中-公开
    用于电极阵列上电化学低聚物合成的电化学去块溶液

    公开(公告)号：US20070034513A1

    公开(公告)日：2007-02-15

    申请号：US11090096

    申请日：2005-03-25

    Applicant: Karl Maurer ,  John Cooper ,  Michael Strathmann

    Inventor： Karl Maurer ,  John Cooper ,  Michael Strathmann

    IPC: C12Q1/68

    CPC classification number: C25B3/00 ,  B01J19/0046 ,  B01J2219/00653 ,  C07B41/02 ,  C07B41/06 ,  C07C50/00 ,  C07C309/30 ,  C07D213/16 ,  C07H21/02 ,  C07H21/04 ,  C25B3/02 ,  C25B3/04 ,  C25B3/10 ,  Y02P20/55

    Abstract: There is disclosed an electrochemical deblocking solution for use on an electrode microarray. There is further disclosed a method for electrochemical synthesis on an electrode array using the electrochemical deblocking solution. The solution and method are for removing acid-labile protecting groups for synthesis of oligonucleotides, peptides, small molecules, or polymers on a microarray of electrodes while substantially improving isolation of deblocking to active electrodes. The method comprises applying a voltage or a current to at least one electrode of an array of electrodes. The array of electrodes is covered by the electrochemical deblocking solution.

    Abstract translation: 公开了一种用于电极微阵列的电化学去块解决方案。 还公开了使用电化学去块溶液在电极阵列上进行电化学合成的方法。 该解决方案和方法是用于在电极的微阵列上除去用于合成寡核苷酸，肽，小分子或聚合物的酸不稳定保护基团，同时基本上改善了去活化对活性电极的分离。 该方法包括向电极阵列的至少一个电极施加电压或电流。 电极阵列被电化学去块溶液覆盖。

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