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    Organo-1-oxa-4-azonium cyclohexane compounds
    1.
    发明授权
    Organo-1-oxa-4-azonium cyclohexane compounds 有权

    公开(公告)号：US10654817B2

    公开(公告)日：2020-05-19

    申请号：US15981148

    申请日：2018-05-16

    Applicant: UOP LLC

    Inventor： Christopher P. Nicholas ,  Mark A. Miller ,  Melissa M. Galey ,  Benjamin D. Yuhas ,  Sesh Prabhakar

    IPC: C07D295/037 ,  C07D295/023 ,  C07D295/027

    Abstract: Novel 1-oxa-4-azonium cyclohexane salts are described. These compounds can be used as structure directing agents, and they overcome many of the typical problems associated with OSDA synthesis and subsequent zeolite synthesis. Methods for synthesis of the 1-oxa-4-azonium cyclohexane salts from a variety of starting materials are also described. A substituted hydrocarbon is added to water to form a mixture, and a 1-oxa-4-azacyclohexane derivative is then added. The reaction mixture stirred until a solution containing the 1-oxa-4-azonium cyclohexane salt is obtained.

    Organo-1-oxa-4-azonium cyclohexane compounds
    2.
    发明授权
    Organo-1-oxa-4-azonium cyclohexane compounds 有权

    公开(公告)号：US10597373B2

    公开(公告)日：2020-03-24

    申请号：US15981435

    申请日：2018-05-16

    Applicant: UOP LLC

    Inventor： Christopher P. Nicholas ,  Mark A. Miller ,  Melissa M. Galey ,  Benjamin D. Yuhas ,  Sesh Prabhakar

    IPC: C07D295/037 ,  C07D295/023 ,  C07D295/027

    Abstract: Novel 1-oxa-4-azonium cyclohexane salts are described. These compounds can be used as structure directing agents, and they overcome many of the typical problems associated with OSDA synthesis and subsequent zeolite synthesis. Methods for synthesis of the 1-oxa-4-azonium cyclohexane salts from a variety of starting materials are also described. A substituted hydrocarbon is added to water to form a mixture, and a 1-oxa-4-azacyclohexane derivative is then added. The reaction mixture stirred until a solution containing the 1-oxa-4-azonium cyclohexane salt is obtained.

    ZEOLITES USING AN ORGANO-1-OXA-4-AZONIUMCYCLOHEXANE COMPOUND
    7.
    发明申请
    ZEOLITES USING AN ORGANO-1-OXA-4-AZONIUMCYCLOHEXANE COMPOUND 有权
    使用有机-1-氧代-4-亚氨基半胱氨酸六氢化合物的沸石

    公开(公告)号：US20160159655A1

    公开(公告)日：2016-06-09

    申请号：US14561112

    申请日：2014-12-04

    Applicant: UOP LLC

    Inventor： Christopher P. Nicholas ,  Mark A. Miller ,  Melissa M. Galey

    IPC: C01B39/32 ,  B01J29/60 ,  B01J37/00 ,  C01B39/04

    CPC classification number: C01B39/32 ,  B01J29/60 ,  B01J37/0018 ,  C01B39/04 ,  C01B39/48

    Abstract: A method for synthesizing a zeolite is described. The method may include the steps of: (a) preparing an aqueous mixture comprising water, a substituted hydrocarbon, and a 1-oxa-4-azacyclohexane derivative; (b) reacting the aqueous mixture; (c) obtaining a solution comprising an organo-1-oxa-4-azoniumcyclohexane compound; (d)) forming a reaction mixture comprising reactive sources of Al, and Si, and the solution; and (e) heating the reaction mixture to form the zeolite.

