SYNTHESIS OF ZEOLITES USING AN ORGANOAMMONIUM COMPOUND
    42.
    发明申请
    SYNTHESIS OF ZEOLITES USING AN ORGANOAMMONIUM COMPOUND 审中-公开
    使用有机金属化合物合成ZOOLITE

    公开(公告)号:US20150158020A1

    公开(公告)日:2015-06-11

    申请号:US14552654

    申请日:2014-11-25

    申请人: UOP LLC

    摘要: A method for synthesizing a zeolite includes the steps of: (a) preparing an aqueous mixture comprising water, a substituted hydrocarbon and an amine; (b) reacting the aqueous mixture; (c) obtaining a solution comprising an organoammonium product; (d) forming a reaction mixture including reactive sources of M, Al, Si, optionally seeds of a layered material L, and the solution, wherein M is a metal; and (e) heating the reaction mixture to form the zeolite. The substituted hydrocarbon can be an α,ω-dihalogen substituted alkane, and the amine is preferably essentially incapable of undergoing pyramidal inversion.

    摘要翻译: 合成沸石的方法包括以下步骤:(a)制备含水,取代的烃和胺的含水混合物; (b)使含水混合物反应; (c)获得包含有机铵产物的溶液; (d)形成包含M,Al,Si的反应性源的反应混合物,任选的层状材料L的种子和溶液,其中M是金属; 和(e)加热反应混合物以形成沸石。 取代的烃可以是α,ω-二卤素取代的烷烃,并且胺优选基本上不能经历锥体反转。

    Synthesis of MSE-framework type molecular sieves
    43.
    发明授权
    Synthesis of MSE-framework type molecular sieves 有权
    MSE-骨架型分子筛的合成

    公开(公告)号:US09035058B2

    公开(公告)日:2015-05-19

    申请号:US14541777

    申请日:2014-11-14

    IPC分类号: C07D453/02 C07D211/12

    摘要: A method of synthesizing a crystalline molecular sieve having an MSE framework type comprises crystallizing a reaction mixture comprising a source of water, a source of an oxide of a tetravalent element, Y, selected from at least one of silicon, tin, titanium, vanadium, and germanium, optionally a source of a trivalent element, X, a source of an alkali or alkaline earth metal, M, and a source of organic dications, Q, such as 3-hydroxy-1-(4-(1-methylpiperidin-1-ium-1-yl)butyl)quinuclidin-1-ium, 3-hydroxy-1-(5-(1-methylpiperidin-1-ium-1-yl)pentyl)quinuclidin-1-ium, 1,1′-(butane-1,4-diyl)bis(1-methylpiperidin-1-ium), 1,1′-(pentane-1,5-diyl)bis(1-methylpiperidin-1-ium), 1,1′-(hexane-1,6-diyl)bis(1-methylpiperidin-1-ium), and 1,1′-((3as,6as)-octahydropentalene-2,5-diyl)bis(1-methylpiperidin-1-ium).

    摘要翻译: 合成具有MSE骨架类型的结晶分子筛的方法包括使包含水源,四价元素的氧化物源Y的反应混合物结晶,Y选自硅,锡,钛,钒, 和锗,任选的三价元素的源,X,碱金属或碱土金属的源,M和有机二价元素的Q,例如3-羟基-1-(4-(1-甲基哌啶-4-基) (1-(1-甲基哌啶-1-基)戊基)奎宁环ium,1,1'ium基-1- yl基)丁基)奎宁环ium,3-羟基-1- - (丁烷-1,4-二基)双(1-甲基哌啶-1-基),1,1' - (戊烷-1,5-二基)双(1-甲基哌啶-1-基),1,1' - (己烷-1,6-二基)双(1-甲基哌啶-1-基)和1,1' - ((3as,6as) - 八氢二烯-2,5-二基)双(1-甲基哌啶-1-基) ium)。

    Salt forms of [R-(R*,R*)]-2-(4-fluorophenyl)-beta, alpha-dihydroxy-5-(1-methylethyl)-3-phenyl-4-[(phenylamino)carbonyl]-1H-pyrrole-1-heptanoic acid
    47.
    发明授权
    Salt forms of [R-(R*,R*)]-2-(4-fluorophenyl)-beta, alpha-dihydroxy-5-(1-methylethyl)-3-phenyl-4-[(phenylamino)carbonyl]-1H-pyrrole-1-heptanoic acid 有权
    盐形式的[R-(R *,R *)] -2-(4-氟苯基) - ,α-二羟基-5-(1-甲基乙基)-3-苯基-4 - [(苯基氨基)羰基] 1H-吡咯-1-庚酸

    公开(公告)号:US08236966B2

    公开(公告)日:2012-08-07

    申请号:US12966488

    申请日:2010-12-13

    IPC分类号: C07D207/00

    摘要: Novel salt forms of [R—(R*,R*)]-2-(4-fluorophenyl)-β,δ-dihydroxy-5-(1-methylethyl)-3-phenyl-4-[(phenylamino)carbonyl]-1H-pyrrole-1-heptanoic acid characterized by their X-ray powder diffraction pattern and solid-state NMR spectra are described, as well as methods for the preparation and pharmaceutical composition of the same, which are useful as agents for treating hyperlipidemia, hypercholesterolemia, osteoporosis, benign prostatic hyperplasia, and Alzheimer's Disease.

    摘要翻译: [R-(R *,R *)] - 2-(4-氟苯基) - ,b-的新型盐形式,δ-二羟基-5-(1-甲基乙基)-3-苯基-4 - [(苯基氨基)羰基 ] -1H-吡咯-1-庚酸,其特征在于它们的X射线粉末衍射图和固态NMR光谱,以及其制备方法和药物组合物,其可用作治疗高脂血症的药剂 ,高胆固醇血症,骨质疏松症,良性前列腺增生症和阿尔茨海默病。