    Abstract translation: 对沸石的合成方法进行说明。 该方法可以包括以下步骤：（a）制备含水，取代的烃和1-氧杂-4-氮杂环己烷衍生物的含水混合物; （b）使含水混合物反应; （c）得到包含有机-1-氧杂-4-氮鎓环己烷化合物的溶液; （d））形成包含Al和Si的反应性源的反应混合物和溶液; 和（e）加热反应混合物以形成沸石。

    UZM-39 ALUMINOSILICATE ZEOLITE
    9.
    发明申请
    UZM-39 ALUMINOSILICATE ZEOLITE 有权
    UZM-39铝酸钠沸石

    公开(公告)号：US20150025287A1

    公开(公告)日：2015-01-22

    申请号：US14507941

    申请日：2014-10-07

    Applicant: UOP LLC

    Inventor： Christopher P. Nicholas ,  Mark A. Miller

    IPC: B01J20/18 ,  B01J29/80 ,  B01J29/87 ,  C07C2/66

    CPC classification number: B01J43/00 ,  B01D15/08 ,  B01J20/18 ,  B01J29/70 ,  B01J29/80 ,  B01J29/86 ,  B01J29/87 ,  B01J29/88 ,  B01J35/002 ,  C01B39/023 ,  C01B39/46 ,  C01B39/48 ,  C07C2/66 ,  C07C2/76 ,  C07C7/13 ,  C07C2529/70 ,  C10G47/20

    Abstract: A new family of coherently grown composites of TUN and IMF zeotypes have been synthesized. These zeolites are represented by the empirical formula. NanMmk+TtAl1-xExSiyOz where “n” is the mole ratio of Na to (Al+E), M represents a metal or metals from zinc, Group 1, Group 2, Group 3 and or the lanthanide series of the periodic table, “m” is the mole ratio of M to (Al+E), “k” is the average charge of the metal or metals M, T is the organic structure directing agent or agents, and E is a framework element such as gallium. These zeolites are similar to TNU-9 and IM-5 but are characterized by unique compositions and synthesis procedures and have catalytic properties for carrying out various hydrocarbon conversion processes and separation properties for carrying out various separations.

    Abstract translation: 已经合成了一系列连续生长的TUN和IMF染色体型复合物。 这些沸石由经验公式表示。 NanMmk + TtAl1-xExSiyOz其中“n”是Na与（Al + E）的摩尔比，M表示来自锌，第1族，第2族，第3族和/或周期表的镧系的金属或金属， m“是M与（Al + E）的摩尔比，”k“是金属或金属M的平均电荷，T是有机结构导向剂或试剂，E是骨架元素如镓。 这些沸石类似于TNU-9和IM-5，但是其特征在于独特的组成和合成方法，并且具有用于进行各种烃转化方法和用于进行各种分离的分离性能的催化性能。

    Aromatic transformation using UZM-39 aluminosilicate zeolite
    10.
    发明授权
    Aromatic transformation using UZM-39 aluminosilicate zeolite 有权
    使用UZM-39铝硅酸盐沸石进行芳香族转化

    公开(公告)号：US08927798B2

    公开(公告)日：2015-01-06

    申请号：US14100710

    申请日：2013-12-09

    Applicant: UOP LLC

    Inventor： Christopher P. Nicholas ,  Mark A. Miller ,  Antoine Negiz

    IPC: C07C2/66 ,  C07C4/18 ,  B01J29/70 ,  B01J35/00

    CPC classification number: C07C2/66 ,  B01J29/70 ,  B01J35/002 ,  C07C2529/70 ,  C07C15/02

    Abstract: A new family of coherently grown composites of TUN and IMF zeotypes has been synthesized and shown to be effective catalysts for aromatic transformation reactions. These zeolites are represented by the empirical formula: NanMmk+TtAll-xExSiyOz where “n” is the mole ratio of Na to (Al+E), M represents at least one meta, “m” is the mole ratio of M to (Al+E), “k” is the average charge of the metal or metals M, T is the organic structure directing agent or agents, “t” is the mole ratio of N from the organic structure directing agent or agents to (Al+E), and E is a framework element such as gallium. The process involves contacting at least a first aromatic with the coherently grown composites of TUN and IMF zeotypes to produce at least a second aromatic.

    Abstract translation: 已经合成了一系列TUN和IMF染色体的相干生长复合材料，并被证明是芳香族转化反应的有效催化剂。 这些沸石由经验式：NanMmk + TtAll-xExSiyOz表示，其中“n”是Na与（Al + E）的摩尔比，M表示至少一个元，“m”是M与（Al + E），“k”是金属或金属M的平均电荷，T是有机结构导向剂或试剂，“t”是N与有机结构导向剂或试剂与（Al + E）的摩尔比 ），E是诸如镓的骨架元素。 该方法包括使至少第一芳族化合物与TUN和IMF zeotype的相干生长的复合物接触以产生至少第二芳族化合物。

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